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1. 发明授权

US09062160B1 Catalyst-free methods of forming polyurethanes from pentafluorophenyl carbonates 有权
标题翻译：从五氟苯基碳酸酯形成聚氨酯的无催化剂方法
公开(公告)号：US09062160B1
公开(公告)日：2015-06-23
申请号：US14162222
申请日：2014-01-23
申请人： International Business Machines Corporation , Agency For Science, Technology and Research , Universidad del Pais Vasco/Euskal Herriko Unibertsitatea
发明人： Julian M. W. Chan , Daniel J. Coady , Amanda C. Engler , Jeannette M. Garcia , James L. Hedrick , Zhan Yuin Ong , Haritz Sardon , Yi Yan Yang
IPC分类号： C08G73/24 , C08G71/04 , C08G65/00 , C08G73/02
CPC分类号： C08G71/04 , C08G65/007 , C08G73/02 , C08G73/0206
摘要： One catalyst-free method of forming a polyurethane comprises forming a first emulsion comprising a first monomer, a surfactant, a water immiscible organic solvent, and water. The first monomer comprises two or more pentafluorophenyl carbonate groups. The first emulsion is combined with an aqueous mixture containing a second monomer comprising two or more nucleophilic amine groups, thereby forming a second emulsion. The first and second monomers of the second emulsion are allowed to react by interfacial polymerization, thereby forming a polyurethane. The polyurethane can have a number average molecular weight (Mn) of about 30000 to about 80000. The method is compatible with introducing pendant functionality into the polyurethane by way of cyclic carbonate precursors to the first monomer.
摘要翻译：形成聚氨酯的一种无催化剂的方法包括形成包含第一单体，表面活性剂，与水不混溶的有机溶剂和水的第一乳液。第一单体包含两个或多个五氟苯基碳酸酯基团。将第一乳液与含有包含两个或多个亲核胺基团的第二单体的含水混合物组合，从而形成第二乳液。通过界面聚合使第二乳液的第一和第二单体反应，由此形成聚氨酯。聚氨酯的数均分子量（Mn）可以为约30000至约80000.该方法与通过环状碳酸酯前体向第一单体引入侧链官能团相容。

2. 发明授权

US08344192B2 Process for the recovery of fluoromonomers 有权
标题翻译：回收氟单体的方法
公开(公告)号：US08344192B2
公开(公告)日：2013-01-01
申请号：US12514961
申请日：2007-12-07
申请人： Tadaharu Isaka , Tadashi Ino , Masaharu Nakazawa , Masahiro Kondo
发明人： Tadaharu Isaka , Tadashi Ino , Masaharu Nakazawa , Masahiro Kondo
IPC分类号： C08F2/00 , C08F12/20 , C08F14/14 , C08G75/00 , C08G73/24 , C07C315/00 , C07C17/00 , C07C25/13 , C07C21/18 , C07C17/38
CPC分类号： C08F214/186 , C08F6/003 , C08F14/18 , C08L27/12 , C08F2/22
摘要： The invention provides a technique enabling the separation and recovery of an unreacted fluoromonomer from an aqueous fluoropolymer dispersion obtained by emulsion polymerization, without using any extraction solvent, and enabling the prevention of a hydrolysis of —SO2F and a like sulfonic acid precursor functional group convertible to sulfonic acid group. Thus, the invention provides a recovering method fluoromonomer having a sulfonic acid precursor functional group convertible to a sulfonic acid group and remaining unreacted from an aqueous fluoropolymer dispersion obtained by emulsion polymerization of the fluoromonomer, wherein the unreacted fluoromonomer is recovered from the aqueous fluoropolymer dispersion by evaporation, wherein the aqueous fluoropolymer dispersion has an acidic pH.
摘要翻译：本发明提供一种能够通过乳液聚合得到的含氟聚合物水分散体分离和回收未反应的含氟单体的技术，而不使用任何提取溶剂，并且能够防止-SO2F等可转化为磺酸基。因此，本发明提供了一种具有磺酸前体官能团可转化成磺酸基团的还原方法的含氟单体，并且通过所述含氟单体的乳液聚合得到的含氟聚合物水分散体残留未反应，其中从含氟聚合物水分散体中回收未反应的含氟单体，蒸发，其中含氟聚合物水分散体具有酸性pH。

