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1. 发明申请

US20220259435A1 Fibre Reactive Dyes, Their Preparation and Their Use 有权
公开(公告)号：US20220259435A1
公开(公告)日：2022-08-18
申请号：US17629810
申请日：2020-06-24
申请人： Huntsman Advanced Materials (Switzerland) GMBH
发明人： Hubert Jean Luc CHRISTNACHER , Fanny EHRET , Michael NICOLLET , Jean-Christophe GRACIET , Georg ROENTGEN
IPC分类号： C09B62/255 , C09B67/22 , D06P3/66 , C09D11/328
摘要： A reactive dye of formula wherein M is hydrogen, an alkali metal or one equivalent of an alkaline earth metal, Z1 is vinyl, β-sulfatoethyl or the radical —NHCO—(CH2)3—SO2—CH2CH2Cl; R1 denotes H or sulfo; and R2 is H, methyl, methoxy or sulfo, n is the number 3; Y is vinyl or a radical —CH2—CH2-U and U is —Cl or —OSO3H, is suitable for dyeing and printing cellulosic or amide-group-containing fibre materials.

2. 发明授权

US5001227A Fibre-reactive 1:1 chromium complex azo or azomethine dyes having a bidentate chelating group and a monofunctional neutral ligand 失效
公开(公告)号：US5001227A
公开(公告)日：1991-03-19
申请号：US669942
申请日：1984-11-09
申请人： Hans U. Schutz , Ulrich Schlesinger , Gerhard Back
发明人： Hans U. Schutz , Ulrich Schlesinger , Gerhard Back
IPC分类号： C09B62/012 , C09B62/095 , C09B62/255 , C09B62/477
CPC分类号： C09B62/477 , C09B62/095
摘要： The invention relates to chromium complexes of the formula ##STR1## in which L is H.sub.2 O, NH.sub.3, R.sub.2 --OH, R.sub.2 --NH.sub.2, (R.sub.2).sub.2 NH, (R.sub.2).sub.3 N or pyridine, wherein R.sub.2 is C.sub.1-6 -alkyl unsubstituted or substituted by halogen, C.sub.1-4 -alkoxy or amino, B is 8-hydroxyquinoline, 5-chloro-8-hydroxyquinoline, 5-hydroxyacridine, 6-hydroxy-4,7-phenanthroline, pyridine-2-carboxylic acid, 8-carboxyquinoline, 5,7-dibromo-8-hydroxyquinoline, o-hydroxyaniline, o-hydroxynaphthylamine, proline, glycine, serine, aspartic acid or R.sub.1 --CH(NH.sub.2)--COOH, wherein R.sub.1 is C.sub.1-6 -alkyl unsubstituted or substituted by halogen, C.sub.1-4 -alkoxy or amino, D is benzene or naphthalene, Y is the nitrogen atom or the CH group, K, in the event that Y is the nitrogen atom, is naphthol, naphthylamine, 5-pyrazolone, 5-aminopyrazole, 1-phenyl- or 1-naphthyl-5-aminopyrazole, 1-phenyl- or 1-naphthyl-5-pyrazolone, 2,6-dihydroxy-3-cyano- or -3-carboxamido-4-alkylpyridine, 6-hydroxypyrid-2-one, acetoacetanilide, benzoylacetanilide or phenol, or, in the event that Y is the CH group K is o-hydroxybenzaldehyde or o-hydroxynaphthaldehyde, D and K independently of each other are unsubstituted or substituted by C.sub.1-5 -alkyl, C.sub.1-4 -alkoxy, acylamino having 1 to 6 carbon atoms, benzoylamino, amino, monoalkylamino or dialkylamino each having 1 to 4 carbon atoms, phenylamino, alkoxycarbonyl having 1 to 4 carbon atoms in the alkoxy, radical, nitro, cyano, trifluoromethyl, halogen, sulfamoyl, carbamoyl, ureido, hydroxyl, C.sub.1-4 -alkylsulfonyl, carboxyl, sulfomethyl, phenylazo or naphthylazo, and D and K contain the --(CO).sub.0-1 --O-- and --[O or N(R)]-- adjacent to the --N.dbd.Y-- and R is hydrogen, C.sub.1-4 -alkyl or phenyl, Ka is a cation, X is acryloyl, monohalogenoacryloyl, dihalogenoacryloyl, trihalogenoacryloyl, monohalogenomethacryloyl, dihalogenomethacryloyl, trihalogenomethacryloyl, monohalogenopropionyl, dihalogenopropionyl, phenylsulfonylpropionyl, methylsulfonylpropionyl, vinylsulfonyl, .beta.-chloroethylsulfonyl, .beta.-sulfatoethylsulfonyl, monohalogenopyrimidyl, dihalogenopyrimidyl, trihalogenopyrimidyl, monohalogenotriazinyl, dihalogenotriazinyl, X is bonded to D, K or B, D and K, D and B or K and B directly or via ##STR2## or --CH.sub.2 --N(R)--, m is 1, 2 or 3 and n is 1 or 2. These chromium complexes are suitable for dyeing nitrogen-containing or hydroxy-containing materials and they produce level dyeings having good all-round fastness properties.

