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    • 6. 发明申请
    • A METHOD AND SYSTEM FOR THE PRODUCTION OF A SPINNING DOPE COPOSITION
    • 生产纺丝DOPE复合物的方法和系统
    • WO2017178531A1
    • 2017-10-19
    • PCT/EP2017/058785
    • 2017-04-12
    • TREETOTEXTILE AB
    • OLSSON, CarinaHAGSTRÖM, BengtKÖHNKE, Tobias
    • D01D1/02D01F2/02C08B1/00C08J3/05
    • The present invention describes a method for the production of a spinning dope composition, said method comprising a homogenization involving vigorous mixing of a cellulosic pulp material in alkali solution, vigorous mixing implying supplying a power density to agitators used in the homogenization step of at least 150 k W/m 3 (k W supplied to agitators per mixed unit of liquid volume), and thereafter a dissolution involving mixing of the cellulosic pulp material in the alkali solution to obtain a spinning dope composition, wherein the power density supplied to agitators used in the dissolution step is maximum 75 k W/m 3 (k W supplied to agitators per mixed unit of liquid volume); and wherein the cellulosic pulp material in alkali solution is kept at a temperature of less than 0º C during the homogenization and during at least part of the dissolution. The present invention is also directed to a system intended for the production of a spinning dope composition.
    • 本发明描述了用于生产纺丝液组合物的方法,所述方法包括将纤维素纸浆材料在碱溶液中剧烈混合的均质化,剧烈混合,意味着向所使用的搅拌器提供功率密度 在匀化步骤中至少150kW / m 3(kW以液体体积的每个混合单位供应到搅拌器),然后进行涉及纤维素纸浆材料在碱溶液中混合的溶解以及 获得纺丝原液组合物,其中供给到溶解步骤中使用的搅拌器的功率密度最大为75kW / m 3(kW,以每个混合液体体积单位供应到搅拌器); 并且其中碱溶液中的纤维素纸浆材料保持在小于0℃的温度; C在均化期间和至少部分溶解期间。 本发明还涉及用于生产纺丝原液组合物的系统。
    • 7. 发明申请
    • PROCESS FOR SPINNING ALKALINE CELLULOSE SPIN DOPE
    • WO2023280779A1
    • 2023-01-12
    • PCT/EP2022/068459
    • 2022-07-04
    • TREETOTEXTILE AB
    • HEDLUND, ArturHAGSTRÖM, Bengt
    • D01D4/02D01D5/06D01F2/00D01F2/02D01D1/02
    • Disclosed is a process for spinning an alkaline cellulose spin dope, comprising dissolved cellulose, to cellulose filaments (10). The process comprising the steps of: - feeding the alkaline cellulose spin dope to at least one spinning head (20) with a plurality of holes (21), wherein the spinning head (20) comprises at least two parallel, rectangular spinneret dies (22), each with a plurality of holes (21), the spinneret dies (22) being arranged spaced apart with a flow spacing (23) in between them; - extruding the alkaline cellulose spin dope through the plurality of holes (21) into a flow (35) of aqueous alkaline coagulation bath liquid, the aqueous alkaline coagulation bath liquid comprising a sodium coagulation salt, whereby forming cellulose filaments (10), wherein the aqueous alkaline coagulation bath liquid flows through the flow spacing (23) and then past the spinneret dies (22) in a flow direction, the flow direction of the aqueous alkaline coagulation bath liquid being parallel to the direction in which the alkaline cellulose spin dope is extruded into the aqueous alkaline coagulation bath liquid; and - withdrawing the cellulose filaments (10) from the aqueous alkaline coagulation bath liquid.
    • 10. 发明申请
    • PROCESS FOR SPINNING DISSOLVED CELLULOSE
    • 纺制溶解纤维素的方法
    • WO2017178532A1
    • 2017-10-19
    • PCT/EP2017/058786
    • 2017-04-12
    • TREETOTEXTILE AB
    • HEDLUND, ArturKÖHNKE, Tobias
    • D01F2/02D01F13/02C08B1/00
    • The present invention relates to a process for forming cellulose fibers or film from dissolved cellulose. The process comprises the steps of: dissolving cellulose in an aqueous coagulation sodium salt solution to provide a cellulose spin dope; extruding the cellulose spin dope into a coagulation bath liquid comprising an aqueous coagulation sodium salt solution to provide cellulose fibers or film; withdrawing a portion of the coagulation bath comprising coagulation sodium salt and sodium hydroxide (NaOH); cooling the withdrawn portion of the coagulation bath to precipitate solid coagulation sodium salt to recover sodium hydroxide (NaOH) substantially free from the coagulation salt; and using at least a portion of the recovered sodium hydroxide (NaOH) in dissolving the cellulose to provide the cellulose spin dope.
    • 本发明涉及由溶解的纤维素形成纤维素纤维或薄膜的方法。 该方法包括以下步骤:将纤维素溶解在含水凝固钠盐溶液中以提供纤维素纺丝原液; 将纤维素纺丝原液挤入包含含水凝固钠盐溶液的凝固浴液中以提供纤维素纤维或薄膜; 取出包含凝固钠盐和氢氧化钠(NaOH)的一部分凝固浴; 冷却凝固浴的回收部分以沉淀固体凝固钠盐以回收基本上不含凝结盐的氢氧化钠(NaOH); 并使用至少一部分回收的氢氧化钠(NaOH)溶解纤维素以提供纤维素纺丝原液。