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1. 发明申请

WO2006124152A3 METHOD FOR USING A STATIC ELECTRIC FIELD TO INDUCE CRYSTALLIZATION AND TO CONTROL CRYSTAL FORM 审中-公开
标题翻译：使用静电场诱导结晶和控制晶体形式的方法
公开(公告)号：WO2006124152A3
公开(公告)日：2007-01-04
申请号：PCT/US2006013324
申请日：2006-04-11
申请人： UNIV POLYTECHNIC , GARETZ BRUCE A , MYERSON ALLAN S , ARNOLD STEPHEN , ABER JANICE E
发明人： GARETZ BRUCE A , MYERSON ALLAN S , ARNOLD STEPHEN , ABER JANICE E
IPC分类号： C07K14/47 , B01D9/00 , C07K1/30 , C12N13/00 , C30B7/00 , C30B29/54 , C30B30/02
CPC分类号： C30B29/58 , B01D9/005 , C07K1/306 , C12N13/00 , C30B7/00 , C30B29/54 , C30B30/02
摘要： Applying a strong static DC electric field to supersaturated aqueous glycine solutions resulted in the nucleation of the Y polymorph attributed to the electric-field induced orientation of the highly polar glycine molecules in large preexisting solute clusters, helping them organize into a crystalline structure. A method to induce crystallization and to prepare polymorphs and/or morphologies of materials by using a static electric field to cause nucleation and crystal growth to occur in a supersaturated solution in such a way as to obtain a crystal structure that would not normally appear without the use of the static electric field. Aqueous glycine solutions were prepared by combining solid glycine and water. Supersaturated solutions were generated by heating the tubes to 62- 640C and holding them at that temperature in an ultrasonicator overnight. Once the glycine was completely dissolved, the solutions were slowly cooled to room temperature. A chamber was constructed consisting of two brass electrodes separated by a 5 mm insulating gap, with a hole drilled down through the center, parallel to the gap-electrode interface, with a diameter large enough to accommodate the test tube. A DC voltage was applied across the electrodes; large enough to produce electric fields in the range of 400,000 to 800,000 V/m. Tests tubes containing the aged solutions were placed in the high-voltage chamber. Exposure of the aged solutions to fields of 600,000 V/m resulted in crystallization typically within 30-90 min. The onset of nucleation was observed visually by the formation of a needle-shaped crystallite.
摘要翻译：将强静态DC电场应用于过饱和甘氨酸水溶液导致Y型多晶型物的成核归因于大型预先存在的溶质簇中高极性甘氨酸分子的电场诱导取向，有助于它们组织成晶体结构。通过使用静电场引起结晶并制备材料的多晶型物和/或形态的方法，以使得在过饱和溶液中发生成核和晶体生长，以获得通常不会出现的晶体结构使用静电场。通过结合固体甘氨酸和水制备甘氨酸水溶液。通过将管加热至62-64℃并将其在超声波隔离器中保持在该温度下而产生过饱和溶液。一旦甘氨酸完全溶解，将溶液缓慢冷却至室温。由两个黄铜电极构成的腔体由两个黄铜电极隔开，绝缘间隔为5mm，孔穿过中心平行于间隙 - 电极界面钻出，直径足够大以容纳试管。跨电极施加直流电压; 足够大以产生在400,000至800,000V / m范围内的电场。将含有老化溶液的试管置于高压室中。将老化溶液暴露于600,000V / m的场中，结晶通常在30-90分钟内。通过形成针状微晶目测观察成核的开始。

