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91. 发明申请

WO02054934A3 METHOD FOR STERILIZING CYANOACRYLATE COMPOSITIONS 审中-公开
标题翻译：灭菌氰化丙烯酸酯组合物的方法
公开(公告)号：WO02054934A3
公开(公告)日：2003-05-01
申请号：PCT/US0143270
申请日：2001-11-21
申请人： FLOWERS PARK LTD , ASKILL IAN N , KARNIK SHANE C , NORTON RICHARD L
发明人： ASKILL IAN N , KARNIK SHANE C , NORTON RICHARD L
IPC分类号： A61L2/08 , C07C253/32 , C07C253/34 , C07C255/23 , C08F2/46 , C08F2/48 , C08K3/28
CPC分类号： C07C253/34 , C07C255/23
摘要： Disclosed are methods for sterilizing cyanoacrylate prepolymer compositions under visible light irradiation conditions wherein the prepolymer remains in polymerizable form after sterilization.
摘要翻译：公开了在可见光照射条件下灭菌氰基丙烯酸酯预聚物组合物的方法，其中预聚物在灭菌后保持可聚合形式。

92. 发明申请

WO02006212A2 IMPROVED PROCESS FOR THE PURIFICATION AND RECOVERY OF ACETONITRILE 审中-公开
标题翻译：改进ACETONITRILE的纯化和回收方法
公开(公告)号：WO02006212A2
公开(公告)日：2002-01-24
申请号：PCT/US2001/019709
申请日：2001-06-21
IPC分类号： C07C253/24 , C07C253/26 , C07C253/34 , C07C255/03 , C07C253/00
CPC分类号： C07C253/26 , C07C253/24 , C07C253/34 , Y10S203/20 , C07C255/03
摘要： A method for the purification of crude acetonitrile comprising distilling the crude acetonitrile in a first fractional distillation column at below atmospheric pressure, withdrawing a first side draw fraction comprising acetonitrile, distilling the first side draw fraction in a second fractional distillation column at super atmospheric pressure, and withdrawing from the second distillation a second side draw fraction comprising purified acetonitrile.
摘要翻译：一种用于纯化粗乙腈的方法，包括在低于大气压的第一分馏塔中蒸馏粗乙腈，取出包含乙腈的第一侧馏分，在第二分馏塔中在超大气压下蒸馏第一侧馏分，并从第二次蒸馏中取出包含纯化乙腈的第二侧馏分。

93. 发明申请

WO01085673A1 PHENYL-SUBSTITUTED 2-ENAMINO-KETO NITRILES 审中-公开
标题翻译：苯基取代2-酮腈烯
公开(公告)号：WO01085673A1
公开(公告)日：2001-11-15
申请号：PCT/EP2001/004636
申请日：2001-04-25
IPC分类号： C07D249/08 , A01N37/18 , A01N37/34 , A01N41/12 , A01N43/16 , A01N43/40 , A01N43/653 , A01N43/84 , C07C231/02 , C07C233/65 , C07C237/16 , C07C237/20 , C07C253/30 , C07C253/34 , C07C255/42 , C07C255/43 , C07C255/46 , C07C325/02 , C07C327/48 , C07C327/58 , C07D211/56 , C07D211/58 , C07D213/38 , C07D213/53 , C07D265/36 , C07D309/08 , C07D309/14 , A01N37/44
CPC分类号： C07D211/56 , C07C237/20 , C07C255/42 , C07C255/43 , C07C255/46 , C07C325/02 , C07C2601/02 , C07C2601/08 , C07C2601/14 , C07D213/38 , C07D265/36 , C07D309/08
摘要： The invention relates to novel phenyl-substituted 2-enamino-keto nitriles of formula (I), wherein Ar, X, Z, Y and K have the meanings as cited in the description. The invention also relates to several methods for producing said phenyl-substituted 2-enamino-keto nitriles, and to their use as herbicides and pesticides.
摘要翻译：本发明涉及式（I），其中Ar，X，Z，Y和K具有说明书中给出的含义，的新颖苯基取代的2-烯氨基酮腈它们的制备方法和它们作为除草剂和杀虫剂使用几个进程。

