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1. 发明申请

WO1995031422A1 PROCESSES FOR THE PREPARATION OF FLUORINATED OLEFINS AND HYDROFLUOROCARBONS USING FLUORINATED OLEFIN 审中-公开
标题翻译：使用氟化烯烃制备氟化烯烃和氢氟代烃的方法
公开(公告)号：WO1995031422A1
公开(公告)日：1995-11-23
申请号：PCT/US1995005028
申请日：1995-04-24
申请人： ALLIEDSIGNAL INC.
发明人： ALLIEDSIGNAL INC. , VAN DER PUY, Michael , MADHAVAN, G., V., Bindu , THENAPPAN, Alagappan , TUNG, Hsueh, Sung
IPC分类号： C07C21/18
CPC分类号： C07C21/18 , C07C17/00 , C07C17/087 , C07C17/25 , C07C17/275 , C07C19/08
摘要： The invention relates to a cost effective and convenient process for the manufacture of fluorinated olefins of the formula RCF2CH=CH2 where R is CxClyFz and y + z = 2x + 1. The invention is also directed to a practical process for converting these olefins to hydrofluorocarbons via the catalyzed fluorination with hydrogen fluoride. Hydrofluorocarbons produced via this process have application as solvents among other uses.
摘要翻译：本发明涉及用于制造式RCF 2 CH = CH 2的氟化烯烃的成本有效和方便的方法，其中R是C x ClyF z且y + z = 2x + 1。本发明还涉及将这些烯烃转化为氢氟烃的实际方法通过氟化氢催化氟化。通过该方法生产的氢氟烃可用作其他用途的溶剂。

2. 发明申请

WO1997011043A1 PROCESS FOR THE PRODUCTION OF DIFLUOROMETHANE 审中-公开
标题翻译：二茂铁生产工艺
公开(公告)号：WO1997011043A1
公开(公告)日：1997-03-27
申请号：PCT/US1996014734
申请日：1996-09-13
申请人： ALLIEDSIGNAL INC.
发明人： ALLIEDSIGNAL INC. , CLEMMER, Paul, Gene , SMITH, Addison, Miles , TUNG, Hsueh, Sung , BASS, John, Stephen
IPC分类号： C07C19/08
CPC分类号： C07C17/206 , C07C19/08
摘要： The present invention provides a vapor phase process for the production of difluoromethane, HFC-32. The process of this invention provides for the preparation of HFC-32 by a process that exhibits both good product yield and selectively.
摘要翻译：本发明提供用于生产二氟甲烷HFC-32的气相方法。本发明的方法提供通过显示出良好的产物收率和选择性的方法制备HFC-32。

3. 发明申请

WO1997007084A1 PROCESS FOR THE MANUFACTURE OF 1,1,1,2-TETRAFLUOROETHANE 审中-公开
标题翻译： 1,1,1,2-四氢呋喃的制备方法
公开(公告)号：WO1997007084A1
公开(公告)日：1997-02-27
申请号：PCT/US1996013229
申请日：1996-08-16
申请人： ALLIEDSIGNAL INC.
发明人： ALLIEDSIGNAL INC. , TUNG, Hsueh, Sung , VISO, Nemesio, Rogelio , SMITH, Addison, Miles , MCKOWN, Jeffrey, Warren , FRIEDENSON, Jay, Philip , CLEMMER, Paul, Gene , CERRI, Gustavo , CHIU, Yuon , JASKOT, Stanley, Michael
IPC分类号： C07C19/08
CPC分类号： C07C19/08 , C07C17/10 , C07C17/206 , C07C17/21 , C07C17/269 , C07C17/383
摘要： This invention relates to a process for producing 1,1,1,2-tetrafluoroethane (HFC-134a). The process reacts, 1,1,1-trifluoro-2-chloroethane (HCFC-133a) and hydrogen fluoride in a first reactor. The product resulting from the first reaction step is brought to a second reactor together with trichloroethylene and hydrogen fluoride. The second reaction is conducted at a higher temperature than the first reactor. Optionally, HCl is removed prior to removal of the crude HFC-134a product. Unreacted HCFC-133a, trichloroethylene and hydrogen fluoride may be recycled back to the first reactor.
摘要翻译：本发明涉及一种生产1,1,1,2-四氟乙烷（HFC-134a）的方法。该方法在第一反应器中使1,1,1-三氟-2-氯乙烷（HCFC-133a）和氟化氢反应。将由第一反应步骤得到的产物与三氯乙烯和氟化氢一起送至第二反应器。第二反应在比第一反应器更高的温度下进行。任选地，在除去粗HFC-134a产物之前除去HCl。未反应的HCFC-133a，三氯乙烯和氟化氢可循环回第一反应器。

