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41. 发明申请

WO2006134081A1 VERFAHREN ZUR HERSTELLUNG VON POLYOXYMETHYLENDIALKYLETHERN AUS TRIOXAN UND DIALKYLETHER 审中-公开
标题翻译：用于生产聚甲醛二烷基醚和二烷基三烷OFF
公开(公告)号：WO2006134081A1
公开(公告)日：2006-12-21
申请号：PCT/EP2006/063074
申请日：2006-06-12
申请人： BASF AKTIENGESELLSCHAFT , STRÖFER, Eckhard , SCHELLING, Heiner , HASSE, Hans , BLAGOV, Sergej
发明人： STRÖFER, Eckhard , SCHELLING, Heiner , HASSE, Hans , BLAGOV, Sergej
IPC分类号： C07C41/50 , C07C43/30
CPC分类号： C07C41/50 , C07C41/58 , C07C43/303 , C07C43/30
摘要： Verfahren zur Herstellung von Polyoxymethylendialkylethern der Formel H 2m+1 C m O(CH 2 O) n C m H 2m+1 mit n = 2 - 10, m, gleich oder verschieden, = 1 oder 2 bei dem ein Dialkylether, ausgewählt aus Dimethylether, Methylethylether und Diethylether, und Trioxan in einen Reaktor eingespeist werden und in Gegenwart eines sauren Katalysators umgesetzt werden, wobei die durch den Dialkylether, Trioxan und/oder den Katalysator in das Reaktionsgemisch eingebrachte Wassermenge
摘要翻译：一种用于制备式H _{2M + 1 C _{米 O（CH _{2 O）_{名词的C聚甲醛二烷基醚的过程< 其中从二甲醚，甲基乙基醚和乙醚，和三恶烷中选择的二烷基醚SUB>米ħ_{2M + 1 ，其中n = 2-10，米，相同或不同，= 1或2 送入反应器中并在酸催化剂，其中所述的由二烷基醚，三恶烷和/或在反应混合物中水的量的催化剂引入的存在下反应<1重量％，基于反应混合物。}}}}}

42. 发明申请

WO0029365A3 PREPARATION OF POLYOXYMETHYLENE DIMETHYL ETHERS BY ACID-ACTIVATED CATALYTIC CONVERSION OF METHANOL WITH FORMALDEHYDE 审中-公开
标题翻译：通过甲酸与甲醛的酸活化催化转化制备聚羟基甲基二甲基
公开(公告)号：WO0029365A3
公开(公告)日：2000-10-05
申请号：PCT/US9920751
申请日：1999-09-09
申请人： BP AMOCO CORP
发明人： HAGEN GARY P , SPANGLER MICHAEL J
IPC分类号： C07C41/56 , C10L10/02 , C10L10/04 , C07C43/30 , C10L1/18
CPC分类号： C10L10/08 , C07C41/56 , C10L10/02 , Y02P20/127 , C07C43/30
摘要： A particularly useful process which includes the steps of providing a feedstream comprising methanol, a soluble condensation promoting component capable of activating a heterogeneous acidic catalyst and a source of formaldehyde; and heating this feedstream with the heterogeneous acidic catalyst in a catalytic distillation column to convert methanol and formaldehyde present to methylal and higher polyoxymethylene dimethyl ethers and to separate the methylal from the higher polyoxymethylene dimethyl ethers is disclosed. Advantageously, methylal and higher polyoxymethylene dimethyl ethers are formed and separated in a catalytic distillation column. By including within the column a section containing an anion exchange resin, an essentially acid-free product is obtained. Products can be used directly as a blending component, or fractionated, as by further distillation, to provide more suitable components for blending into diesel fuel.
摘要翻译：一种特别有用的方法，其包括提供包含甲醇的进料流，能够活化多相酸性催化剂和甲醛源的可溶性缩合促进组分的步骤; 并在催化蒸馏塔中用异质酸性催化剂加热该进料流，以将甲醇和甲醛转化成甲醛和更高级的聚甲醛二甲醚，并将甲缩醛与较高级的聚甲醛二甲醚分开。有利地，甲缩醛和更高级的聚甲醛二甲醚在催化蒸馏塔中形成并分离。通过在柱内包含含有阴离子交换树脂的部分，获得基本上无酸的产物。产品可以直接用作混合组分，或通过进一步蒸馏分级，以提供用于混合成柴油燃料的更合适的组分。

