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1. 发明授权

US4743694A Diastereocontrolled synthesis of 2-amino alcohols 失效
标题翻译： 2-氨基醇的非对映控制合成
公开(公告)号：US4743694A
公开(公告)日：1988-05-10
申请号：US851073
申请日：1986-04-11
申请人： David A. Claremon
发明人： David A. Claremon
IPC分类号： C07D307/52 , C07D333/36 , C07F1/02 , C07F7/08 , C07D327/00 , C07C109/12 , C07C109/16
CPC分类号： C07C251/72 , C07C243/00 , C07D307/52 , C07F7/0818
摘要： The addition of organolithium to dimethylhydrazones of certain ethers of a-hydroxyaldehydes results in the synthesis of threo- or erythro- intermediates readily convertible to threo- or erythro-2-amino alcohols.
摘要翻译：将有机锂添加到α-羟基醛的某些醚的二甲基腙中导致苏氨酸或赤型 - 中间体的合成容易转化成苏氨基或赤式-2-氨基醇。

2. 发明授权

US4621156A Optical filter agents and photographic products and processes containing same 失效
标题翻译：光学过滤剂和含有它们的摄影产品和方法
公开(公告)号：US4621156A
公开(公告)日：1986-11-04
申请号：US309914
申请日：1981-10-08
申请人： Derek H. R. Barton , Irena Y. Bronstein-Bonte , Lloyd D. Taylor
发明人： Derek H. R. Barton , Irena Y. Bronstein-Bonte , Lloyd D. Taylor
IPC分类号： G03C8/48 , C07C109/12
CPC分类号： G03C8/48
摘要： Optical filter agents and photographic products and processes using same are disclosed. The optical filter agents are pH-sensitive hydrazone compounds conforming to the following structural formula: ##STR1## where R is any group which can provide a double bond for conjugation with the ##STR2## portion of the compound to provide light-absorbing capability or color for the agent at a pH above its pKa, X is a substituent of R providing at least one electron-withdrawing group and each R' can be defined as any substituent that does not impair the light-absorbing capacity of the compound at a pH above the pKa thereof. The pH-sensitive optical filter agents have a highly colored light-absorbing form at a pH above the pKa and are substantially non-absorbing at a pH below the pKa. The pH-sensitive optical filter agents are useful in photographic film units and processes for the protection of photoexposed photosensitive elements against the occurrence of fogging during in-light development.
摘要翻译：公开了使用其的光学过滤剂和照相产品和方法。光学过滤剂是符合以下结构式的pH敏感腙化合物：其中R是可以提供双键与化合物的部分缀合以提供光吸收能力或颜色的任何基团对于高于其pKa的pH的试剂，X是提供至少一个吸电子基团的R的取代基，并且每个R'可以被定义为在上述pH下不影响化合物的光吸收能力的任何取代基其pKa。 pH敏感的光学过滤剂在高于pKa的pH下具有高度着色的光吸收形式，并且在低于pKa的pH下基本上不吸收。 pH敏感的光学过滤剂可用于照相胶片单元和用于保护光敏元件免于在光照显影过程中发生起雾的过程。

3. 发明授权

US4387104A N-Substituted pyruvic acid hydrazones, preparation thereof and pharmaceutical compositions containing them 失效
标题翻译： N-取代的丙酮酸腙，其制备物和含有它们的药物组合物
公开(公告)号：US4387104A
公开(公告)日：1983-06-07
申请号：US292869
申请日：1981-08-14
申请人： Ruth Heerdt , Hans P. Wolff , Fritz Kaiser , Wolfgang Schaumann , Hans Kuhnle
发明人： Ruth Heerdt , Hans P. Wolff , Fritz Kaiser , Wolfgang Schaumann , Hans Kuhnle
IPC分类号： A61K31/15 , A61K31/19 , A61K31/195 , A61P3/08 , A61P3/10 , C07C67/00 , C07C241/00 , C07C251/08 , C07C251/76 , C07C317/14 , C07C109/12
CPC分类号： C07C251/72
摘要： A pyruvic acid hydrazone derivative of the formula: ##STR1## wherein R is an aryl radical optionally substituted by lower alkyl or is an aliphatic hydrocarbon radical which can be substituted by a lower alkoxy, a cycloalkyl or an optionally substituted aryl radical,A is an alkylene radical containing 2 to 8 carbon atoms, with at least 2 carbon atoms between B and the nitrogen atom, andB is an oxygen or sulphur atom;or a physiologically acceptable salt, ester or amide thereof which possesses hypoglycaemic activity.
摘要翻译：一种下式的丙酮酸腙衍生物，其中R是任选被低级烷基取代的芳基，或者是可被低级烷氧基，环烷基或任意取代的芳基取代的脂族烃基，A是含有2至8个碳原子的亚烷基，B和氮原子之间至少有2个碳原子，B是氧或硫原子; 或其具有低血糖活性的生理上可接受的盐，酯或酰胺。