94. 发明申请

WO01017950A1 TREATMENT OF NITRILES WITH GLYCOLIC ACID 审中-公开
标题翻译：用甘油酸处理硝酸盐
公开(公告)号：WO01017950A1
公开(公告)日：2001-03-15
申请号：PCT/US2000/005602
申请日：2000-03-02
IPC分类号： C07C253/34 , C07C255/08
CPC分类号： C07C253/34 , C07C255/08
摘要： A process for purifyiing a nitrile such as acrylonitrile is disclosed. The process comprises (1) contacting a product mixture, which comprises acrylonitrile and hydrogen cyanide, with glycolic acid or a glycolic acid-generating compound to produce a glycolic acid-treated product; and (2) recovering the nitrile from the glycolic acid-treated product. The product mixture can be produced by contacting ammonia with an olefin under a condition effective to produce a nitrile and hydrogen cyanide.
摘要翻译：公开了一种净化腈如丙烯腈的方法。该方法包括（1）使包含丙烯腈和氰化氢的产物混合物与乙醇酸或乙醇酸产生化合物接触以产生乙醇酸处理产物; 和（2）从乙醇酸处理的产物中回收腈。产物混合物可以通过在有效产生腈和氰化氢的条件下使氨与烯烃接触来制备。

95. 发明申请

WO01007382A2 IMPROVED METAL-LIGAND COMPLEX CATALYZED PROCESSES 审中-公开
标题翻译：改进的金属配体复合催化工艺
公开(公告)号：WO01007382A2
公开(公告)日：2001-02-01
申请号：PCT/US2000/020251
申请日：2000-07-26
IPC分类号： B01J31/40 , B01J38/00 , C07B61/00 , C07B63/00 , C07C29/141 , C07C45/49 , C07C45/50 , C07C45/78 , C07C45/80 , C07C45/82 , C07C47/32 , C07C47/347 , C07C47/36 , C07C209/26 , C07C209/48 , C07C209/84 , C07C211/18 , C07C253/30 , C07C253/34 , C07C255/46 , C07C255/47 , C07B37/12 , C07F9/02 , C08G63/00 , C09D4/00
CPC分类号： C07B63/00 , B33Y40/00 , B33Y70/00 , C07B2200/09 , C07C29/141 , C07C45/49 , C07C45/50 , C07C45/78 , C07C45/80 , C07C47/32 , C07C209/26 , C07C253/30 , C07C2601/14 , Y02P20/582 , C07C47/347 , C07C47/36 , C07C31/276
摘要： This invention relates to a process for separating one or more cyclic products from a reaction product fluid comprising one or more cyclic reactants, a metal-organophosphorus ligand complex catalyst, optionally free organophosphorus ligand, a non-polar solvent and said one or more cyclic products, wherein said process comprises: (1) reacting said one or more cyclic reactants in the presence of said metal-organophosphorus ligand complex catalyst, optionally free organophosphorus ligand and non-polar solvent to form a multiphase reaction product fluid; and (2) separating said multiphase reaction product fluid to obtain a non-polar phase comprising said one or more cyclic reactants, metal-organophosphorus ligand complex catalyst, optionally free organophosphorus ligand and non-polar solvent and a polar phase comprising said one or more cyclic products.
摘要翻译：本发明涉及从反应产物流体中分离一种或多种环状产物的方法，该方法包括一种或多种环状反应物，金属 - 有机磷配位体配位催化剂，任选的游离有机磷配体，非极性溶剂和所述一种或多种环状产物其中所述方法包括：（1）在所述金属 - 有机磷配体配合物催化剂，任选的游离有机磷配体和非极性溶剂的存在下使所述一种或多种环状反应物反应以形成多相反应产物流体; 和（2）分离所述多相反应产物流体以获得包含所述一种或多种环状反应物，金属 - 有机磷配体络合物催化剂，任选的游离有机磷配体和非极性溶剂的非极性相和包含所述一种或多种循环产品。