2. 发明申请

WO1997049637A1 BENEFICIATION OF FURNACE DUST FOR THE RECOVERY OF CHEMICAL AND METAL VALUES 审中-公开
标题翻译：用于恢复化学和金属值的炉渣的受益
公开(公告)号：WO1997049637A1
公开(公告)日：1997-12-31
申请号：PCT/US1997011404
申请日：1997-06-26
申请人： METALS RECYCLING TECHNOLOGIES CORP. , MYERSON, Allan, S. , ROBINSON, Peter
发明人： METALS RECYCLING TECHNOLOGIES CORP.
IPC分类号： C01G09/00
CPC分类号： C01G9/02 , C21B13/006 , C22B3/12 , C22B3/14 , C22B3/46 , C22B5/10 , C22B7/008 , C22B7/02 , C22B13/045 , C22B17/04 , C22B19/24 , C22B19/26 , C22B19/28 , C22B19/30 , C22B19/34 , Y02P10/136 , Y02P10/216 , Y02P10/234 , Y10S75/961
摘要： A process for beneficiation of an electric arc furnace dust is disclosed. EAF dust (101) is briquetted with coal (60). The briquettes (64) are added to a furnace (12) along with a scrap metal charge (400). Zinc oxide fume (102) is driven off and collected for hydrometallurgical processing (100). Any iron containing insolubles (68) recovered from that process are added to the briquetting mix (60). A product solution (74) is processed (300) to recover zinc. Any iron insolubles (86) may be reintroduced into the briquetting process (60).
摘要翻译：公开了一种用于选矿的电弧炉灰尘的方法。 EAF粉尘（101）用煤（60）压块。煤渣（64）与废金属装料（400）一起加入到炉子（12）中。氧化锌烟（102）被驱除并收集用于湿法冶金加工（100）。将从该方法回收的任何含铁不溶物（68）加入到压块混合物（60）中。加工产品溶液（74）（300）以回收锌。任何铁不溶物（86）可以重新引入到压块过程（60）中。

3. 发明申请

WO2006071924A3 HYDRODYNAMIC CAVITATION CRYSTALLIZATION DEVICE AND PROCESS 审中-公开
标题翻译：水动力结晶结晶装置及工艺
公开(公告)号：WO2006071924A3
公开(公告)日：2006-11-30
申请号：PCT/US2005047204
申请日：2005-12-28
申请人： FIVE STAR TECHNOLOGIES INC , KOZYUK OLEG V , MYERSON ALLAN S , WEINBERG ROGER
发明人： KOZYUK OLEG V , MYERSON ALLAN S , WEINBERG ROGER
IPC分类号： C30B7/02 , C03B7/14 , C30B7/04 , C30B7/06 , C30B7/10 , C30B29/54
CPC分类号： C30B7/00 , C30B29/54
摘要： A device and process (10) for crystallizing a compound using hydrodynamic cavitation comprising the steps of mixing at least one stream of a feed solution of such compound to be crystallized with at least one stream of an anti-solvent in a nucleating section via collision of the feed solution and the anti-solvent (11), passing the mixed streams at an elevated pressure through at least one local constriction of flow to create hydrodynamic cavitation thereby causing nucleation and the production of seed crystals, passing the fluid stream containing the seed crystals through an intermediate section (12) to a crystal growth section, passing the fluid stream containing the seed crystals through the crystal growth (13) section at an elevated pressure through at least one local constriction of flow to create hydrodynamic cavitation thereby causing further crystallization of the compound contained in the solution.
摘要翻译：一种用于使用流体动力空化使化合物结晶的装置和方法（10），包括以下步骤：将待结晶的化合物的进料溶液的至少一种流与成核区中的至少一种抗溶剂流混合，进料溶液和反溶剂（11），使混合物流在升高的压力下通过至少一个局部的流动收缩，从而产生流体动力学空化，从而引起晶核的成核和产生，使包含晶种的流体流通过中间部分（12）到晶体生长部分，使包含晶种的流体流在升高的压力下通过晶体生长（13）部分通过至少一个局部的流动收缩，从而产生流体动力学空化，从而进一步结晶包含在溶液中的化合物。