3. 发明授权

US4544739A Fibre-reactive chromium complex Azo-azomethine dyes 失效
标题翻译：纤维反应铬复合偶氮偶氮甲染料
公开(公告)号：US4544739A
公开(公告)日：1985-10-01
申请号：US425595
申请日：1982-09-28
申请人： Hans U. Schutz , Arthur Buhler
发明人： Hans U. Schutz , Arthur Buhler
IPC分类号： C09B62/006 , C09B62/012 , C09B62/095 , C09B62/255 , C09B62/477
CPC分类号： C09B62/012 , C09B62/0068
摘要： Chromium complex dyes which, in the form of the free acid, have the formula ##STR1## wherein Z is hydrogen, nitro, chlorine or naphthylazo or phenylazo, wherein naphthyl or phenyl is unsubstituted or substituted by nitro, chlorine, bromine, C.sub.1-5 -alkyl or C.sub.1-5 -alkoxy, A is naphthyl or phenyl containing the oxygen atom in o-position to the azomethine and wherein naphthyl or phenyl is unsubstituted or substituted by C.sub.1-5 -alkyl, halogen or naphthylazo or phenylazo wherein naphthyl or phenyl is unsubstituted or substituted by nitro, chlorine, bromine, C.sub.1-5 -alkyl or C.sub.1-5 -alkoxy, D is sulfophenyl which is unsubstituted or substituted by nitro or chlorine, or sulfonaphthyl which is unsubstituted or substituted by nitro, and is bonded to the azo group in the ortho-position to the oxygen atom and R is chloroacetyl, bromoacetyl, .alpha.-chloroacryloyl, .alpha.-bromoacryloyl, .alpha.,.beta.-dichloropropionyl, .alpha.,.beta.-dibromopropionyl, 5-chloro-2,4-difluoropyrimidyl or 2-chloro- or 2-fluorotriazin-6-yl substituted in 4-position by substituted or unsubstituted amino, free or etherified hydroxy or mercapto. These dyes are obtained by chroming the corresponding o,o'-dihydrokyazo compounds and o,o'-dihydroxyazomethine compounds, the reactive radical R being introduced by acylation before or after the chroming. They are suitable for dyeing natural or synthetic polyamide material.
摘要翻译：游离酸形式的铬配合物染料具有下式：其中Z为氢，硝基，氯或萘基偶氮或苯偶氮，其中萘基或苯基未被取代或被硝基，氯，溴，C1-5 - 烷基或C 1-5 - 烷氧基，A是在甲氧基甲基的邻位含有氧原子的萘基或苯基，其中萘基或苯基未被取代或被C 1-5 - 烷基，卤素或萘基偶氮或苯偶氮取代，其中萘基或苯基未取代或被硝基，氯，溴，C 1-5 - 烷基或C 1-5 - 烷氧基取代，D是未被取代或被硝基或氯取代的磺基苯基，或未被取代或被硝基取代的磺基萘，与氧原子邻位的偶氮基，R是氯乙酰基，溴乙酰基，α-氯丙烯酰基，α-溴丙烯酰，α，β-二氯丙酰基，α，β-二溴丙酰基，5-氯-2,4-二氟嘧啶基或2 - 氯 - 或2-氟三氮杂被取代或未取代的氨基，游离的或醚化的羟基或巯基取代在4-位上的6-6位。这些染料是通过对相应的o，o'-二羟基偶氮化合物和o'-二羟基偶氮甲基化合物进行镀色得到的，反应性基团R是通过在镀铬之前或之后的酰化引入的。它们适用于染色天然或合成聚酰胺材料。

4. 发明授权

US3198782A Metallised azo halopyrimidine dyestuffs 失效
标题翻译：金属偶氮卤嘧啶染料
公开(公告)号：US3198782A
公开(公告)日：1965-08-03
申请号：US11853761
申请日：1961-06-21
申请人： ICI LTD
发明人： FRANCIS ANDREW HERBERT , DONALD BUCKLEY
IPC分类号： C09B62/255 , H01R13/646
CPC分类号： C09B62/255

