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1. 发明授权

US4036885A Method for decomposing an aromatic aldehyde-hydrogen fluoride-boron fluoride complex 失效
标题翻译：分解芳香醛 - 氟化氢 - 氟化硼配合物的方法
公开(公告)号：US4036885A
公开(公告)日：1977-07-19
申请号：US654625
申请日：1976-02-02
申请人： Susumu Fujiyama , Minoru Takagawa , Shiro Kajiyama
发明人： Susumu Fujiyama , Minoru Takagawa , Shiro Kajiyama
IPC分类号： C07C45/83 , C07C45/85 , C07C45/24
CPC分类号： C07C45/83 , C07C45/85
摘要： This invention relates to a two-step method for decomposing an aromatic aldehyde-hydrogen fluoride-boron trifluoride complex in the presence of benzene as a diluent to obtain an aromatic aldehyde, hydrogen fluoride and boron trifluoride separately without causing any change in the quality of the aromatic aldehyde or without forming undesirable byproducts.
摘要翻译：本发明涉及一种在苯作为稀释剂存在下分解芳族醛 - 氟化氢 - 三氟化硼配合物的二步法，以分别得到芳族醛，氟化氢和三氟化硼，而不会导致任何质量变化芳香醛或不形成不期望的副产物。

2. 发明授权

US3998885A Method of separating components of nitrooxidation reaction mixture 失效
标题翻译：分离反应混合物组分的方法
公开(公告)号：US3998885A
公开(公告)日：1976-12-21
申请号：US371309
申请日：1973-06-18
申请人： Shizuo Yamada , Hiroo Sasaki , Tetsuo Tanaka
发明人： Shizuo Yamada , Hiroo Sasaki , Tetsuo Tanaka
IPC分类号： B01J38/00 , C01C1/18 , C07B61/00 , C07C67/00 , C07C201/00 , C07C201/16 , C07C205/45 , C07C76/02 , C07C45/02 , C07C45/24 , C07C76/06
CPC分类号： C07C201/16
摘要： 2-Nitrocycloalkanone, 2-nitrocycloalkenone or 2-nitrocycloalkadienone is separated from the nitrooxidation reaction mixture of a cyloalkene, a cycloalkadiene or a cycloalkatriene with oxygen and nitrogen oxide by contact with gaseous ammonia.

3. 发明授权

US3962343A Method for decomposing an aromatic aldehyde-hydrogen fluoride-boron fluoride complex 失效
标题翻译：分解芳香醛 - 氟化氢 - 氟化硼配合物的方法
公开(公告)号：US3962343A
公开(公告)日：1976-06-08
申请号：US468025
申请日：1974-05-08
申请人： Susumu Fujiyama , Minoru Takagawa , Shiro Kajiyama
发明人： Susumu Fujiyama , Minoru Takagawa , Shiro Kajiyama
IPC分类号： C07C45/51 , B01J27/32 , B01J38/56 , C01B7/19 , C01B35/06 , C07C45/00 , C07C45/49 , C07C45/83 , C07C45/85 , C07C47/52 , C07C67/00 , C07C45/24
CPC分类号： C07C45/85 , C07C45/00 , C07C45/49 , C07C45/83
摘要： This invention relates to a two-step method for decomposing an aromatic aldehyde-hydrogen fluoride-boron trifluoride complex in the presence of benzene as a diluent to obtain an aromatic aldehyde, hydrogen fluoride and boron trifluoride separately without causing any change in the quality of the aromatic aldehyde or without forming undesirable byproducts.
摘要翻译：本发明涉及一种在苯作为稀释剂存在下分解芳族醛 - 氟化氢 - 三氟化硼配合物的二步法，以分别得到芳族醛，氟化氢和三氟化硼，而不会导致任何质量变化芳香醛或不形成不期望的副产物。

4. 发明授权

US3895071A Separation of nitroketone from a crude nitrooxidation reaction product 失效
标题翻译：从粗硝基氧化反应产物中分离出硝基酮
公开(公告)号：US3895071A
公开(公告)日：1975-07-15
申请号：US43813474
申请日：1974-01-30
申请人： TEXACO INC
发明人： KABLAOUI MAHMOUD S , LOVE RICHARD F
IPC分类号： C07C201/16 , C07C45/24
CPC分类号： C07C201/16 , C01C1/10 , C01C1/185 , C07C205/45
摘要： Method for the purification of nitroketones from crude mixtures containing, in addition to the nitroketone, nitronitrates, nitroalcohols, denitrating agent and nitric acid, wherein the crude mixture is initially treated with ammonia thereby forming and separating the ammonium salt of the nitroketone and ammonium nitrate from the crude mixture, contacting the ammonium nitrate and ammonium salt of the nitroketone with a liquid hydrocarbon at a temperature sufficient to decompose the ammonium salt of the nitroketone to ammonia and said nitroketone, separating ammonia and ammonium nitrate from the hydrocarbon and nitroketone and separating the nitroketone from the hydrocarbon.
摘要翻译：从含有硝基酮，硝酸酯，硝基醇，脱硝剂和硝酸的粗混合物中纯化硝基酮的方法，其中粗混合物最初用氨处理，从而形成和分离硝基酮和硝酸铵的铵盐粗混合物，使硝基酮的硝酸铵和铵盐与液态烃接触，反应温度足以将硝基酮的铵盐分解成氨和硝基酮，从碳氢化合物和硝基酮中分离出氨和硝酸铵，并分离出硝基酮从烃。