4. 发明申请

WO2006124152A2 METHOD FOR USING A STATIC ELECTRIC FIELD TO INDUCE CRYSTALLIZATION AND TO CONTROL CRYSTAL FORM 审中-公开
标题翻译：使用静电场诱导结晶和控制晶体形式的方法
公开(公告)号：WO2006124152A2
公开(公告)日：2006-11-23
申请号：PCT/US2006/013324
申请日：2006-04-11
申请人： POLYTECHNIC UNIVERSITY , GARETZ, Bruce, A. , MYERSON, Allan, S. , ARNOLD, Stephen , ABER, Janice, E.
发明人： GARETZ, Bruce, A. , MYERSON, Allan, S. , ARNOLD, Stephen , ABER, Janice, E.
IPC分类号： C07K14/47
CPC分类号： C30B29/58 , B01D9/005 , C07K1/306 , C12N13/00 , C30B7/00 , C30B29/54 , C30B30/02
摘要： Applying a strong static DC electric field to supersaturated aqueous glycine solutions resulted in the nucleation of the Y polymorph attributed to the electric-field induced orientation of the highly polar glycine molecules in large preexisting solute clusters, helping them organize into a crystalline structure. A method to induce crystallization and to prepare polymorphs and/or morphologies of materials by using a static electric field to cause nucleation and crystal growth to occur in a supersaturated solution in such a way as to obtain a crystal structure that would not normally appear without the use of the static electric field. Aqueous glycine solutions were prepared by combining solid glycine and water. Supersaturated solutions were generated by heating the tubes to 62- 640C and holding them at that temperature in an ultrasonicator overnight. Once the glycine was completely dissolved, the solutions were slowly cooled to room temperature. A chamber was constructed consisting of two brass electrodes separated by a 5 mm insulating gap, with a hole drilled down through the center, parallel to the gap-electrode interface, with a diameter large enough to accommodate the test tube. A DC voltage was applied across the electrodes; large enough to produce electric fields in the range of 400,000 to 800,000 V/m. Tests tubes containing the aged solutions were placed in the high-voltage chamber. Exposure of the aged solutions to fields of 600,000 V/m resulted in crystallization typically within 30-90 min. The onset of nucleation was observed visually by the formation of a needle-shaped crystallite.
摘要翻译：将强静态DC电场应用于过饱和甘氨酸水溶液导致Y型多晶型物的成核归因于大型预先存在的溶质簇中高极性甘氨酸分子的电场诱导取向，有助于它们组织成晶体结构。通过使用静电场引起结晶并制备材料的多晶型物和/或形态的方法，以使得在过饱和溶液中发生成核和晶体生长，以获得通常不会出现的晶体结构使用静电场。通过结合固体甘氨酸和水制备甘氨酸水溶液。通过将管加热至62-64℃并将其在超声波隔离器中保持在该温度下而产生过饱和溶液。一旦甘氨酸完全溶解，将溶液缓慢冷却至室温。由两个黄铜电极构成的腔体由两个黄铜电极隔开，绝缘间隔为5mm，孔穿过中心平行于间隙 - 电极界面钻出，直径足够大以容纳试管。跨电极施加直流电压; 足够大以产生在400,000至800,000V / m范围内的电场。将含有老化溶液的试管置于高压室中。将老化溶液暴露于600,000V / m的场中，结晶通常在30-90分钟内。通过形成针状微晶目测观察成核的开始。

5. 发明申请

WO2011094423A1 METHODS TO TREAT MIXTURES OF GLYCOSIDES TO OBTAIN ONE OR MORE OF THESE GLYCOSIDES IN MORE PURE FORM 审中-公开
标题翻译：用于治疗糖尿病混合物的方法，以获得更多纯粹形式的这些糖蛋白的一种或多种
公开(公告)号：WO2011094423A1
公开(公告)日：2011-08-04
申请号：PCT/US2011/022741
申请日：2011-01-27
申请人： CARGILL, INCORPORATED , ERICKSON, Aron , HAHN, John Joseph , MYERSON, Allan S. , OHMES, Andrew Keith , RHONEMUS, Troy Allen , STORO, Kern M. , TYLER, Christopher Austin
发明人： ERICKSON, Aron , HAHN, John Joseph , MYERSON, Allan S. , OHMES, Andrew Keith , RHONEMUS, Troy Allen , STORO, Kern M. , TYLER, Christopher Austin
IPC分类号： A23L1/236
CPC分类号： C07H15/256 , A23L2/60 , A23L27/36 , A23V2002/00
摘要： The present invention provides methods to treat mixtures containing natural rebaudioside A (Reb A), rebaudioside B (Reb B), and rebaudioside D (Reb D), synthetic counterparts of these, and/or derivatives of the natural or synthetic embodiments obtain one or more of these glycosides in more pure form. In many embodiments, the invention can be used to process glycoside mixtures obtained at least in part from natural sources such as the Stevia plant. This allows, for instance, the recovery of a product including Reb A material in more pure form relative to Reb B material or Reb D material. As an alternative or in addition to recovery of the purified Reb A material, a product including Reb B material and/or Reb D material in more pure form relative to Reb A material can be obtained.
摘要翻译：本发明提供了治疗含有天然莱鲍迪甙A（Reb A），莱鲍迪甙B（Reb B）和莱鲍迪甙D（Reb D），其合成对应物和/或天然或合成实施方案的衍生物的混合物的方法，更多的这些糖苷更纯净的形式。在许多实施方案中，本发明可用于处理至少部分从天然来源（例如甜叶菊植物）获得的糖苷混合物。这允许例如相对于Reb B材料或Reb D材料回收包括Reb A材料的产品更纯净。作为纯化的Reb A材料的回收的替代或补充，可以获得包含相对于Reb A材料更纯的形式的Reb B材料和/或Reb D材料的产品。