3. 发明授权

US07910686B2 Block copolymer and application thereof 失效
标题翻译：嵌段共聚物及其应用
公开(公告)号：US07910686B2
公开(公告)日：2011-03-22
申请号：US10531265
申请日：2003-10-14
申请人： Hiroshi Shinoda , Atsushi Terahara
发明人： Hiroshi Shinoda , Atsushi Terahara
IPC分类号： C08G73/24
CPC分类号： C08L53/00 , C08G65/00 , C08G65/007 , C08G65/40 , C08J5/2256 , C08J2371/12 , C08J2387/00 , H01B1/122 , H01M4/86 , H01M8/1004 , H01M8/1025 , H01M8/1027 , H01M8/1032 , H01M8/1039 , H01M2300/0082 , C08L2666/02
摘要： The present invention relates to a block copolymer having at least one block having an acid group and at least one block having substantially no acid group, wherein one end group of a repeating unit in at least one block of all blocks is oxygen and/or sulfur, and at least one repeating unit of a block having substantially no acid group contains a halogen atom. The block copolymer of the present invention gives a polymer electrolyte membrane which is excellent not only in heat resistance and proton conductivity but also in water resistance and chemical stability, and is useful as an electrolyte for a proton conducting membrane etc. of a fuel cell.
摘要翻译：本发明涉及具有至少一个具有酸基的嵌段和至少一个基本上没有酸基的嵌段的嵌段共聚物，其中所有嵌段的至少一个嵌段中的重复单元的一个端基是氧和/或硫，并且基本上不含酸基的嵌段的至少一个重复单元含有卤素原子。本发明的嵌段共聚物得到不仅在耐热性和质子传导性以及耐水性和化学稳定性方面优异的高分子电解质膜，而且可用作燃料电池的质子传导膜等的电解质。

4. 发明授权

US07847056B2 Method for producing fluorine-containing (meth)acrylate polymer and polymer produced by such method 有权
标题翻译：制备含氟（甲基）丙烯酸酯聚合物和通过这种方法制备的聚合物的方法
公开(公告)号：US07847056B2
公开(公告)日：2010-12-07
申请号：US10594977
申请日：2005-03-25
申请人： Etsuo Horii , Hirosuke Kawabata , Toshikazu Hirao , Akiya Ogawa , Xiaoliang Xu
发明人： Etsuo Horii , Hirosuke Kawabata , Toshikazu Hirao , Akiya Ogawa , Xiaoliang Xu
IPC分类号： C08G63/50 , C08G73/24 , C08F6/06
CPC分类号： C08F8/18 , C08F8/14 , C08F20/12
摘要： An object of the invention is to provide a fluorine-containing (meth)acrylate polymer readily at a low cost without using any special polymerization facilities. Thus, the invention provides a fluorine-containing (meth)acrylate polymer obtained by reacting a (meth)acrylate polymer with an alcohol containing a fluorine atom represented by General Formula 1: Rf(CH2)nOH (1) wherein Rf is a fluoroalkyl group or a fluoroalkyl ether group of 1 to 15 carbon atoms containing at least one or more fluorine atoms and n is an integer of 0 to 10 as well as a method for producing the same.
摘要翻译：本发明的目的是在不使用任何特殊聚合设备的情况下以低成本容易地提供含氟（甲基）丙烯酸酯聚合物。因此，本发明提供通过使（甲基）丙烯酸酯聚合物与通式1表示的含氟原子的醇反应得到的含氟（甲基）丙烯酸酯聚合物：Rf（CH2）nOH（1）其中Rf为氟烷基或含有至少一个以上氟原子的1〜15个碳原子的氟烷基醚基，以及n为0〜10的整数，以及其制造方法。