5. 发明授权

US06060591A Water-soluble fiber-reactive dyes, processes for their preparation, and their use 失效
标题翻译：水溶性纤维反应性染料，其制备方法及其用途
公开(公告)号：US06060591A
公开(公告)日：2000-05-09
申请号：US987939
申请日：1997-12-01
申请人： Wilfried Hansmann , Hermann Henk , Stefan Ehrenberg , Wolfram Reddig
发明人： Wilfried Hansmann , Hermann Henk , Stefan Ehrenberg , Wolfram Reddig
IPC分类号： C07D239/42 , C09B62/02 , C09B62/032 , C09B62/20 , C09B62/255 , C09B62/44 , D06P1/382
CPC分类号： C09B62/032 , C09B62/02 , C09B62/20 , C09B62/205 , C09B62/255 , C09B62/4422
摘要： The disclosed dyes (which are fiber-reactive and are useful for dyeing materials containing OH and/or carboxamide groups) are compounds of the formula (1)Fb--Z.sub.n (1)in which:Fb is the radical of various classes of dyestuffs, including the formazans, azomethines, phthalocyanines, etc., and particularly sulfo group-containing monoazo or disazo dyes of the formulas (a-1) through (a-5):D.sup.1 --N.dbd.N--K.sup.2 -- (a-1)--D.sup.2 --N.dbd.N--(E--N.dbd.N).sub.v --K.sup.1 (a-2)--D.sup.2 --N.dbd.N--(E--N.dbd.N).sub.v --K.sup.2 -- (a-3)D.sup.1 --N.dbd.N--K.sup.0 --N.dbd.N--D.sup.2 -- (a-4)--D.sup.1 --N.dbd.N--K.sup.0 --N.dbd.N--D.sup.2 -- (a-5)in which in which D.sup.1 is a substituted or unsubstituted phenyl or naphthyl radical, D.sup.2 is the radical of a diazo component and K.sup.1, K.sup.2, and K.sup.0 are various coupling components, and E is a middle component.
摘要翻译：所公开的染料（其是纤维反应性的并且可用于含有OH和/或羧酰胺基团的染色材料）是式（1）Fb-Zn（1）的化合物，其中：Fb是各种类型的染料的基团，包括式（a-1）至（a-5）中的甲ans，偶氮甲碱，酞菁等，特别是含磺基的单偶氮或双偶氮染料：D1-N = N-K2-（a-1） - D2-N = N-（EN = N）v-K1（a-2）-D2-N = N-（EN = N）v-K2-（a-3）D1-N = N-K0-N = N-D2-（a-4）-D1-N = N-K0-N = N-D2-（a-5）其中D1是取代或未取代的苯基或萘基，D2是重氮组分和K1，K2和K0是各种偶合组分，E是中间组分。

6. 发明授权

US4813972A Fiber-reactive chromium complexes and their preparation and use for polyamide, leather and cotton 失效
标题翻译：纤维反应性铬配合物及其制备和用于聚酰胺，皮革和棉花
公开(公告)号：US4813972A
公开(公告)日：1989-03-21
申请号：US105344
申请日：1987-10-07
申请人： Hans U. Schutz , Ulrich Schlesinger , Gerhard Back
发明人： Hans U. Schutz , Ulrich Schlesinger , Gerhard Back
IPC分类号： C09B62/44 , C09B62/002 , C09B62/012 , C09B62/04 , C09B62/095 , C09B62/20 , C09B62/255 , C09B62/465 , C09B62/477 , C09B62/503 , C09B62/515 , D06P1/382 , D06P1/384 , C09B62/01 , D06P1/38 , D06P3/10
CPC分类号： C09B62/477 , C09B62/012 , Y10S8/917 , Y10S8/918 , Y10S8/924
摘要： The invention relates to chromium complexes of the formula ##STR1## in which A is the radical of a dicyclically metallizable azo or azomethine dye, B is the radical of a potentially at least bidentate bianionic complexible organic compound which contains no azo or azomethine group, L is a colorless monofunctional ligand, X is a fibre-reactive radical, Ka is a cation, K is 0 or 1, m is 1, 2 or 3, n is 1 or 2, and the X radical and the SO.sub.3.sup..crclbar. Ka group are each bonded to the radicals A and B, to a process for preparing the chromium complexes of the formula (1), and to a combined preparation and dyeing process.
摘要翻译：本发明涉及式（1）的铬配合物，其中A是双环可金属化的偶氮或偶氮甲碱染料的基团，B是不含偶氮或偶氮甲碱的潜在至少二齿双键络合的有机化合物的基团基团，L是无色单官能配体，X是纤维反应性基团，Ka是阳离子，K是0或1，m是1,2或3，n是1或2，X基团和SO 3（ - ）Ka基团各自键合到基团A和B，与制备式（1）的铬络合物的方法以及组合的制备和染色方法。