96. 发明申请

WO00059871A1 IMPROVED ACRYLONITRILE RECOVERY PROCESS 审中-公开
标题翻译：改进的丙烯腈回收方法
公开(公告)号：WO00059871A1
公开(公告)日：2000-10-12
申请号：PCT/US2000/006732
申请日：2000-03-15
IPC分类号： C07C253/34 , C07C255/08
CPC分类号： C07C253/34 , C07C255/08
摘要： The process of the present invention comprises transporting a reactor effluent containing acrylonitrile/methacrylonitrile to a first column (quench) where the reactor effluent is cooled with a first aqueous stream, transporting the cooled effluent into an indirect contact cooler to condensed at least some of the cooled effluent to form a condensate comprising water and acrylonitrile/methacrylonitrile, transporting the remaining cooled gaseous effluent containing acrylonitrile/methacrylonitrile into a second column (absorber) where the cooled effluent is contacted with a second aqueous stream to absorb substantially all of the remaining acrylonitrile/methacrylonitrile into the second aqueous stream, transporting the second aqueous stream containing the acrylonitrile/methacrylonitrile to a first distillation column (recovery column) for separation of the crude acrylonitrile/methacrylonitrile from the second aqueous stream, and transporting the separated crude acrylonitrile/methacrylonitrile to a second distillation column (heads column) to remove at least some impurities from the crude acrylonitrile/methacrylonitrile, and transporting the partially purified acrylonitrile/methacrylonitrile, to a third distillation column (product column) to further purify the acrylonitrile/methacrylonitrile, and recovering the purified acrylonitrile/methacrylonitrile, wherein the improvement comprises transporting the condensate formed in the indirect contact cooler to a decanter where the condensate is separated into an organic phase comprising acrylonitrile/methacrylonitrile, an aqueous phase and a vapor phase, and the organic phase is introduced into the recovery column without passing through the absorber column.
摘要翻译：本发明的方法包括将含有丙烯腈/甲基丙烯腈的反应器流出物输送到第一塔（骤冷），其中反应器流出物用第一含水流冷却，将冷却的流出物输送到间接接触冷却器中以冷凝至少一些将含有丙烯腈/甲基丙烯腈的剩余的冷却的气态流出物输送到第二塔（吸收器）中，其中冷却的流出物与第二含水流接触以吸收基本上所有剩余的丙烯腈/ 甲基丙烯腈转移到第二含水流中，将含有丙烯腈/甲基丙烯腈的第二含水流输送到第一蒸馏塔（回收塔），以从第二含水流中分离粗丙烯腈/甲基丙烯腈，并将分离的粗丙烯腈/甲基丙烯腈向第二蒸馏塔（头柱）除去粗丙烯腈/甲基丙烯腈中的至少一些杂质，并将部分纯化的丙烯腈/甲基丙烯腈输送到第三蒸馏塔（产物柱）以进一步纯化丙烯腈/甲基丙烯腈，以及回收纯化的丙烯腈/甲基丙烯腈，其中改进包括将在间接接触冷却器中形成的冷凝物输送到滗析器，其中冷凝物被分离成包含丙烯腈/甲基丙烯腈，水相和气相的有机相，有机相为引入回收塔而不通过吸收塔。

97. 发明申请

WO00024706A1 AZO-TYPE COMPOUND GRANULES 审中-公开
标题翻译： AZO型复合颗粒
公开(公告)号：WO00024706A1
公开(公告)日：2000-05-04
申请号：PCT/FR1999/002249
申请日：1999-09-22
IPC分类号： B01J2/20 , C07C253/34 , C07C255/65 , C08F4/04
CPC分类号： C07C255/65 , C07C2601/02 , C07C2601/14
摘要： The invention concerns a composition comprising an azo compound in the form of granules with size ranging between 200 mu m and 10 mm whereof the cumulative volume of pores ranges between 0.2 and 2 ml/g. The invention also concerns the method for preparing said composition which consists in: wetting a powder comprising said azo compound; granulating it by passing it under mechanical stress through a die; and drying the resulting granules at a temperature less than 45 DEG C.
摘要翻译：本发明涉及一种组合物，其包含粒径为200μm至10mm的颗粒形式的偶氮化合物，其中孔的累积体积为0.2-2ml / g。本发明还涉及制备所述组合物的方法，该方法包括：润湿包含所述偶氮化合物的粉末; 通过在机械应力下通过模具将其造粒; 并在低于45℃的温度下干燥得到的颗粒。

