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1. 发明授权

US4347383A Process for producing benzophenone-azines 失效
标题翻译：生产二苯甲酮吖嗪的方法
公开(公告)号：US4347383A
公开(公告)日：1982-08-31
申请号：US147194
申请日：1980-05-06
申请人： Tomiya Isshiki , Tetsuo Tomita , Shuzabu Sakaguchi , Toshiaki Kohzaki , Osamu Aoki , Norio Takeda , Yoshiyuki Aoki
发明人： Tomiya Isshiki , Tetsuo Tomita , Shuzabu Sakaguchi , Toshiaki Kohzaki , Osamu Aoki , Norio Takeda , Yoshiyuki Aoki
IPC分类号： C07C255/67 , C07C109/16
CPC分类号： C07C251/88
摘要： A process for producing a benzophenone-azine which comprises reacting the corresponding benzophenone-imine with molecular oxygen or benzophenone with ammonia and molecular oxygen in the presence of a catalyst selected from the group consisting of metals, metal oxides and alloys of two or more metals, particularly copper or copper alloy-containing catalyst, is disclosed.
摘要翻译：一种二苯甲酮 - 吖嗪的制备方法，其包括使相应的二苯甲酮 - 亚胺与分子氧或二苯甲酮与氨和分子氧在选自金属，金属氧化物和两种或更多种金属的合金的催化剂存在下反应，特别是含铜或含铜合金的催化剂。

2. 发明授权

US3857887A 5-substituted benzophenone hydrazone compounds 失效
标题翻译： 5-取代苯并噻吩氢化合物
公开(公告)号：US3857887A
公开(公告)日：1974-12-31
申请号：US37366073
申请日：1973-06-26
申请人： CHUGAI PHARMACEUTICAL CO LTD
发明人： SHINDO M , KAKIMOTO M , NAGANO H
IPC分类号： C07C109/16
CPC分类号： C07C251/72
摘要： 5-Substituted benzophenone hydrazones which possess an activity on the central nervous system are disclosed. The 5-substituted benzophenone hydrazones are prepared by the reaction of 5substituted benzophenones with hydrazine.
摘要翻译：公开了在中枢神经系统上具有活性的5-取代的二苯甲酮腙。 5-取代的二苯甲酮腙通过5-取代的二苯甲酮与肼的反应制备。

3. 发明授权

US4727190A Process for preparing benzophenone-azines 失效
标题翻译：制备二苯甲酮吖嗪的方法
公开(公告)号：US4727190A
公开(公告)日：1988-02-23
申请号：US918656
申请日：1986-10-14
申请人： Takanari Nawata , Shuzabu Sakaguchi , Toshiaki Kohzaki , Osamu Aoki , Norio Takeda , Yoshiyuki Aoki , Masafumi Shimpo
发明人： Takanari Nawata , Shuzabu Sakaguchi , Toshiaki Kohzaki , Osamu Aoki , Norio Takeda , Yoshiyuki Aoki , Masafumi Shimpo
IPC分类号： C09B17/00 , B01J27/122 , C01B21/16 , C07B61/00 , C07C249/16 , C07C251/88 , C07C109/16
CPC分类号： C07C251/88 , C01B21/16
摘要： A process for continuously preparing benzophenone-azines comprising oxidizing benzophenone-imines with molecular oxygen or a molecular oxygen-containing gas in the presence of a copper halide catalyst is disclosed. The oxidation reaction is carried out in a multistage system under an oxygen partial pressure gradually decreasing from the former stage to the latter stage and at a conversion gradually decreasing from the former stage to the latter stage, while controlling the conversion so that the molar ratio of the benzophenone-imines to the copper halide in the final stage be maintained at 1 or more. By the process, the continuous reaction can stably be performed at a high conversion of the benzophenone-imines without involving insolubilization and sedimentation of the catalyst.
摘要翻译：公开了一种连续制备二苯甲酮吖嗪的方法，包括在卤化铜催化剂存在下用分子氧或含分子氧气体氧化二苯甲酮 - 亚胺。氧化反应在多级体系中，在从前一阶段到后一阶段逐渐降低的氧分压下进行，并且转化率从前一阶段逐渐降低到后一阶段，同时控制转化率，使得在最后阶段将二苯甲酮 - 亚胺与卤化铜保持在1以上。通过该方法，连续反应可以稳定地在二苯甲酮 - 亚胺的高转化率下进行，而不会引起催化剂的不溶解和沉淀。

