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1. 发明申请

WO2010093899A2 CATALYTIC MATERIALS FOR FABRICATING NANOSTRUCTURES 审中-公开
标题翻译：用于制造纳米结构的催化材料
公开(公告)号：WO2010093899A2
公开(公告)日：2010-08-19
申请号：PCT/US2010024069
申请日：2010-02-12
申请人： BABCOCK & WILCOX TECHNICAL SER , UT BATTELLE LLC , SEALS ROLAND D , MENCHHOFER PAUL A , HOWE JANE Y , WANG WEI
发明人： SEALS ROLAND D , MENCHHOFER PAUL A , HOWE JANE Y , WANG WEI
IPC分类号： B01J23/74 , B01J23/00 , B01J35/02 , B82B1/00
CPC分类号： B01J35/0013 , B01J21/08 , B01J23/74 , B01J23/745 , B01J31/0274 , B01J35/006 , B01J37/0072 , B01J37/033 , B01J37/18
摘要： Nano-catalysts that have utility for forming nanostructures and manufacturing nanomaterials are described. In some embodiments the nano-catalyst is formed from a powder-based substrate material and is some embodiments the nano-catalyst is formed from a solid-based substrate material. In some embodiments the substrate material may include metal, ceramic, or silicon or another metalloid. The nano-catalysts typically have metal nanoparticles disposed adjacent the surface of the substrate material. Methods of forming the nano-catalysts are disclosed. The methods typically include functionalizing the surface of the substrate material with a chelating agent, such as a chemical having dissociated carboxyl functional groups (-COO), that provides an enhanced affinity for metal ions. The functionalized substrate surface may then be exposed to a chemical solution that contains metal ions. The metal ions are then bound to the substrate material and may then be reduced, such as by a stream of gas that includes hydrogen, to form metal nanoparticles adjacent the surface of the substrate.
摘要翻译：描述了用于形成纳米结构和制造纳米材料的纳米催化剂。在一些实施方式中，纳米催化剂由粉末基底材料形成，并且在一些实施方式中，纳米催化剂由固体基底材料形成。在一些实施例中，衬底材料可以包括金属，陶瓷或硅或另一种准金属。纳米催化剂通常具有邻近基底材料表面设置的金属纳米颗粒。公开了形成纳米催化剂的方法。所述方法通常包括用螯合剂（例如具有解离的羧基官能团（-COO）的化学品）对基底材料的表面进行官能化，所述螯合剂对金属离子提供增强的亲和力。然后可以将官能化的基材表面暴露于含有金属离子的化学溶液。然后将金属离子结合到基底材料上，然后可以例如通过包含氢气的气流将其还原，以在基底表面附近形成金属纳米颗粒。