4. 发明申请

WO1997007083A1 PROCESS FOR THE PREPARATION OF HALOGENATED ALKANES 审中-公开
标题翻译：制备卤代烷烃的方法
公开(公告)号：WO1997007083A1
公开(公告)日：1997-02-27
申请号：PCT/US1996012341
申请日：1996-07-26
申请人： ALLIEDSIGNAL INC.
发明人： ALLIEDSIGNAL INC. , RYGAS, Tadeusz, Piotr , TUNG, Hsueh, Sung , SMITH, Addison, Miles
IPC分类号： C07C17/278
CPC分类号： C07C17/278 , C07C19/01
摘要： A process for the preparation of halogenated alkanes is provided . In particular, a process is provided for the highly selective preparation of haloalkanes, including 1,1,1,3,3-pentachloropropane, pentachlorobutane, and hepatchlorohexane, in good yield.
摘要翻译：提供卤代烷烃的制备方法。特别地，提供了以高产率高选择性地制备卤代烷烃的方法，包括1,1,1,3,3-五氯丙烷，五氯丁烷和肝四氟乙烷。

5. 发明申请

WO1995011875A1 PROCESS FOR PURIFYING 1,1-DICHLORO-2,2,2-TRIFLUOROETHANE AND 1-CHLORO-1,2,2,2-TETRAFLUOROETHANE 审中-公开
标题翻译：纯化1,1-二氯-2,2,2-三氟乙基和1 - 氯-1,2,2,2-四氢呋喃的方法
公开(公告)号：WO1995011875A1
公开(公告)日：1995-05-04
申请号：PCT/US1994010988
申请日：1994-09-29
申请人： ALLIEDSIGNAL INC.
发明人： ALLIEDSIGNAL INC. , TUNG, Hsueh, Sung
IPC分类号： C07C17/395
CPC分类号： B01J23/26 , C07C17/395 , C07C19/12
摘要： The invention relates to a novel process for purifying HCFC-123 and HCFC-124 comprising: (a) reacting a fluorination reaction product comprising HCFC-123 and HCFC-123a and/or HCFC-124 and HCFC-124a wherein at least one of said HCFC-123a or HCFC-124a is present in an amount not less than 5 weight percent relative to HCFC-123 or HCFC-124 respectively in the product with anhydrous HF in the presence of a fluorination catalyst under conditions such that the amount of HCFC-123a and/or HCFC-124a relative to HCFC-123 and/or HCFC-124 respectively in the product is reduced to less than 5 weight percent. The pure product (i.e., HCFC-123 or HCFC-124) may be used in a variety of applications including solvent, refrigerant, sterilant gas and blowing agent applications.
摘要翻译：本发明涉及一种用于净化HCFC-123和HCFC-124的新方法，包括：（a）使包含HCFC-123和HCFC-123a和/或HCFC-124和HCFC-124a的氟化反应产物与至少一种所述在氟化催化剂存在下，HCFC-123a或HCFC-124a的含量分别相对于HCFC-123或HCFC-124在无水HF中的含量为5重量％ 123a和/或HCFC-124a相对于HCFC-123和/或HCFC-124分别降低到小于5重量％。纯产品（即，HCFC-123或HCFC-124）可用于各种应用，包括溶剂，制冷剂，杀菌剂气体和发泡剂应用。

6. 发明申请

WO1994019301A1 PURIFICATION OF A COMPONENT OF A BINARY AZEOTROPE 审中-公开
标题翻译：二烯类化合物的组分的纯化
公开(公告)号：WO1994019301A1
公开(公告)日：1994-09-01
申请号：PCT/US1994001117
申请日：1994-01-31
申请人： ALLIEDSIGNAL INC.
发明人： ALLIEDSIGNAL INC. , CLEMMER, Paul, Gene , TUNG, Hsueh, Sung , SMITH, Addison, Miles
IPC分类号： C07C17/38
CPC分类号： C07C17/383 , B01D3/14 , Y10S203/13 , C07C19/08
摘要： The invention generally relates to a process for the purification of a component of a binary azeotrope in which the composition of the azeotrope changes by about 10 mole percent with pressure comprising: a) subjecting a binary azeotrope to a distillation step in which most of one of the binary components is removed as distillate (distillate 1) with the bottoms (bottoms 1) enriched in the other component; b) subjecting distillate 1 to at least one additional distillation step conducted at a different pressure in which most of the component recovered as bottoms 1 is removed as distillate 2 with the bottoms 2 enriched in the component enriched in distillate 1; c) optionally repeating step (b) as many times as desired; and d) recovering the desired purified component. The invention is particularly useful in the purification of pentafluoroethane in a pentafluoroethane/chloropentafluoroethane azeotrope.
摘要翻译：本发明一般涉及纯化二元共沸物组分的方法，其中共沸物的组成随着压力而变化约10摩尔％，包括：a）使二元共沸物经受蒸馏步骤，其中大部分将二元组分作为馏出物（馏出物1）除去富含其它组分的塔底物（塔底物1）; b）使馏出物1进行至少一个额外的蒸馏步骤，该蒸馏步骤以不同的压力进行，其中作为塔底物1回收的大部分组分作为馏出物2被除去，富含富含馏分1的组分的塔底物2富集; c）任选地重复步骤（b）多次; 和d）回收所需的纯化组分。本发明特别可用于五氟乙烷/氯五氟乙烷共沸物中五氟乙烷的提纯。

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