5. 发明申请

US20100222526A1 METHOD FOR PRODUCING A COPOLYMER FOR PHOTORESIST 有权
标题翻译：用于生产光电聚合物的共聚物的方法
公开(公告)号：US20100222526A1
公开(公告)日：2010-09-02
申请号：US12702356
申请日：2010-02-09
申请人： Tomo Oikawa , Eiichi Ikawa
发明人： Tomo Oikawa , Eiichi Ikawa
IPC分类号： C08F2/00 , C08G63/08 , C08G65/00 , C08G73/00 , C08G65/34 , C08G73/24
CPC分类号： C08F2/06 , C08F2/00 , C08F220/28
摘要： The present invention provides a method for production of a copolymer for photoresists in which the bias of the monomer composition ration is small. This method for production is a method for production of a copolymer for photoresists, which copolymer containing at least two types of repeating units, the method having a supplying step of supplying a monomer solution and a solution containing a polymerization initiator into a polymerization reaction system, wherein the range of fluctuation of the monomer composition ratio of unreacted monomers is within the range between minus 15% and plus 15% or the standard deviation of the monomer composition ratio of unreacted monomers is within 2 in the polymerization reaction system during the period from the start of the polymerization reaction to the end of supplying of the monomer solution.
摘要翻译：本发明提供一种制备光聚合物共聚物的方法，其中单体组成比例的偏差小。该制造方法是制造光致抗蚀剂共聚物的方法，该共聚物含有至少两种重复单元，该方法具有将单体溶液和含有聚合引发剂的溶液供给到聚合反应体系中的供给工序，其中未反应单体的单体组成比的波动范围在-15％和15％之间的范围内，或者在聚合反应体系中未反应单体的单体组成比的标准偏差在2以内的范围内开始聚合反应直到单体溶液的供应结束。

6. 发明申请

US20100160598A1 PROCESS FOR PRODUCING FLUOROPOLYMER PARTICLES 有权
标题翻译：生产氟聚合物颗粒的方法
公开(公告)号：US20100160598A1
公开(公告)日：2010-06-24
申请号：US12644306
申请日：2009-12-22
申请人： Susumu SAITO , Tetsuji SHIMOHIRA , Takashi SAEKI , Junichi TAYANAGI
发明人： Susumu SAITO , Tetsuji SHIMOHIRA , Takashi SAEKI , Junichi TAYANAGI
IPC分类号： C08G75/00 , C08G73/24
CPC分类号： C08F6/24 , C08F6/001 , C08F6/003 , C08F6/12 , C08F6/20 , C08F6/22 , C08F14/18 , C08L27/12 , C08F2/04
摘要： To provide a process for producing fluoropolymer particles, whereby formation of fine particles is suppressed.A process for producing fluoropolymer particles, which comprises (i) a step of preparing a solution or dispersion of a fluoropolymer (A) having the fluoropolymer (A) dissolved or dispersed in a solvent (B), wherein the solvent (B) contains a good solvent (B2) whereby the degree of swelling of the fluoropolymer (A) exceeds 50%, and the degree of swelling of the fluoropolymer (A) by the solvent (B) is from 50 to 1,200%; and (ii) a step of mixing the solution or dispersion of a fluoropolymer (A) with a solvent (C) to flocculate the fluoropolymer (A) thereby to form particles of the fluoropolymer (A), wherein the solvent (C) contains a poor solvent (C1) whereby the degree of swelling of the fluoropolymer (A) is at most 50%, the degree of swelling of the fluoropolymer (A) by a mixed solvent (BC) of the solvents (B) and (C) is from 0 to 100%, the ratio (WC/WB) of the mass (WC) of the solvent (C) to the mass (WB) of the solvent (B) is from 1 to 5, and the ratio (SBC/SB) of the degree of swelling (SBC) of the fluoropolymer (A) by the mixed solvent (BC) to the degree of swelling (SB) of the fluoropolymer (A) by the solvent (B) is at most 0.5.
摘要翻译：提供一种生产含氟聚合物颗粒的方法，从而抑制细颗粒的形成。一种制备含氟聚合物颗粒的方法，其包括（i）制备溶解或分散在溶剂（B）中的含氟聚合物（A）的含氟聚合物（A）的溶液或分散体的步骤，其中溶剂（B）含有良溶剂（B2），含氟聚合物（A）的溶胀度超过50％，溶剂（B）的含氟聚合物（A）的溶胀度为50〜1200％和（ii）将含氟聚合物（A）的溶液或分散体与溶剂（C）混合以使含氟聚合物（A）絮凝从而形成含氟聚合物（A）的颗粒的步骤，其中溶剂（C）含有不良溶剂（C1），含氟聚合物（A）的溶胀度为50％以下，溶剂（B）和（C）的混合溶剂（BC）的含氟聚合物（A）的溶胀度为 0〜100％时，溶剂（C）的质量（WC）与溶剂（B）的质量（WB）的比（WC / WB）为1〜5，比例（SBC / SB ）混合溶剂（BC）的含氟聚合物（A）的溶胀度（SBC）与溶剂（B）的含氟聚合物（A）的溶胀度（SB）之比为0.5以下。