5. 发明授权

US3574765A Process for decolorization of glyoxal 失效
标题翻译： GLYOXAL脱胶工艺
公开(公告)号：US3574765A
公开(公告)日：1971-04-13
申请号：US3574765D
申请日：1968-08-30
申请人： UNION CARBIDE CORP
发明人： KURYLA WILLIAM C , JACKSON JACK
IPC分类号： C07C45/78 , C07C45/24
CPC分类号： C07C45/78 , C07C47/127
摘要： A PROCESS FOR REDUCING COLOR FROM COLORED GLYOXAL SOLUTION WHICH COMPRISES CONTACTING COLORED GLYOXAL SOLUTION WITH OZONE IN AN AMOUNT AND FOR A TIME SUFFICIENT TO REDUCE THE COLOR OF SAID GLYOXAL SOLUTION.

6. 发明授权

US3558719A Recovery of aqueous formaldehyde by extraction with an alkanol followed by distillation 失效
标题翻译：通过蒸馏除去含有甲醛的水溶性甲醛的还原
公开(公告)号：US3558719A
公开(公告)日：1971-01-26
申请号：US3558719D
申请日：1968-05-27
申请人： EXXON RESEARCH ENGINEERING CO
发明人： CIER HARRY E
IPC分类号： C07C45/80 , C07C45/82 , C07C45/24
CPC分类号： C07C45/80 , C07C45/82 , C07C47/04
摘要： AN AQUEOUS FORMALDEHYDE-CONTAINING STREAM SUCH AS ONE FROM THE SULFURIC ACID CATALYZED CONDENSATION OF AROMATIC HYDROCARBON AND FORMALDEHYDE IS EXTRACTED WITH AN ALCOHOL HAVING AT LEAST 4 CARBON ATOMS AT A TEMPERATURE BELOW THE ALCOHOL-FORMALDEHYDE DISSOCIATION TEMPERATURE, THE ALCOHOL EXTRACTANT BEING SEPARATED FROM THE AQUEOUS STREAM AND DISTILLED UNDER SPECIFIC CONDITIONS TO RECOVER THE FORMALDEHYDE.

7. 发明授权

US3480676A Process of purifying ketene 失效
标题翻译：净化KETENE的过程
公开(公告)号：US3480676A
公开(公告)日：1969-11-25
申请号：US3480676D
申请日：1967-11-03
申请人： LONZA AG
发明人： SCHEUBER HERMANN
IPC分类号： C07C45/90 , C07C49/22 , C07C45/24
CPC分类号： C07C45/90

8. 发明授权

US4202828A Process for separation of naphthoquinone and phthalic acid 失效
标题翻译：分离萘醌和邻苯二甲酸的方法
公开(公告)号：US4202828A
公开(公告)日：1980-05-13
申请号：US868349
申请日：1978-01-10
申请人： Ryo Matsuura , Tatsuyoshi Komatsu , Yukio Nomiyama , Kenji Usui
发明人： Ryo Matsuura , Tatsuyoshi Komatsu , Yukio Nomiyama , Kenji Usui
IPC分类号： C07C46/04 , C07C46/10 , C07C51/487 , C07C45/24 , C07C49/66 , C07C51/48 , C07C63/16
CPC分类号： C07C46/10 , C07C46/04 , C07C51/487
摘要： In a process for separation of naphthoquinone and phthalic acid from an aqueous slurry prepared by contacting a reaction mixture gas formed by a catalytic vapor phase oxidation of naphthalene with an aqueous medium, the decomposition of naphthoquinone is prevented and phthalic acid is substantially separated by adding a base to the aqueous slurry so as to neutralize only sulfuric acid component and maleic acid component without substantially neutralizing phthalic acid component and heating the aqueous slurry to dissolve phthalic acid to form a slurry of naphthoquinone in an aqueous solution of phthalic acid and extracting naphthoquinone with a solvent while preventing a crystallization of phthalic acid.A pH of the aqueous slurry is adjusted in a range of 1.2 to 2.5 before the heat dissolution of phthalic acid and the extraction of naphthoquinone.An aqueous phase obtained after the extraction of naphthoquinone is cooled to crystallize phthalic acid and then the filtrate separating from the resulting slurry is used as an aqueous medium for contacting with the reaction mixture gas, optionally after adjusting pH in a range of 1.2 to 2.5.
摘要翻译：在通过将通过萘的催化气相氧化形成的反应混合物气体与水性介质接触而制备的水性浆液分离萘醌和邻苯二甲酸的方法中，萘醌的分解被防止，邻苯二甲酸通过加入以仅中和硫酸成分和马来酸成分，而基本不中和邻苯二甲酸成分，加热含水浆料溶解邻苯二甲酸，形成萘醌在邻苯二甲酸水溶液中的浆液，并用萘磺酸提取萘醌溶剂，同时防止邻苯二甲酸的结晶。在邻苯二甲酸的热溶解和萘醌的萃取之前，将水性浆液的pH调节在1.2〜2.5的范围内。冷却萃取萘醌后得到的水相，使邻苯二甲酸结晶，然后将所得浆液分离出的滤液用作与反应混合物气体接触的水性介质，任选在将pH调节在1.2〜2.5的范围内后，