43. 发明申请

WO00029364A1 PREPARATION OF POLYOXYMETHYLENE DIMETHYL ETHERS BY REACTION OF DIMETHYLETHER WITH FORMALDEHYDE OVER HETEROGENEOUS CATALYSTS 审中-公开
标题翻译：通过二甲醚与异戊二烯在异构催化剂上的反应制备聚甲基乙烯二甲醚
公开(公告)号：WO00029364A1
公开(公告)日：2000-05-25
申请号：PCT/US1999/020439
申请日：1999-09-07
IPC分类号： C07C41/56 , C07C43/04 , C07C43/30 , C07C45/38 , C10L1/18
CPC分类号： C07C41/56 , Y02P20/127 , C07C43/30
摘要： A particularly useful process which includes the steps of providing a source of formaldehyde, preferably formed by conversion of methanol in the presence of a catalyst comprising silver as an essential catalyst component; and contacting the source of formaldehyde and a predominantely dimethyl ether feedstream with a heterogeneous, condensation promoting catalyst capable of hydrating dimethyl ether under conditions of reaction sufficient to form an effluent comprising water, methanol, formaldehyde, dimethyl ether, and polyoxymethylene dimethyl ethers is disclosed. Unreacted dimethyl ether is recovered from the effluent and recycled to the formation of polyoxymethylene dimethyl ethers. The resulting dimethyl ether-free liquid mixture is heated in the presence of an acidic catalyst to convert at least the methanol and formaldehyde present to polyoxymethylene dimethyl ethers. Advantageously, methylal and higher polyoxymethylene dimethyl ethers are formed and separated in a catalytic distillation column. By including in the column an anion exchange resin, an essentially acid-free product is obtained which can be used directly as a blending component, or fractionated, as by further distillation, to provide more suitable components for blending into diesel fuel.
摘要翻译：一种特别有用的方法，其包括提供甲醛源的步骤，优选通过在包含作为必需催化剂组分的银的催化剂存在下甲醇转化而形成; 并且公开了使甲醛源和主要为二甲醚的原料流与能够在足以形成包含水，甲醇，甲醛，二甲醚和聚甲醛二甲醚的流出物的反应条件下使二甲醚水合的异相缩合促进催化剂。从流出物中回收未反应的二甲醚，再循环至形成聚甲醛二甲醚。将所得的无二甲醚液体混合物在酸性催化剂存在下加热至少将甲醇和甲醛转化为聚甲醛二甲醚。有利地，甲缩醛和更高级的聚甲醛二甲醚在催化蒸馏塔中形成并分离。通过在柱中包含阴离子交换树脂，获得基本上不含酸的产物，其可以直接用作共混组分，或通过进一步蒸馏分离，以提供用于混合到柴油中的更合适的组分。

44. 发明申请

WO1988007989A1 PROCESS FOR THE PURIFICATION OF DIETHOXYMETHANE FROM A MIXTURE WITH ETHANOL AND WATER 审中-公开
标题翻译：用乙醇和水从混合物中纯化二乙氧基硅烷的方法
公开(公告)号：WO1988007989A1
公开(公告)日：1988-10-20
申请号：PCT/US1988001089
申请日：1988-04-07
申请人： EASTMAN KODAK COMPANY
发明人： EASTMAN KODAK COMPANY , MARTIN, Daniel, Lee , RAYNOLDS, Peter, Webb
IPC分类号： C07C43/30
CPC分类号： C07C41/58 , B01D3/36 , C07C43/30
摘要： A process for purifying diethoxymethane from a mixture containing ethanol and, optionally, water. The process involves the addition of an amount of water, DEM, or an appropriate mixture of any two or three of water, DEM and ethanol that is effective in moving the mixture into the two liquid phase region on an equilibrium tie-line which crosses the critical distillation boundary without the need for additional azeotrope-forming agents such as cyclohexane.

45. 发明申请

WO8704426A3 VINYL COMPOSITIONS 审中-公开
标题翻译： VINYL组合物
公开(公告)号：WO8704426A3
公开(公告)日：1987-10-22
申请号：PCT/EP8600754
申请日：1986-12-16
申请人： MERCK PATENT GMBH , WAECHTLER ANDREAS , KRAUSE JOACHIM , EIDENSCHINK RUDOLF , SCHEUBLE BERNHARD , HITTICH REINHARD
发明人： WAECHTLER ANDREAS , KRAUSE JOACHIM , EIDENSCHINK RUDOLF , SCHEUBLE BERNHARD , HITTICH REINHARD
IPC分类号： C07C43/14 , C07C1/00 , C07C13/28 , C07C15/18 , C07C15/40 , C07C15/50 , C07C41/00 , C07C43/115 , C07C43/164 , C07C43/18 , C07C43/188 , C07C43/20 , C07C43/21 , C07C43/215 , C07C43/225 , C07C43/30 , C07C45/00 , C07C49/00 , C07C67/00 , C07C69/75 , C07C69/92 , C07C241/00 , C07C253/00 , C07C255/49 , C07C255/50 , C07C255/53 , C07D239/26 , C07D239/34 , C07D319/06 , C09K19/06 , C09K19/08 , C09K19/18 , C09K19/20 , C09K19/30 , C09K19/34 , C09K19/46 , G02F1/13 , C07C121/75
CPC分类号： C07D239/26 , C07C43/115 , C07C43/188 , C07C43/21 , C07C43/215 , C07C255/00 , C07C2601/14 , C07D319/06 , C09K19/18 , C09K19/2007 , C09K19/3003 , C09K19/3028 , C09K19/3402 , C09K19/3469 , C09K2019/0444 , C09K2019/3422
摘要： Vinyl compositions having formula (I): R1-(A1-Z1)m-(A2-Z2)n-(A3)o-Q-CH=CH-R2, in which R1, R2, A1, A2 and A3, Z1 and Z2, m and o, n, Q and p have the definitions given in claim 1, are useful as components of liquid crystal phases.

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