7. 发明申请

US20090061152A1 Methods for fabricating isolated micro- and nano- structures using soft or imprint lithography 有权
标题翻译：使用软或压印光刻制造隔离微结构和纳米结构的方法
公开(公告)号：US20090061152A1
公开(公告)日：2009-03-05
申请号：US11825469
申请日：2007-07-06
申请人： Joseph M. DeSimone , Jason P. Rolland , Benjamin W. Maynor , Larken E. Euliss , Ginger Denison Rothrock , Ansleye Dennis , Edward T. Samulski , R. Jude Samulski
发明人： Joseph M. DeSimone , Jason P. Rolland , Benjamin W. Maynor , Larken E. Euliss , Ginger Denison Rothrock , Ansleye Dennis , Edward T. Samulski , R. Jude Samulski
IPC分类号： B32B3/12 , B29C35/04 , B32B27/00 , C12N5/06 , C12N15/87 , C08G73/24
CPC分类号： A61K9/14 , A61K9/0097 , A61K9/5138 , A61K9/5153 , A61K9/5192 , A61K47/34 , B81C99/0085 , B82Y10/00 , B82Y40/00 , G03F7/0002 , H01L51/0004 , H01L51/0021 , Y10T428/24273 , Y10T428/24479 , Y10T428/3154
摘要： The presently disclosed subject matter describes the use of fluorinated elastomer-based materials, in particular perfluoropolyether (PFPE)-based materials, in high-resolution soft or imprint lithographic applications, such as micro- and nanoscale replica molding, and the first nano-contact molding of organic materials to generate high fidelity features using an elastomeric mold. Accordingly, the presently disclosed subject matter describes a method for producing free-standing, isolated nanostructures of any shape using soft or imprint lithography technique.
摘要翻译：目前公开的主题描述了基于氟化弹性体的材料，特别是基于全氟聚醚（PFPE）的材料在高分辨率软或压印光刻应用中的应用，例如微米和纳米级复制成型，以及第一纳米接触使用弹性体模具成型有机材料以产生高保真特征。因此，目前公开的主题描述了使用软或压印光刻技术生产任何形状的独立的，分离的纳米结构的方法。

8. 发明授权

US07432340B2 Fluorinated alkyl substituted-thieno[3,4-]thiophene monomers and polymers therefrom 有权
标题翻译：氟化烷基取代噻吩并[3,4-b]噻吩单体及其聚合物
公开(公告)号：US07432340B2
公开(公告)日：2008-10-07
申请号：US11128538
申请日：2005-05-13
申请人： Steffen Zahn , Gauri Sankar Lal , William Franklin Burgoyne, Jr. , Kristen Elaine Minnich , Andrew Francis Nordquist , Lloyd Mahlon Robeson , Francis Joseph Waller
发明人： Steffen Zahn , Gauri Sankar Lal , William Franklin Burgoyne, Jr. , Kristen Elaine Minnich , Andrew Francis Nordquist , Lloyd Mahlon Robeson , Francis Joseph Waller
IPC分类号： C08G73/24 , C08F4/80 , C08G75/00
CPC分类号： C08G61/123 , C08G61/126
摘要： Partially and fully fluorinated alkyl substituted thienothiophene monomers (and polymers thereof) wherein the monomers are represented by the formula: wherein R is a partially or fully fluorinated primary, secondary or tertiary alkyl having from 1 to 8 carbon atoms; and X and X′ are independently selected from the group consisting of H, F, Cl, Br, I, MgCl, MgBr, Mgl, Sn(R′)3, CH═CHR″, —OR″, —COOR″, —S—COR″, —B(OR″)2, —COR″, —C≡CH, and a polymerizable cyclic pi-conjugated carbon-ring structure optionally comprising S, N or O heteroatoms; wherein R′ is a primary, secondary or tertiary alkyl having from 1 to 6 carbon atoms, and R″ is H or a primary, secondary or tertiary alkyl having from 1 to 6 carbon atoms.
摘要翻译：部分和完全氟化的烷基取代的噻吩并噻吩单体（及其聚合物），其中单体由下式表示：其中R是具有1至8个碳原子的部分或完全氟化的伯，仲或叔烷基; 并且X和X'独立地选自H，F，Cl，Br，I，MgCl，MgBr，MgI，Sn（R'）3，CH-CHR“， - OR“，-COOR”，-S-COR“，-B（OR”）2，-COR“，-C≡CH和可聚合的环状π-共轭碳任选地包含S，N或O杂原子的环结构; 其中R'是具有1至6个碳原子的伯，仲或叔烷基，R“是H或具有1至6个碳原子的伯，仲或叔烷基。