2. 发明申请

WO2010093905A2 METHOD OF PRODUCING CATALYTIC MATERIALS FOR FABRICATING NANOSTRUCTURES 审中-公开
标题翻译：生产用于制备纳米结构的催化材料的方法
公开(公告)号：WO2010093905A2
公开(公告)日：2010-08-19
申请号：PCT/US2010024078
申请日：2010-02-12
申请人： BABCOCK & WILCOX TECHNICAL SER , UT BATTELLE LLC , SEALS ROLAND D , MENCHHOFER PAUL A , HOWE JANE Y , WANG WEI
发明人： SEALS ROLAND D , MENCHHOFER PAUL A , HOWE JANE Y , WANG WEI
IPC分类号： B01J23/755 , B01J23/74 , B01J37/02 , B01J37/16 , B82B3/00
CPC分类号： B01J23/755 , B01J21/08 , B01J23/74 , B01J23/745 , B01J31/0274 , B01J35/0013 , B01J37/0072 , B01J37/033 , B01J37/18 , B82Y40/00 , Y10S977/773 , Y10S977/81 , Y10S977/892
摘要： Methods of fabricating nano-catalysts are described. In some embodiments the nano-catalyst is formed from a powder-based substrate material and is some embodiments the nano-catalyst is formed from a solid-based substrate material. In some embodiments the substrate material may include metal, ceramic, or silicon or another metalloid. The nano-catalysts typically have metal nanoparticles disposed adjacent the surface of the substrate material. The methods typically include functionalizing the surface of the substrate material with a chelating agent, such as a chemical having dissociated carboxyl functional groups (-COO), that provides an enhanced affinity for metal ions. The functionalized substrate surface may then be exposed to a chemical solution that contains metal ions. The metal ions are then bound to the substrate material and may then be reduced, such as by a stream of gas that includes hydrogen, to form metal nanoparticles adjacent the surface of the substrate.
摘要翻译：描述了制备纳米催化剂的方法。在一些实施方案中，纳米催化剂由粉末基底材料形成，并且是一些实施方案，纳米催化剂由固体基底材料形成。在一些实施方案中，基底材料可以包括金属，陶瓷或硅或另一种准金属。纳米催化剂通常具有邻近衬底材料的表面设置的金属纳米颗粒。所述方法通常包括用螯合剂（例如具有解离的羧基官能团（-COO）的化学物质）官能化底物材料的表面，其提供对金属离子的增强的亲和力。然后可以将功能化的衬底表面暴露于含有金属离子的化学溶液。然后将金属离子结合到衬底材料上，然后可以例如通过包括氢的气体流来还原，以形成邻近衬底表面的金属纳米颗粒。

3. 发明申请

WO2010093932A2 ANCHORED NANOSTRUCTURE MATERIALS AND BALL MILLING METHOD OF FABRICATION 审中-公开
标题翻译：锚固纳米结构材料和球磨法制造方法
公开(公告)号：WO2010093932A2
公开(公告)日：2010-08-19
申请号：PCT/US2010024114
申请日：2010-02-12
申请人： BABCOCK & WILCOX TECHNICAL SER , UT BATTELLE LLC , MENCHHOFER PAUL A , SEALS ROLAND D , CONTESCU CRISTIAN I , BURCHELL TIMOTHY D
发明人： MENCHHOFER PAUL A , SEALS ROLAND D , CONTESCU CRISTIAN I , BURCHELL TIMOTHY D
IPC分类号： B82B3/00 , B22F9/06 , C01B31/02
CPC分类号： B22F1/0062 , B22F1/0018 , B22F1/02 , B22F2998/10 , B82Y30/00 , C22C19/03 , C22C21/00 , B22F9/04 , B22F1/0085
摘要： Anchored nanostructure materials and methods for their fabrication are described. The anchored nanostructure materials may utilize nano-catalysts that are formed by mechanical ball milling of a metal powder. Nanostructures may be formed as anchored to the nano-catalyst by heating the nanocatalysts and then exposing the nano-catalysts to an organic vapor. The nanostructures are typically single wall or multi-wall carbon nanotubes.
摘要翻译：描述了锚定的纳米结构材料及其制造方法。锚定的纳米结构材料可以利用通过金属粉末的机械球磨形成的纳米催化剂。纳米结构可以通过加热纳米催化剂然后将纳米催化剂暴露于有机蒸气而形成锚定于纳米催化剂。纳米结构通常是单壁或多壁碳纳米管。