4. 发明授权

US4355177A Substituted 11-amino-undeca-4,8-dienal and 11-amino-undecanal derivatives and processes for their preparation 失效
标题翻译：取代的11-氨基 - 十一烷-4,8-二烯酸和11-氨基 - 十一烷醛衍生物及其制备方法
公开(公告)号：US4355177A
公开(公告)日：1982-10-19
申请号：US230081
申请日：1981-01-30
申请人： Dieter Reinehr , Josef Pfeifer
发明人： Dieter Reinehr , Josef Pfeifer
IPC分类号： C08G59/00 , C07C67/00 , C07C209/00 , C07C209/40 , C07C209/42 , C07C209/52 , C07C209/62 , C07C211/09 , C07C211/17 , C07C211/25 , C07C211/27 , C07C211/29 , C07C239/00 , C07C241/00 , C07C251/04 , C07C251/16 , C07C251/34 , C07C251/52 , C07C251/78 , C07C251/80 , C07C251/82 , C07C281/06 , C07C281/08 , C07D225/00 , C07D225/02 , C07D225/04 , C07D307/52 , C07D333/06 , C07D333/20 , C08G59/50 , C08G69/26 , C07C109/16 , C07C119/08 , C07C119/10 , C07C133/02
CPC分类号： C07C251/72 , C07D225/00 , C07D225/02 , C07D225/04 , C07D307/52 , C07D333/20 , C08G59/50 , C08G69/26
摘要： Novel substituted 11-amino-undeca-4,8-dienal and 11-amino-undecanal aldehyde-derivatives of the formulae Ia ##STR1## in which R.sub.1 to R.sub.6, Y and m are as defined in patent claim 1, and processes for their preparation are described. The compounds of the formulae Ia and Ib can be catalytically hydrogenated to novel 1,11-diaminoundecanes, which, in turn, can be used, for example, for the preparation of polycondensation products, in particular transparent polyamides, or as curing agents for epoxide resins.
摘要翻译：式Ia（Ia）或Ib（Ib）+ TR 的新型取代的11-氨基 - 十一烷-4,8-二烯酸和11-氨基 - 十一醛醛衍生物，其中R 1至R 6 ，Y和m如专利权利要求1中所定义，并描述了其制备方法。式Ia和Ib的化合物可以催化氢化成新的1,11-二氨基十一烷，其又可用于例如缩聚产物，特别是透明聚酰胺的制备，或作为环氧化物的固化剂树脂。

5. 发明授权

US4258181A Substituted 9,10-anthracenebishydrazones 失效
标题翻译：取代9,10-蒽二腙
公开(公告)号：US4258181A
公开(公告)日：1981-03-24
申请号：US36924
申请日：1979-05-07
申请人： Keith C. Murdock , Frederick E. Durr
发明人： Keith C. Murdock , Frederick E. Durr
IPC分类号： C07C281/14 , A61K31/15 , A61K31/17 , A61K31/415 , A61K31/505 , A61K31/54 , A61P35/00 , C07C15/28 , C07C17/32 , C07C47/453 , C07C47/457 , C07C47/47 , C07C47/55 , C07C47/57 , C07C47/575 , C07C67/00 , C07C239/00 , C07C241/00 , C07C251/80 , C07C251/86 , C07C281/18 , C07C325/00 , C07C337/08 , C07D213/42 , C07D213/77 , C07D233/52 , C07D233/88 , C07D239/18 , C07D239/42 , C07D243/04 , C07D295/12 , C07D295/13 , C07D307/52 , C07D317/70 , C07D333/20 , C07C109/16
CPC分类号： C07D295/13 , C07C17/32 , C07C251/72 , C07C281/18 , C07C47/453 , C07C47/457 , C07C47/47 , C07C47/55 , C07C47/57 , C07C47/575 , C07D213/42 , C07D213/77 , C07D233/52 , C07D239/18 , C07D243/04 , C07D307/52 , C07D317/70 , C07D333/20 , C07C2103/24
摘要： This disclosure describes anthracene-9,10-bis-carbonyl-hydrazones and derivatives thereof useful as antibacterial agents, for inhibiting the growth of transplanted mouse tumors, and for inducing the regression and/or palliation of leukemia and related cancers.
摘要翻译：本公开描述了用作抑制移植的小鼠肿瘤生长以及用于诱导白血病和相关癌症的消退和/或缓解的蒽-9,10-双羰基 - 腙及其衍生物。