9. 发明申请

US20080090179A1 Novel polymer, resist composition and patterning process using the same 有权
标题翻译：新型聚合物，抗蚀剂组合物和使用其的图案化工艺
公开(公告)号：US20080090179A1
公开(公告)日：2008-04-17
申请号：US11902760
申请日：2007-09-25
申请人： Takanobu Takeda , Osamu Watanabe , Satoshi Watanabe , Ryuji Koitabashi , Keiichi Masunaga , Tamotsu Watanabe
发明人： Takanobu Takeda , Osamu Watanabe , Satoshi Watanabe , Ryuji Koitabashi , Keiichi Masunaga , Tamotsu Watanabe
IPC分类号： C08G65/34 , C08G73/24 , G03C1/00 , G03C5/00
CPC分类号： G03F7/0397 , Y10S430/106
摘要： There is disclosed a polymer at least comprising repeating units represented by the following general formulae (1) and (2), and the polymer having a mass average molecular weight of 1,000 to 500,000. There can be provided a polymer, and a resist composition, in particular, a chemically amplified positive resist composition that exhibit higher resolution than conventional positive resist compositions, good in-plane dimension uniformity of developed resist patterns on substrates such as mask blanks and high etching resistance.
摘要翻译：公开了至少包含由以下通式（1）和（2）表示的重复单元，聚合物的质均分子量为1,000至500,000的聚合物。可以提供聚合物和抗蚀剂组合物，特别是具有比常规正性抗蚀剂组合物更高分辨率的化学放大正性抗蚀剂组合物，在诸如掩模毛坯和高蚀刻的基底上显影的抗蚀剂图案的良好的面内尺寸均匀性抵抗性。

10. 发明申请

US20060205921A1 Process for preparing peroxidic perfluoropolyethers 有权
标题翻译：制备过氧化全氟聚醚的方法
公开(公告)号：US20060205921A1
公开(公告)日：2006-09-14
申请号：US11366598
申请日：2006-03-03
申请人： Giuseppe Marchionni , Pier Guarda , Elvira Pagano
发明人： Giuseppe Marchionni , Pier Guarda , Elvira Pagano
IPC分类号： C08G73/24
CPC分类号： C08G65/007
摘要： A process for preparing peroxidic perfluoropolyethers having a perioxidic content (PO) lower than or equal to 1.2 of formula A-CF2O(CF2CF2O)m(CF2O)n—(CF2CF2OO)m1(CF2OO)n1CF2—B (I) Wherein A, B equal to or different from each other are —C1, —F, —F2CC1, —COF, —OCOF, —CF3, m, m1, n, n1 are integers such that the (m+m1)/(n+n1) ratio is between 0.6 and 1.3 and the m/n ration is between 0.5 and 1.2; the number average molecular weight is in the range 35,000-45,000, by tetrafluoroethylene (TFE) photooxidation in the presence of UV light, at a temperature from −80° C. to −40° C., in the presence of a mixture of solvents formed of HFC-227 (hepta-fluoropropane) and a solvent selected between HFC-125 (pentafluoroethane) and FC-218 (perfluoropropane).
摘要翻译：一种制备过氧化全氟聚醚的方法，该过氧化全氟聚醚具有低于或等于式（β）的1.2的线型式描述=“在线公式”中的最大值=“铅”→A-CF2 （CF 2 O 2）O（CF 2 O 2）O（CF 2 O 2）n（CF 2 O 2）n （CF 2 O 2）m1（CF 2 O 2）n1（CF 2 O 2）n1 其中A，B等于或不同于每一个，其中A，B等于或不同于每个其它是-C1，-F，-F2C1，-COF，-OCOF，-CF3，m，m1，n，n1是整数，使得（ m + m1）/（n + n1）的比例在0.6和1.3之间，m / n比在0.5和1.2之间; 在UV光的存在下，在-80℃至-40℃的温度下，在溶剂混合物存在下，数均分子量在35,000-45,000范围内，通过四氟乙烯（TFE）光氧化由HFC-227（七氟丙烷）和选自HFC-125（五氟乙烷）和FC-218（全氟丙烷）之间的溶剂形成。

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