4. 发明申请

WO2010141113A3 NANO-MATERIAL AND METHOD OF FABRICATION 审中-公开
标题翻译：纳米材料和制造方法
公开(公告)号：WO2010141113A3
公开(公告)日：2011-02-24
申请号：PCT/US2010024121
申请日：2010-02-12
申请人： BABCOCK & WILCOX TECH SERV Y12 , UT BATTELLE LLC , MENCHHOFER PAUL A , SEALS ROLAND D , HOWE JANE Y , WANG WEI
发明人： MENCHHOFER PAUL A , SEALS ROLAND D , HOWE JANE Y , WANG WEI
IPC分类号： B82B1/00 , B82B3/00
CPC分类号： B01J23/755 , B01J23/745 , B01J23/75 , B82Y30/00 , C01B31/022 , C01B32/158 , Y10T428/298 , Y10T428/2991
摘要： A fluffy nano-material and method of manufacture are described. At 2000X magnification the fluffy nanomaterial has the appearance of raw, uncarded wool, with individual fiber lengths ranging from approximately four microns to twenty microns. Powder-based nanocatalysts are dispersed in the fluffy nanomaterial. The production of fluffy nanomaterial typically involves flowing about 125 cc/min of organic vapor at a pressure of about 400 torr over powder-based nano-catalysts for a period of time that may range from approximately thirty minutes to twenty-four hours.
摘要翻译：描述了蓬松的纳米材料和制造方法。在2000X放大倍数下，蓬松的纳米材料具有原始的未梳理羊毛的外观，单个纤维长度范围为约4微米至20微米。粉末状纳米催化剂分散在蓬松的纳米材料中。蓬松的纳米材料的生产通常涉及在大约400托的压力下将大约125cc /分钟的有机蒸气在粉末状纳米催化剂上流动约30分钟至24小时的时间。

5. 发明申请

WO2010141112A2 ANCHORED NANOSTRUCTURE MATERIALS AND METHOD OF FABRICATION 审中-公开
标题翻译：锚固的纳米结构材料和制造方法
公开(公告)号：WO2010141112A2
公开(公告)日：2010-12-09
申请号：PCT/US2010024098
申请日：2010-02-12
申请人： BABCOCK & WILCOX TECH SERV Y12 , UT BATTELLE LLC , SEALS ROLAND D , MENCHHOFER PAUL A , HOWE JANE Y , WANG WEI
发明人： SEALS ROLAND D , MENCHHOFER PAUL A , HOWE JANE Y , WANG WEI
IPC分类号： B82B1/00 , B82B3/00
CPC分类号： B01J2/006 , B01J21/08 , B01J23/745 , B01J31/0274 , B01J35/0013 , B01J35/006 , B01J37/0207 , B01J37/0209 , B01J37/033 , B01J37/18 , B22F1/025 , B82Y30/00 , B82Y40/00 , C01B32/15 , Y10T428/12181 , Y10T428/25 , Y10T428/2991 , Y10T428/2993
摘要： Anchored nanostructure materials and methods for their fabrication are described. The anchored nanostructure materials may utilize nano-catalysts that include powder-based or solid-based support materials. The support material may comprise metal, such as NiAl, ceramic, a cermet, or silicon or other metalloid. Typically, nanoparticles are disposed adjacent a surface of the support material. Nanostructures may be formed as anchored to nanoparticles that are adjacent the surface of the support material by heating the nano- catalysts and then exposing the nano-catalysts to an organic vapor. The nanostructures are typically single wall or multi-wall carbon nanotubes.
摘要翻译：描述了锚定的纳米结构材料及其制造方法。锚定的纳米结构材料可以使用包括基于粉末或固体的支撑材料的纳米催化剂。载体材料可以包括金属，例如NiAl，陶瓷，金属陶瓷或硅或其它准金属。通常，纳米颗粒邻近支撑材料的表面设置。纳米结构可以通过加热纳米催化剂然后将纳米催化剂暴露于有机蒸气而锚定在邻近载体材料表面的纳米颗粒上。纳米结构通常是单壁或多壁碳纳米管。