6. 发明申请

WO2010118218A1 SWEETENER COMPOSITION COMPRISING HIGH SOLUBILITY FORM OF REBAUDIOSIDE A AND METHOD OF MAKING 审中-公开
标题翻译：包含重溶剂A的高溶解度形式的吸收剂组合物及其制备方法
公开(公告)号：WO2010118218A1
公开(公告)日：2010-10-14
申请号：PCT/US2010/030370
申请日：2010-04-08
申请人： CARGILL, INCORPORATED , FOSDICK, Lawrence, E. , HAHN, John, Joseph , JASINSKI, Yauching, W. , MYERSON, Allan, S. , RHONEMUS, Troy, Allen , TYLER, Christopher, Austin , ZHENG, Guo-Hua
发明人： FOSDICK, Lawrence, E. , HAHN, John, Joseph , JASINSKI, Yauching, W. , MYERSON, Allan, S. , RHONEMUS, Troy, Allen , TYLER, Christopher, Austin , ZHENG, Guo-Hua
IPC分类号： A23L1/236
CPC分类号： A23L27/36
摘要： Disclosed are sweetener compositions comprising rebaudioside A and methods of making the sweetener compositions. The sweetener compositions comprise a highly soluble crystal form of rebaudioside A that displays, in some embodiments, a solubility at 24°C in water of about 25 (grams rebaudioside A/per 100 grams water) or greater. The high solubility of the sweetener composition of the invention allows it to be used in applications such as syrups and concentrates.
摘要翻译：公开了包含莱鲍迪苷A的甜味剂组合物和制备甜味剂组合物的方法。甜味剂组合物包含高度可溶性的莱鲍迪甙A的晶体形式，在一些实施方案中，其在24℃下在约25（克莱鲍迪甙A /每100克水）或更高的水中的溶解度显示出来。本发明的甜味剂组合物的高溶解度允许其用于诸如糖浆和浓缩物的应用中。

7. 发明申请

WO2008151034A1 IMPROVED PROCESS FOR PURIFICATION OF ARYL CARBOXYLIC ACIDS 审中-公开
标题翻译：改进芳基羧酸的改进方法
公开(公告)号：WO2008151034A1
公开(公告)日：2008-12-11
申请号：PCT/US2008/065348
申请日：2008-05-30
申请人： THE UNIVERSITY OF ALABAMA , ROGERS, Robin, D. , MYERSON, Allan, S. , HINES, C., Corey
发明人： ROGERS, Robin, D. , MYERSON, Allan, S. , HINES, C., Corey
IPC分类号： C07C51/42
CPC分类号： C09K3/00 , C07C51/43 , Y02P20/542 , C07C63/26
摘要： Disclosed herein is a process for purifying aryl carboxylic acids, in particular terephthalic acid, wherein the impure acid is dissolved or dispersed in an ionic liquid and a non-solvent is added to precipitate the purified acid. The present disclosure further relates to compositions comprising terephthalic acid and one or more ionic liquids.
摘要翻译：本文公开了一种净化芳基羧酸，特别是对苯二甲酸的方法，其中不纯的酸溶解或分散在离子液体中，加入非溶剂以沉淀纯化的酸。本公开还涉及包含对苯二甲酸和一种或多种离子液体的组合物。