7. 发明授权

US3502642A Reactive copper-containing benzeneazonaphthalene dyes containing a trichloropyrimidine group 失效
标题翻译：含有三氯苯胺组合物的含有苯并苯并噻吩的反应性
公开(公告)号：US3502642A
公开(公告)日：1970-03-24
申请号：US3502642D
申请日：1967-07-24
申请人： GEIGY AG J R
发明人： DUSSY PAUL
IPC分类号： C09B62/255 , C09B62/24 , D06P3/04 , D06P3/60
CPC分类号： C09B62/255

8. 发明授权

US3362949A Reactive copper complex monoazo dyes containing pyrazolone and polyhalo-pyrimidylamino groups 失效
标题翻译：含有吡唑啉酮和多卤代嘧啶氨基的活性铜络合物单偶氮染料
公开(公告)号：US3362949A
公开(公告)日：1968-01-09
申请号：US41832964
申请日：1964-12-14
申请人： SANDOZ LTD
发明人： JAKOB BENZ , KURT BRENNEISEN
IPC分类号： C09B62/24 , C09B62/255
CPC分类号： C09B62/255 , C09B62/24

9. 发明授权

US07105645B2 Water-soluble fiber-reactive dyes, method for the production and use thereof 有权
标题翻译：水溶性纤维反应性染料，其制造方法和使用方法
公开(公告)号：US07105645B2
公开(公告)日：2006-09-12
申请号：US10512380
申请日：2003-04-22
申请人： Günther Schwaiger , Stefan Meier , Werner Russ
发明人： Günther Schwaiger , Stefan Meier , Werner Russ
IPC分类号： C09B62/515 , C09B62/255 , C09B62/415 , D06P1/384
CPC分类号： C09B62/4416 , C09B62/515
摘要： Dyes of general formula (I) wherein R1, R2, M, Y and x have the meaning cited in the description, the production and use thereof for dyeing or printing material containing hydroxy and/or carbonamide groups, preferably fiber material.
摘要翻译：通式（I）的染料，其中R 1，R 2，M，Y和x具有说明书中引用的含义，其用于染色或印刷的生产和使用含有羟基和/或碳酰胺基团的材料，优选纤维材料。

10. 发明授权

US5386015A Monoazo and disazo compounds having 5-cyano-2,4-and 4,6-dichloropyrimidyl groups 失效
标题翻译：具有5-氰基-2,4-和4,6-二氯嘧啶基的单偶氮和双偶氮化合物
公开(公告)号：US5386015A
公开(公告)日：1995-01-31
申请号：US90227
申请日：1993-07-09
申请人： Paul Doswald , Werner Koch
发明人： Paul Doswald , Werner Koch
IPC分类号： C09B62/245 , C09B62/24 , C09B62/25 , C09B62/255 , D06P1/382
CPC分类号： C09B62/24 , Y10S534/01
摘要： Compounds of the formula ##STR1## and salts thereof, and mixtures of such compounds and salts, wherein F.sub.c is ##STR2## wherein D.sub.1 is an unsubstituted or substituted phenyl or naphthyl diazo component radical,each of Q.sub.1, Q.sub.2 and Q.sub.3 is independently hydrogen or a substituent,each R.sub.5 is independently hydrogen, C.sub.1-4 alkyl or C.sub.1-4 alkoxy,each R.sub.6 is independently hydrogen, halo, C.sub.1-4 alkyl, C.sub.1-4 alkoxy, (C.sub.1-4 alkyl)carbonylamino or --NH--CO--NH.sub.2,R.sub.16 is hydrogen or --SO.sub.3 H,r is 1 or 2, andt is 2 or 3, andb is 1 or 2,whereineach R.sub.1 is independently hydrogen or C.sub.1-4 alkyl,each R.sub.7 is independently hydroxy, C.sub.1-4 alkoxy or --NH.sub.2,each Z is independently ##STR3## and each m is independently 0 or 1.
摘要翻译：下式化合物及其盐，以及这些化合物和盐的混合物，其中Fc是未取代或取代的苯基或萘基重氮组分基团，Q1，Q2和Q3各自独立地为氢或取代基，每个R 5独立地为氢，C 1-4烷基或C 1-4烷氧基，每个R 6独立地为氢，卤素，C 1-4烷基，C 1-4烷氧基， -4-烷基）羰基氨基或-NH-CO-NH 2，R 16是氢或-SO 3 H，r是1或2，t是2或3，b是1或2，其中每个R 1独立地是氢或C 1-4烷基，每个R 7独立地是羟基，C 1-4烷氧基或-NH 2，每个Z独立地是＆lt; IMAGE＆gt;每个m独立地是0或1。

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