6. 发明申请

WO2010093926A3 COMPOSITE MATERIALS FORMED WITH ANCHORED NANOSTRUCTURES 审中-公开
标题翻译：形成具有锚定纳米结构的复合材料
公开(公告)号：WO2010093926A3
公开(公告)日：2010-12-02
申请号：PCT/US2010024107
申请日：2010-02-12
申请人： BABCOCK & WILCOX TECH SERV Y12 , UT BATTELLE LLC , SEALS ROLAND D , MENCHHOFER PAUL A , HOWE JANE Y , WANG WEI
发明人： SEALS ROLAND D , MENCHHOFER PAUL A , HOWE JANE Y , WANG WEI
IPC分类号： B82B3/00 , B82B1/00
CPC分类号： B01J23/74 , B01J23/745 , B01J35/0013 , B01J35/006 , B01J37/0207 , B01J37/0217 , B01J37/0221 , B01J37/033 , B01J37/18 , B22F1/025 , C22C29/08 , Y10S977/742 , Y10S977/773 , Y10S977/843
摘要： A method of forming nano-structure composite materials that have a binder material and a nanostructure fiber material is described. A precursor material may be formed using a mixture of at least one metal powder and anchored nanostructure materials. The metal powder mixture may be (a) Ni powder and (b) NiAl powder. The anchored nanostructure materials may comprise (i) NiAl powder as a support material and (ii) carbon nanotubes attached to nanoparticles adjacent to a surface of the support material. The process of forming nano-structure composite materials typically involves sintering the mixture under vacuum in a die. When Ni and NiAl are used in the metal powder mixture M3AI may form as the binder material after sintering. The mixture is sintered until it consolidates to form the nano-structure composite material.
摘要翻译：描述了形成具有粘合剂材料和纳米结构纤维材料的纳米结构复合材料的方法。前体材料可以使用至少一种金属粉末和锚定纳米结构材料的混合物形成。金属粉末混合物可以是（a）Ni粉末和（b）NiAl粉末。锚定的纳米结构材料可以包含（i）作为载体材料的NiAl粉末和（ii）附着到与载体材料的表面相邻的纳米颗粒上的碳纳米管。形成纳米结构复合材料的过程通常涉及在模具中在真空下烧结混合物。当在金属粉末混合物中使用Ni和NiAl时，在烧结之后可以形成M3Al作为粘合剂材料。将混合物烧结直至其固结形成纳米结构复合材料。

7. 发明申请

WO2007146508A3 HIGH VOLUME PRODUCTION OF NANOSTRUCTURED MATERIALS 审中-公开
标题翻译：纳米结构材料的大批量生产
公开(公告)号：WO2007146508A3
公开(公告)日：2008-04-03
申请号：PCT/US2007067993
申请日：2007-05-02
申请人： BWXT Y 12 LLC , UT BATTELLE LLC , RIPLEY EDWARD B , MORRELL JONATHAN S , SEALS ROLAND D , LUDTKA GERARD M
发明人： RIPLEY EDWARD B , MORRELL JONATHAN S , SEALS ROLAND D , LUDTKA GERARD M
IPC分类号： C01F17/00 , H05H1/26
CPC分类号： B01J19/126 , B01J23/74 , B01J2219/0847 , B01J2219/0871 , B01J2219/0879 , B01J2219/0894 , B22F9/12 , B22F2005/002 , B22F2999/00 , B82Y30/00 , B82Y40/00 , C01B32/162 , H05H1/46 , B22F2202/13
摘要： A system and method for high volume production of nanoparticles, nanotubes, and items incorporating nanoparticles and nanotubes. Microwave, radio frequency, or infrared energy vaporizes a metal catalyst which, as it condenses, is contacted by carbon or other elements such as silicon, germanium, or boron to form agglomerates. The agglomerates may be annealed to accelerate the production of nanotubes. Magnetic or electric fields may be used to align the nanotubes during their production. The nanotubes may be separated from the production byproducts in aligned or non-aligned configurations. The agglomerates may be formed directly into tools, optionally in compositions that incorporate other materials such as abrasives, binders, carbon-carbon composites, and cermets.
摘要翻译：用于大量生产纳米颗粒，纳米管和纳入纳米颗粒和纳米管的物质的系统和方法。微波，射频或红外能量汽化金属催化剂，其在凝结时与碳或其它元素如硅，锗或硼接触以形成附聚物。可以将附聚物退火以加速纳米管的生产。可以使用磁场或电场来在其生产期间对准纳米管。纳米管可以以对准或非对准构型与生产副产物分离。附聚物可以直接形成工具，任选地在包含其它材料如研磨剂，粘合剂，碳 - 碳复合材料和金属陶瓷的组合物中形成。