9. 发明授权

US4163027A Working-up of reaction mixtures containing cyclohexanol and cyclohexanone 失效
标题翻译：含有环己醇和环己酮的反应混合物的处理
公开(公告)号：US4163027A
公开(公告)日：1979-07-31
申请号：US844985
申请日：1977-10-25
申请人： Peter Magnussen , Guenter Herrmann , Elmar Frommer
发明人： Peter Magnussen , Guenter Herrmann , Elmar Frommer
IPC分类号： C07C20060101 , C07C27/12 , C07C27/26 , C07C35/08 , C07C49/303 , C07C49/403 , C07C29/24 , C07C45/24
摘要： A process for working up reaction mixtures containing cyclohexanol and cyclohexanone, which have been obtained by oxidizing cyclohexane with molecular oxygen or gases containing molecular oxygen, in the liquid phase, at from 130.degree. to 200.degree. C. under a pressure of from 5 to 25 bars, working-up being effected by treatment with aqueous solutions of an alkali metal hydroxide and/or alkali metal carbonate in two stages, the fresh aqueous alkali metal hydroxide and/or alkali metal carbonate solution being fed to the second stage and the separated-off spent alkali being brought into contact with fresh reaction mixture in the first stage. The treatment in the first stage is carried out in the presence of inert gases and the inert gases are separated off before the second stage.
摘要翻译：在液相中在130〜200℃下，在5〜25的压力下，通过用分子氧或含有分子氧的气体氧化环己烷而得到的含有环己醇和环己酮的反应混合物的方法通过两步处理碱金属氢氧化物和/或碱金属碳酸盐的水溶液进行后处理，将新鲜的碱金属氢氧化物和/或碱金属碳酸盐水溶液进料到第二阶段，在第一阶段使废碱与新鲜的反应混合物接触。第一阶段的处理是在惰性气体的存在下进行的，惰性气体在第二阶段之前被分离出来。

10. 发明授权

US4162269A Purification process for 3-phenoxybenzaldehyde 失效
标题翻译： 3-苯氧基苯甲醛的纯化方法
公开(公告)号：US4162269A
公开(公告)日：1979-07-24
申请号：US825154
申请日：1977-08-16
申请人： Masato Mizutani , Akio Higo , Nobuo Ohno , Hajime Hirai
发明人： Masato Mizutani , Akio Higo , Nobuo Ohno , Hajime Hirai
IPC分类号： C07C47/575 , C07C45/00 , C07C45/85 , C07C67/00 , C07C301/00 , C07C303/32 , C07C45/24
CPC分类号： C07C45/85
摘要： A purification process for 3-phenoxybenzaldehyde, which comprises reacting crude 3-phenoxybenzaldehyde with an alkali metal or ammonium bisulfite, or metabisulfite in the presence of an organic quaternary ammonium salt, an inorganic acid salt of organic tertiary amines, or a macrocyclic polyether used as a catalyst, isolating the resulting 3-phenoxybenzaldehyde alkali metal or ammonium bisulfite adduct, and decomposing it by using an acid or a base, or by heating.
摘要翻译： 3-苯氧基苯甲醛的纯化方法，其包括在有机季铵盐，有机叔胺的无机酸盐或大环聚醚的存在下使粗3-苯氧基苯甲醛与碱金属或亚硫酸氢铵或偏亚硫酸氢钠反应，或者将大环聚醚用作催化剂，分离得到的3-苯氧基苯甲醛碱金属或亚硫酸氢铵加合物，并用酸或碱分解，或加热。

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