6. 发明授权

US4277621A Substituted 11-amino-undeca-4,8-dienal and 11-amino-undecanal derivatives and processes for their preparation 失效
标题翻译：取代的11-氨基 - 十一烷-4,8-二烯酸和11-氨基 - 十一烷醛衍生物及其制备方法
公开(公告)号：US4277621A
公开(公告)日：1981-07-07
申请号：US83140
申请日：1979-10-09
申请人： Dieter Reinehr , Josef Pfeifer
发明人： Dieter Reinehr , Josef Pfeifer
IPC分类号： C08G59/00 , C07C67/00 , C07C209/00 , C07C209/40 , C07C209/42 , C07C209/52 , C07C209/62 , C07C211/09 , C07C211/17 , C07C211/25 , C07C211/27 , C07C211/29 , C07C239/00 , C07C241/00 , C07C251/04 , C07C251/16 , C07C251/34 , C07C251/52 , C07C251/78 , C07C251/80 , C07C251/82 , C07C281/06 , C07C281/08 , C07D225/00 , C07D225/02 , C07D225/04 , C07D307/52 , C07D333/06 , C07D333/20 , C08G59/50 , C08G69/26 , C07C109/14 , C07C109/16 , C07C131/00
CPC分类号： C07C251/72 , C07D225/00 , C07D225/02 , C07D225/04 , C07D307/52 , C07D333/20 , C08G59/50 , C08G69/26
摘要： Novel substituted 11-amino-undeca-4,8-dienal and 11-amino-undecanal aldehyde-derivatives of the formulae Ia ##STR1## in which R.sub.1 to R.sub.6, Y and m are as defined in patent claim 1, and processes for their preparation are described. The compounds of the formulae Ia and Ib can be catalytically hydrogenated to novel 1,11-diaminoundecanes, which, in turn, can be used, for example, for the preparation of polycondensation products, in particular transparent polyamides, or as curing agents for epoxide resins.
摘要翻译：（Ia）或Ib（VI）的新型取代的11-氨基 - 十一碳-4,8-二烯酸和11-氨基 - 十一醛醛衍生物，其中R 1至R 6，Y 和m如专利权利要求1中所定义，并描述了其制备方法。式Ia和Ib的化合物可以催化氢化成新的1,11-二氨基十一烷，其又可用于例如缩聚产物，特别是透明聚酰胺的制备，或作为环氧化物的固化剂树脂。

7. 发明授权

US4017540A Method of use, composition, and compounds 失效
标题翻译：使用方法，组合物和化合物
公开(公告)号：US4017540A
公开(公告)日：1977-04-12
申请号：US228359
申请日：1972-02-22
申请人： Girts Kaugars , Edwin G. Gemrich, II
发明人： Girts Kaugars , Edwin G. Gemrich, II
IPC分类号： C07C109/16
摘要： Certain benzoyl chloride phenylhydrazones have been found to be active against insects and mites. The benzoyl ring and the phenylhydrazone ring can be substituted with a halogen atom, a nitro group, or an alkyl group of from 1 to 6 carbon atoms, inclusive. A new class of pentahalobenzoyl chloride phenylhydrazones is described, particularly pentafluorobenzoyl chloride phenylhydrazones. A further new class of alkylbenzoyl chloride phenylhydrazones, particularly p-toluoyl chloride phenylhydrazones are also described. The compounds are prepared by reacting a benzoic acid phenylhydrazide with phosphorus pentachloride to obtain a benzoyl chloride (dichlorophosphinyl)phenylhydrazone that is reacted with phenol to produce the desired benzoyl chloride phenylhydrazones. Certain of the compounds can be prepared by direct chlorination of a benzaldehyde phenylhydrazone. Methods of use and compositions are described.
摘要翻译：已经发现某些苯甲酰氯苯腙对昆虫和螨具有活性。苯甲酰基环和苯腙环可以被卤素原子，硝基或含1-6个碳原子的烷基取代。描述了一类新的五卤苯甲酰氯苯腙，特别是五氟苯甲酰氯苯腙。还描述了另一类新的烷基苯甲酰氯苯腙，特别是对甲苯酰氯苯腙。通过苯甲酸苯肼与五氯化磷反应制得化合物，得到与苯酚反应产生所需苯甲酰氯苯腙的苯甲酰氯（二氯膦氧基）苯腙。某些化合物可以通过苯甲醛苯腙的直接氯化来制备。描述使用方法和组合物。