8. 发明申请

WO2007149684A3 CERAMIC NANOSTRUCTURES AND METHODS OF FABRICATION 审中-公开
标题翻译：陶瓷纳米结构和制造方法
公开(公告)号：WO2007149684A3
公开(公告)日：2008-02-14
申请号：PCT/US2007069922
申请日：2007-05-30
申请人： BWXT Y 12 L L C , RIPLEY EDWARD B , SEALS ROLAND D , MORRELL JONATHAN S
发明人： RIPLEY EDWARD B , SEALS ROLAND D , MORRELL JONATHAN S
IPC分类号： B32B9/00 , D01F9/12
CPC分类号： C01F7/027 , B81C99/002 , B82Y30/00 , C01B33/12 , C01F7/02 , C01G23/047 , C01P2004/03 , C01P2004/04 , C01P2004/16 , C01P2004/45 , C01P2004/62 , C01P2004/64 , H02N1/06 , Y10S977/734 , Y10S977/735 , Y10S977/754 , Y10S977/773 , Y10S977/774 , Y10S977/778 , Y10S977/779 , Y10S977/811 , Y10S977/813 , Y10S977/814 , Y10S977/815 , Y10S977/831 , Y10T428/29 , Y10T428/2913 , Y10T428/2927 , Y10T428/298 , Y10T428/2982 , Y10T428/2984
摘要： Structures and methods for the fabrication of ceramic nanostructures. Structures include metal particles, preferably comprising copper, disposed on a ceramic substrate. The structures are heated, preferably in the presence of microwaves, to a temperature that softens the metal particles and preferably forms a pool of molten ceramic under the softened metal particle. A nano-generator is created wherein ceramic material diffuses through the molten particle and forms ceramic nanostructures on a polar site of the metal particle. The nanostructures may comprise silica, alumina, titania, or compounds or mixtures thereof.
摘要翻译：用于制造陶瓷纳米结构的结构和方法。结构包括设置在陶瓷基板上的优选包含铜的金属颗粒。将结构加热，优选在微波存在下加热到软化金属颗粒的温度，并优选在软化的金属颗粒下形成熔融陶瓷池。产生纳米发生器，其中陶瓷材料扩散通过熔融颗粒并在金属颗粒的极性位置上形成陶瓷纳米结构。纳米结构可以包括二氧化硅，氧化铝，二氧化钛，或其化合物或其混合物。

9. 发明申请

WO2007143301A3 CONTROLLED ZONE MICROWAVE PLASMA SYSTEM 审中-公开
标题翻译：控制区微波等离子体系
公开(公告)号：WO2007143301A3
公开(公告)日：2008-10-02
申请号：PCT/US2007067860
申请日：2007-05-01
申请人： BWXT Y 12 LLC , RIPLEY EDWARD B , SEALS ROLAND D , MORRELL JONATHAN S
发明人： RIPLEY EDWARD B , SEALS ROLAND D , MORRELL JONATHAN S
IPC分类号： C23C16/00 , C23F1/00 , H01L21/306
CPC分类号： H01J37/3255 , H01J37/32192 , H01J37/32541 , H05H1/48 , H05H2001/463 , H05H2001/486
摘要： An apparatus and method for initiating a process gas plasma. A conductive plate having a plurality of conductive fingers is positioned in a microwave applicator. An arc forms between the conductive fingers to initiate the formation of a plasma. A transport mechanism may convey process materials through the plasma. A spray port may be provided to expel processed materials.
摘要翻译：一种用于启动处理气体等离子体的装置和方法。具有多个导电指状物的导电板位于微波施加器中。在导电指状物之间形成电弧以开始形成等离子体。运输机构可以通过等离子体传送过程材料。可以提供喷射口以排出加工的材料。

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