98. 发明申请

WO00018728A1 METHOD OF QUENCHING GASEOUS ACRYLONITRILE AND HYDROGEN CYANIDE PRODUCT STREAM 审中-公开
标题翻译：气相丙烯腈和氢化氰化物产品流程的方法
公开(公告)号：WO00018728A1
公开(公告)日：2000-04-06
申请号：PCT/US1999/022484
申请日：1999-09-28
IPC分类号： B01J10/00 , C07C253/24 , C07C253/34 , C07C255/08
CPC分类号： C07C253/26 , C07C253/34 , C07C255/08
摘要： The present invention provides an improvement in a process and apparatus for manufacturing acrylonitrile by the vapor phase ammoxidation of a hydrocarbon. The invention comprises contacting the gaseous product stream with a quench fluid in a reverse jet scrubber. The quenching fluid is injected counter-current to the gas flow, and the gas velocity is sufficient to reverse the flow direction of the water, thereby forming a standing wave or froth zone wherein the quench is rapidly achieved. The quench fluid may be obtained from many sources, but is preferably obtained from a waste process stream emanating from a subsequent recovery or purification step. The quench fluid may contain acid to facilitate removal of ammonia from the gas stream. The quench fluid that is not vaporized may be recirculated. Impurities and contaminants may be removed from the quench fluid prior to recycle. In a most preferred embodiment, the quench fluid is not cooled during recirculation, and the cooling process is essentially adiabatic, with the sensible heat of the hot gaseous stream being converted to latent heat in the form of vapor.
摘要翻译：本发明提供了通过烃的气相氨氧化制备丙烯腈的方法和装置的改进。本发明包括使气态产物流与反向喷射洗涤器中的骤冷流体接触。淬火流体与气流逆流注入，气体流速足以反转水的流动方向，从而形成驻波或泡沫区，其中快速实现骤冷。骤冷流体可以从许多来源获得，但优选地从随后的回收或纯化步骤发出的废物流中获得。骤冷流体可含有酸，以便于从气流中除去氨。未蒸发的骤冷液体可以再循环。杂质和污染物可以在循环之前从骤冷流体中除去。在最优选的实施方案中，骤冷流体在再循环过程中不被冷却，并且冷却过程基本上是绝热的，热气流的显热转化为蒸气形式的潜热。

99. 发明申请

WO99048872A3 METHOD FOR SEPARATING AN AZEPINE DERIVATIVE FROM A MIXTURE CONTAINING AN AMINE AND AN AZEPINE DERIVATIVE 审中-公开
标题翻译：处理对混合物的氮杂衍生物基胺的分离和一个氮杂衍生物
公开(公告)号：WO99048872A3
公开(公告)日：1999-12-02
申请号：PCT/EP1999/001786
申请日：1999-03-18
IPC分类号： C07D223/04 , B01D3/00 , C07C209/48 , C07C209/84 , C07C209/86 , C07C211/12 , C07C253/34 , C07C255/24 , C07D223/12 , B01D3/14
CPC分类号： C07D223/12 , C07C209/48 , C07C209/86 , C07C253/34 , C07C211/12 , C07C255/24
摘要： The invention relates to a method for separating by distillation all or part of an azepine derivative (III) selected from the group consisting of amino hexylidenimine, tetrahydroazepine, hexylhexahydroazepine and amino hexylhexahydroazepine, from a mixture (II) containing an azepine derivative (III) and an amine (I). The invention is characterized in that the distillation is carried out at an overhead temperature of between 160 and 250 DEG C.
摘要翻译：一种用于部分蒸馏分离或全部氮杂衍生物的方法（III）是从由aminohexylideneimine，tetrahydroazepine，Hexylhexahydroazepin和Aminohexylhexahydroazepin组成的组中从（II）含有（III）的氮杂衍生物和胺（I）的混合物中，其特征在于蒸馏在160-250℃的顶部温度下进行

100. 发明申请

WO9948872A2 METHOD FOR SEPARATING AN AZEPINE DERIVATIVE FROM A MIXTURE CONTAINING AN AMINE AND AN AZEPINE DERIVATIVE 审中-公开
标题翻译：处理对混合物的氮杂衍生物基胺的分离和一个氮杂衍生物
公开(公告)号：WO9948872A2
公开(公告)日：1999-09-30
申请号：PCT/EP9901786
申请日：1999-03-18
申请人： BASF AG , REHFINGER ALWIN , LUYKEN HERMANN
发明人： REHFINGER ALWIN , LUYKEN HERMANN
IPC分类号： C07D223/04 , B01D3/00 , C07C209/48 , C07C209/84 , C07C209/86 , C07C211/12 , C07C253/34 , C07C255/24 , C07D223/12
CPC分类号： C07D223/12 , C07C209/48 , C07C209/86 , C07C253/34 , C07C211/12 , C07C255/24
摘要： The invention relates to a method for separating by distillation all or part of an azepine derivative (III) selected from the group consisting of amino hexylidenimine, tetrahydroazepine, hexylhexahydroazepine and amino hexylhexahydroazepine, from a mixture (II) containing an azepine derivative (III) and an amine (I). The invention is characterized in that the distillation is carried out at an overhead temperature of between 160 and 250 DEG C.
摘要翻译：一种用于部分蒸馏分离或全部氮杂衍生物的方法（III）是从由aminohexylideneimine，tetrahydroazepine，Hexylhexahydroazepin和Aminohexylhexahydroazepin组成的组中从（II）含有（III）的氮杂衍生物和胺（I）的混合物中，其特征在于：一个执行头温度为160〜250℃蒸馏

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