8. 发明授权

US3796754A 5-substituted benzophenone hydrazone compounds and process for the production thereof 失效
标题翻译： 5-取代苯并噻吩氢化合物及其生产方法
公开(公告)号：US3796754A
公开(公告)日：1974-03-12
申请号：US3796754D
申请日：1972-04-10
申请人： CHUGAI PHARMACEUTICAL CO LTD
发明人： SHINDO M , KAKIMOTO M , NAGANO H
IPC分类号： A61K31/15 , C07C109/16
CPC分类号： C07C251/72
摘要： 5-SUBSTITUTED BENZOPHENONE HYDRAZONES WHICH POSSESS AN ACTIVITY ON THE CENTRAL NERVOUS SYSTEM ARE DISCLOSED. THE 5-SUBSTITUTED BENZOPHENONE HYDRAZONES ARE PREPARED BY THE REACTION OF 5-SUBSTITUTED BENZOPHENONES WITH HYDRAZINE.

9. 发明授权

US4473708A Preparation of ketozines using organoarsenic compounds 失效
标题翻译：用有机砷化合物制备酮基
公开(公告)号：US4473708A
公开(公告)日：1984-09-25
申请号：US396572
申请日：1982-07-09
申请人： Yasuhisa Kuriyama , Minoru Kakuda , Shoichi Nitoh
发明人： Yasuhisa Kuriyama , Minoru Kakuda , Shoichi Nitoh
IPC分类号： C07B61/00 , B01J23/00 , B01J23/18 , B01J31/00 , B01J31/12 , C07C67/00 , C07C241/00 , C07C251/88 , C07C109/12 , C07C109/14 , C07C109/16 , C07C119/00
CPC分类号： C07C251/88
摘要： A process for preparing a ketazine useful as an intermediate for the synthesis of hydrazine is disclosed. The process comprises reacting an aliphatic or aromatic ketone with ammonia and hydrogen peroxide in the presence of a catalyst of an arsenic compound to produce a corresponding ketazine.
摘要翻译：公开了一种制备可用作肼合成中间体的酮连氮的方法。该方法包括在砷化合物的催化剂存在下使脂族或芳族酮与氨和过氧化氢反应以产生相应的酮连氮。

10. 发明授权

US4233242A Process for producing ketazine by reacting a ketone with ammonia and a peroxide 失效
标题翻译：通过使酮与氨和过氧化物反应制备酮连氮的方法
公开(公告)号：US4233242A
公开(公告)日：1980-11-11
申请号：US27895
申请日：1979-04-06
申请人： Nobuyuki Nagato , Yuichi Sugiyama
发明人： Nobuyuki Nagato , Yuichi Sugiyama
IPC分类号： C07C109/12 , C07C109/14 , C07C109/16 , C07C119/00
CPC分类号： C07C251/88
摘要： Ketazines having the general formula (I) ##STR1## wherein R.sub.1 represents alkyl group having 1 to 4 carbon atoms and R.sub.2 represents (i) an alkyl group having 1 to 4 carbon atoms or (ii) a phenyl group optionally substituted with an alkyl group having 1 to 4 carbon atoms, an alkoxy group having 1 to 4 carbon atoms or a halogen group, and R.sub.1 and R.sub.2 together with the carbon atom to which they are both bonded may form a ring, are advantageously manufactured by reacting an aliphatic or aromatic ketone having the formula (II) ##STR2## wherein R.sub.1 and R.sub.2 are as defined above, with ammonia and a peroxide compound or compounds in the presence of amorphous silica or palladium compounds, as a catalyst, at a temperature of from 0.degree. to 120.degree. C., in a liquid phase.
摘要翻译：具有通式（I）的化合物其中R 1表示具有1至4个碳原子的烷基，R 2表示（i）具有1至4个碳原子的烷基或（ii）任选被具有1至4个碳原子的烷基，具有1至4个碳原子的烷氧基或卤素基团，并且R 1和R 2与它们所连接的碳原子一起形成环可有利地通过使在无定形二氧化硅或钯化合物作为催化剂存在下，在氨气和过氧化物或化合物作为催化剂的情况下，具有式（II）的脂族或芳族酮（II）其中R 1和R 2如上定义，为0〜120℃，为液相。

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