8. 发明申请

WO2001002075A1 METHOD FOR USING LASER LIGHT TO CONTROL CRYSTAL FORM 审中-公开
标题翻译：使用激光来控制晶体形状的方法
公开(公告)号：WO2001002075A1
公开(公告)日：2001-01-11
申请号：PCT/US2000/000294
申请日：2000-01-06
申请人： MYERSON, Allan, S. , GARETZ, Bruce, A.
发明人： MYERSON, Allan, S. , GARETZ, Bruce, A.
IPC分类号： B01D9/02
CPC分类号： C07B61/00 , B01D9/0036 , C07C227/38 , C07K1/306 , C07C229/08
摘要： A method to prepare new polymorphs of materials which have not been observed or to obtain a known polymorph under different conditions than those in which it is usually made by using a laser to cause nucleation and crystal growth to occur in a supersaturated solution in such a way as to obtain a crystal structure which would not normally appear without the use of the laser. For example, laser light can cause spontaneous nucleation of gamma-glycine crystals from a supersaturated aqueous solution.
摘要翻译：制备未观察到的材料的新多晶型物或在不同于通常通过使用激光引起核生成和晶体生长发生的条件下获得已知多晶型物的方法在过饱和溶液中以获得通常在不使用激光器时不会出现的晶体结构的方式。例如，激光可以引起过饱和水溶液中γ-甘氨酸晶体的自发成核。

9. 发明申请

WO2012082493A1 CRYSTALLINE FORMS OF REBAUDIOSIDE B 审中-公开
标题翻译：乙二胺四乙酸的结晶形式
公开(公告)号：WO2012082493A1
公开(公告)日：2012-06-21
申请号：PCT/US2011/063751
申请日：2011-12-07
申请人： CARGILL, INCORPORATED , FURLANO, Bruce , MYERSON, Allan S. , OHMES, Andrew Keith , RHONEMUS, Troy Allen , TYLER, Christopher Austin
发明人： FURLANO, Bruce , MYERSON, Allan S. , OHMES, Andrew Keith , RHONEMUS, Troy Allen , TYLER, Christopher Austin
IPC分类号： C07H15/24
CPC分类号： C07H15/24
摘要： A process for production of crystalline rebaudioside B from rebaudioside A is described. Additionally, four distinct crystal polymorphic forms of rebaudioside B are described, as well as methods for converting from one crystal polymorphic form of rebaudioside B to another crystal polymorphic form of rebaudioside B.
摘要翻译：描述了从莱鲍迪苷A生产结晶莱鲍迪甙B的方法。另外，还描述了四种不同的莱鲍迪甙B的晶体多晶型物质，以及从新蛇菊苷B的一种晶体多晶型转变为另一种莱鲍迪甙B晶体多晶型形式的方法。

10. 发明申请

WO2006052995A3 METHOD FOR PRODUCING CRYSTALS AND SCREENING CRYSTALLIZATION CONDITIONS 审中-公开
标题翻译：生产晶体和筛选结晶条件的方法
公开(公告)号：WO2006052995A3
公开(公告)日：2008-11-20
申请号：PCT/US2005040485
申请日：2005-11-08
申请人： ILLINOIS TECHNOLOGY INST , MYERSON ALLAN S , LEE ALFRED
发明人： MYERSON ALLAN S , LEE ALFRED
IPC分类号： C30B7/02 , C30B29/10
CPC分类号： B82Y30/00 , B01J19/0046 , B01J2219/00432 , B01J2219/00497 , B01J2219/00527 , B01J2219/00585 , B01J2219/00596 , B01J2219/00605 , B01J2219/00612 , B01J2219/00619 , B01J2219/00621 , B01J2219/00637 , B01J2219/00659 , B01J2219/00756 , C30B7/00
摘要： A method for producing crystals and for screening crystallization conditions of chemical materials on distinct metallic islands with specific functional groups, for preparing and screening the conditions necessary to promote a specific polymorph of a crystal, and a means for testing and screening the more precise conditions suitable for achieving a desired size or form of a crystal.
摘要翻译：一种用于生产晶体和用于筛选具有特定官能团的不同金属岛上的化学物质的结晶条件的方法，用于制备和筛选促进晶体的特定多晶型物所必需的条件，以及用于测试和筛选更精确条件的手段以实现期望的大小或形式的晶体。

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