4. 发明授权

US3809675A Phenylhydrazone antioxidants for polyolefins 失效
标题翻译：聚苯乙烯抗氧化剂
公开(公告)号：US3809675A
公开(公告)日：1974-05-07
申请号：US30464272
申请日：1972-11-08
申请人： BELL TELEPHONE LABOR INC
发明人： HANSEN R
IPC分类号： C08K5/30 , C07C109/12 , C08G51/60
CPC分类号： C07C251/72 , C08K5/30 , C08L23/02
摘要： OXIDATIVE DEGRADATION IN POLYMERIC HYDROCARBON MATERIALS SUCH AS POLYETHYLENE AND POLYPROPYLENE IS RETARDED BY INCORPORATION THEREIN OF PHENYLHYDRAZONES.

5. 发明授权

US4570002A Carbazic acid derivatives 失效
标题翻译：咔唑酸衍生物
公开(公告)号：US4570002A
公开(公告)日：1986-02-11
申请号：US573586
申请日：1984-01-24
申请人： Zoltan Budai , Pal Benko , Ildiko Ratz nee Simonek , Eva Rakoczy nee Pinter , Karoly Magyar , Jozsef Kelemen , Attila Mandi
发明人： Zoltan Budai , Pal Benko , Ildiko Ratz nee Simonek , Eva Rakoczy nee Pinter , Karoly Magyar , Jozsef Kelemen , Attila Mandi
IPC分类号： C07C281/02 , A23K1/16 , A23K1/18 , C07C67/00 , C07C239/00 , C07C281/04 , C07C125/065 , A61K31/15 , C07C109/12
CPC分类号： A23K50/30 , A23K20/105 , A23K20/111
摘要： The invention relates to new carbazic acid derivatives, a process for the preparation thereof and compositions--particularly feed additives and animal feeds--containing the same.The new compounds according to the invention correspond to the formula (I)R.sup.1 .dbd.N--NH--COOR.sup.3 (I)whereinR.sup.1 stands for a C.sub.7-12 cycloalkylidene group, an indanylidene group or a group of the formula (IX) ##STR1## wherein A represents a phenyl group optionally carrying one or more identical or different substituents selected from the group consisting of halo nitro, hydroxy, C.sub.1-14 alkoxy, C.sub.1-4 alkyl, amino or C.sub.1-4 alkoxycarbonylhydrazino; phenyl-(C.sub.1-4 alkyl), C.sub.1-16 alkyl, C.sub.3-7 cycloalkyl or indolyl or a C.sub.3 -C.sub.6 cycloalkyl group substituted by a C.sub.3 -C.sub.6 cycloalkyl group;R.sup.2 denotes a hydrogen atom, a C.sub.1-16 alkyl or a C.sub.3-7 cycloalkyl group; andR.sup.3 represents a C.sub.1-4 alkyl group.
摘要翻译：本发明涉及新的卡巴酸衍生物，其制备方法和组合物 - 特别是饲料添加剂和含有它们的动物饲料。根据本发明的新化合物对应于式（I）R 1 = N-NH-COOR 3（I）其中R 1表示C 7-12亚环烷基，亚茚基或式（Ⅸ）的基团）（IX）其中A表示任选携带一个或多个相同或不同的取代基的苯基，所述取代基选自卤代硝基，羟基，C 1-14烷氧基，C 1-4烷基，氨基或C 1-4烷氧基羰基肼; 苯基 - （C 1-4烷基），C 1-16烷基，C 3-7环烷基或吲哚基或被C 3 -C 6环烷基取代的C 3 -C 6环烷基; R2表示氢原子，C1-16烷基或C3-7环烷基; 并且R 3表示C 1-4烷基。

6. 发明授权

US3502721A Selected polyfluorinated hydrazones and hydrazinohydrazones 失效
标题翻译：选择的多氟化合物和水合肼
公开(公告)号：US3502721A
公开(公告)日：1970-03-24
申请号：US3502721D
申请日：1966-08-18
申请人： DU PONT
发明人： KRESPAN CARL G
IPC分类号： C08F2/38 , C07C109/12
CPC分类号： C08F2/38 , C07C251/72

7. 发明授权

US5298658A Photographic elements with reduced print-through 失效
标题翻译：具有减少打印的照片元素
公开(公告)号：US5298658A
公开(公告)日：1994-03-29
申请号：US811771
申请日：1991-12-20
申请人： Dietrich M. Fabricius
发明人： Dietrich M. Fabricius
IPC分类号： G03C1/00 , C09B29/01 , C09B29/15 , C09B29/32 , C09B29/36 , C09B29/52 , G03C1/815 , G03C1/83 , C07C109/12 , C07D109/12 , C07D211/40 , C07D239/70 , C07D491/00
CPC分类号： C09B29/0003 , C09B29/10 , C09B29/3673 , C09B29/3678 , G03C1/831
摘要： A photographic element is detailed which provides for improved resolution by decreasing the blue and ultraviolet radiation typically associated with internal scatter and print-through. These and other improvements are provided in a photographic element comprising a support having thereon at least one hydrophilic colloid layer, and a radiation sensitive silver halide emulsion layer present as a portion of the colloid layer or in a separate layer wherein the emulsion contains a dye of the formula: ##STR1## wherein: A=counterion chosen from the set consisting of lithium, sodium, potassium, ammonium and alkylammonium andZ is a linking group.
摘要翻译：详细的照相材料通过减少通常与内部散射和打印通过相关联的蓝色和紫外线辐射来提供改进的分辨率。这些和其它改进提供在照相元件中，其中包括其上具有至少一个亲水胶体层的支撑体和作为胶体层的一部分存在的辐射敏感卤化银乳剂层或其中乳液含有染料式：（*化学结构*）其中：A =选自由锂，钠，钾，铵和烷基铵组成的组的抗衡离子，Z是连接基团。

8. 发明授权

US4473708A Preparation of ketozines using organoarsenic compounds 失效
标题翻译：用有机砷化合物制备酮基
公开(公告)号：US4473708A
公开(公告)日：1984-09-25
申请号：US396572
申请日：1982-07-09
申请人： Yasuhisa Kuriyama , Minoru Kakuda , Shoichi Nitoh
发明人： Yasuhisa Kuriyama , Minoru Kakuda , Shoichi Nitoh
IPC分类号： C07B61/00 , B01J23/00 , B01J23/18 , B01J31/00 , B01J31/12 , C07C67/00 , C07C241/00 , C07C251/88 , C07C109/12 , C07C109/14 , C07C109/16 , C07C119/00
CPC分类号： C07C251/88
摘要： A process for preparing a ketazine useful as an intermediate for the synthesis of hydrazine is disclosed. The process comprises reacting an aliphatic or aromatic ketone with ammonia and hydrogen peroxide in the presence of a catalyst of an arsenic compound to produce a corresponding ketazine.
摘要翻译：公开了一种制备可用作肼合成中间体的酮连氮的方法。该方法包括在砷化合物的催化剂存在下使脂族或芳族酮与氨和过氧化氢反应以产生相应的酮连氮。

9. 发明授权

US4332948A Novel hydrazone compounds and process for preparing the same 失效
标题翻译：新型腙化合物及其制备方法
公开(公告)号：US4332948A
公开(公告)日：1982-06-01
申请号：US149752
申请日：1980-05-14
申请人： Kiyoshi Sakai , Mitsuru Hashimoto , Kyoji Tsutsui
发明人： Kiyoshi Sakai , Mitsuru Hashimoto , Kyoji Tsutsui
IPC分类号： C07C67/00 , C07C241/00 , C07C251/86 , C07D213/53 , C07D307/36 , C07D307/52 , C07D333/20 , C07D333/22 , C07D333/36 , C09B26/02 , G03C1/72 , G03G5/06 , C07C109/12
CPC分类号： C07D213/53 , C07C251/72 , C07D307/52 , C07D333/22 , G03G5/0616 , G03G5/0629 , G03G5/0637
摘要： Hydrazone compounds having the general formula ##STR1## wherein Ar is selected from the group consisting of a naphthalene ring radical, substituted naphthalene ring radicals, an anthracene ring radical, substituted anthracene ring radicals, styryl, substituted styryls, a pyridine radical, a furan ring radical and a thiophene ring radical.The hydrazone compounds can be prepared by allowing 1-methyl-1-phenylhydrazine having the formula ##STR2## to react with an aldehyde represented by the general formula Ar-CHO, wherein Ar is the same as mentioned above at a substantially equal molar ratio in an organic solvent selected from the group consisting of lower alcohols, cyclic ethers, cellosolves, N,N-dimethylforamide and acetic acid, in the presence of an acid catalyst, by heating and refluxing the reaction mixture.The hydrazone compounds are extremely useful as charge transport materials for use in electrophotographic photoconductors of the type comprising an electroconductive support material and a photosensitive layer containing a charge generation material and a charge transport material.
摘要翻译：具有通式的腙化合物，其中Ar选自萘环基，取代萘环基，蒽环基，取代的蒽环，苯乙烯基，取代的苯乙烯基，吡啶基，呋喃环自由基和噻吩环基团。腙化合物可以通过使具有式“IMAGE”的1-甲基-1-苯肼与通式Ar-CHO表示的醛反应来制备，其中Ar与上述相同，其摩尔比基本相等在酸催化剂存在下，通过加热和回流反应混合物，选自低级醇，环醚，溶纤剂，N，N-二甲基甲酰胺和乙酸的有机溶剂。腙化合物作为用于电子照相感光体的电荷传输材料是非常有用的，其中包括导电载体材料和含有电荷产生材料和电荷传输材料的感光层。

10. 发明授权

US4233242A Process for producing ketazine by reacting a ketone with ammonia and a peroxide 失效
标题翻译：通过使酮与氨和过氧化物反应制备酮连氮的方法
公开(公告)号：US4233242A
公开(公告)日：1980-11-11
申请号：US27895
申请日：1979-04-06
申请人： Nobuyuki Nagato , Yuichi Sugiyama
发明人： Nobuyuki Nagato , Yuichi Sugiyama
IPC分类号： C07C109/12 , C07C109/14 , C07C109/16 , C07C119/00
CPC分类号： C07C251/88
摘要： Ketazines having the general formula (I) ##STR1## wherein R.sub.1 represents alkyl group having 1 to 4 carbon atoms and R.sub.2 represents (i) an alkyl group having 1 to 4 carbon atoms or (ii) a phenyl group optionally substituted with an alkyl group having 1 to 4 carbon atoms, an alkoxy group having 1 to 4 carbon atoms or a halogen group, and R.sub.1 and R.sub.2 together with the carbon atom to which they are both bonded may form a ring, are advantageously manufactured by reacting an aliphatic or aromatic ketone having the formula (II) ##STR2## wherein R.sub.1 and R.sub.2 are as defined above, with ammonia and a peroxide compound or compounds in the presence of amorphous silica or palladium compounds, as a catalyst, at a temperature of from 0.degree. to 120.degree. C., in a liquid phase.
摘要翻译：具有通式（I）的化合物其中R 1表示具有1至4个碳原子的烷基，R 2表示（i）具有1至4个碳原子的烷基或（ii）任选被具有1至4个碳原子的烷基，具有1至4个碳原子的烷氧基或卤素基团，并且R 1和R 2与它们所连接的碳原子一起形成环可有利地通过使在无定形二氧化硅或钯化合物作为催化剂存在下，在氨气和过氧化物或化合物作为催化剂的情况下，具有式（II）的脂族或芳族酮（II）其中R 1和R 2如上定义，为0〜120℃，为液相。

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