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1. 发明授权

US06461989B1 Process for forming 312 phase materials and process for sintering the same 有权
标题翻译：形成312相材料的工艺及其烧结工艺
公开(公告)号：US06461989B1
公开(公告)日：2002-10-08
申请号：US09469893
申请日：1999-12-22
申请人： Tamer El-Raghy , Michel W. Barsoum , Mats Sundberg , Hans Pettersson
发明人： Tamer El-Raghy , Michel W. Barsoum , Mats Sundberg , Hans Pettersson
IPC分类号： C04B3556
CPC分类号： C04B35/5615 , C04B35/56 , C04B35/573 , C04B35/58 , C04B35/5805 , C04B35/6365 , C04B35/64
摘要： A process is provided for forming a material comprising an M3X1Z2 phase comprising the steps of: (a) providing a mixture of (i) at least one transition metal species, (ii) at least one co-metal species selected from the group consisting of aluminum species, germanium species and silicon species, and (iii) at least one non-metal species selected from the group consisting of boron species, carbon species and nitrogen species; (b) heating said mixture to a temperature of about 1000° C. to about 1800° C., in an atmosphere within a substantially enclosed heating zone, for a time sufficient to form said M3X1Z2 phase; wherein the atmosphere has an O2 partial pressure of no greater than about 1×10−6 atm. The process provides a substantially single phase material comprising very little MZx-phase. A process for preparing a dense, substantially single-phase M3X1Z2 phase workpiece includes providing a highly-pure M3X1Z2-phase powder pre-form and sintering said pre-form at a temperature of about 1000° C. to about 1800° C., in an atmosphere within a substantially enclosed heating zone, for a time sufficient to form a dense, substantially single-phase, M3X1Z2-phase workpiece; wherein the atmosphere has an O2 partial pressure of no greater than about 1×10−6 atm.
摘要翻译：提供了一种用于形成包含M3X1Z2相的材料的方法，包括以下步骤：（a）提供（i）至少一种过渡金属物质，（ii）至少一种选自以下的共金属物质的混合物：铝物种，锗物质和硅物质，和（iii）至少一种选自硼物质，碳物质和氮物质的非金属物质; （b）在基本封闭的加热区内的气氛中将所述混合物加热到约1000℃至约1800℃的温度，持续足以形成所述M3X1Z2相的时间; 其中气氛的O 2分压不大于约1×10 -6 atm。该方法提供了包含很少的MZx相的基本单相材料。制备致密的，基本上单相的M3X1Z2相工件的方法包括提供高纯度的M3X1Z2相粉末预成型体，并在约1000℃至约1800℃的温度下烧结所述预成型体，在基本封闭的加热区内的气氛足以形成致密的，基本上单相的M3X1Z2相工件的时间; 其中气氛的O 2分压不大于约1×10 -6 atm。

2. 发明授权

US06277774B1 Grain growth inhibitor for superfine materials 失效
标题翻译：超细材料颗粒生长抑制剂
公开(公告)号：US06277774B1
公开(公告)日：2001-08-21
申请号：US09138137
申请日：1998-08-21
申请人： Danny T. Xiao , Chris W. Strock , Donald M. Wang , Peter R. Strutt
发明人： Danny T. Xiao , Chris W. Strock , Donald M. Wang , Peter R. Strutt
IPC分类号： C04B3556
CPC分类号： C04B35/583 , B22F1/0018 , B22F1/0044 , B22F1/02 , B22F2003/1032 , B22F2009/041 , B22F2998/00 , B22F2998/10 , B82Y30/00 , C01B21/064 , C01P2004/61 , C01P2004/62 , C01P2004/64 , C04B35/56 , C04B35/5607 , C04B35/5611 , C04B35/565 , C04B35/58 , C04B35/58014 , C04B35/58071 , C04B35/58092 , C04B35/581 , C22C1/051 , C22C1/053 , C22C29/08 , Y10S977/844 , Y10S977/896 , Y10S977/897 , Y10S977/90 , B22F9/20 , B22F9/24 , B22F1/0085 , B22F1/0088 , B22F9/026 , B22F9/04 , B22F1/0074
摘要： A method comprising incorporation of an inorganic polymer precursor of a grain growth inhibitor into superfine materials or intermediates useful for the production of superfine materials. The precursor/nanostructured material composite is optionally heat treated at a temperature below the grain growth temperature of the superfine material in order to more effectively disperse the precursor. The composites are then heat treated at a temperature effective to decompose the precursor and to form superfine materials having grain growth inhibitors uniformly distributed at the grain boundaries. Synthesis of the inorganic polymer solution comprises forming an inorganic polymer from a solution of metal salts, filtering the polymer, and drying. Alloying additives as well as grain growth inhibitors may be incorporated into the superfine materials.
摘要翻译：一种方法，包括将晶粒生长抑制剂的无机聚合物前体引入用于生产超细材料的超细材料或中间体中。前体/纳米结构材料复合物任选在低于超细材料的晶粒生长温度的温度下热处理，以便更有效地分散前体。然后在有效分解前体的温度下对复合材料进行热处理，并形成具有均匀分布在晶界处的晶粒生长抑制剂的超细材料。无机聚合物溶液的合成包括由金属盐溶液形成无机聚合物，过滤聚合物并干燥。合金添加剂以及晶粒生长抑制剂可以并入超细材料中。

3. 发明授权

US06231791B1 Silicon carbide articles reinforced with short graphite fibers 有权
标题翻译：用短石墨纤维增强的碳化硅制品
公开(公告)号：US06231791B1
公开(公告)日：2001-05-15
申请号：US09291962
申请日：1999-04-15
申请人： Michael Heine , Udo Gruber
发明人： Michael Heine , Udo Gruber
IPC分类号： C04B3556
CPC分类号： F16D69/023 , C04B35/573 , C04B35/806 , F16D2200/0047
摘要： A composite material article reinforced with high strength short graphite fibers and having a matrix substantially consisting of silicon carbide is prepared which has an elongation at break of 0.25 to 0.5% and thus exhibits quasi-ductile failure behavior. The short reinforcing graphite fibers are enclosed by at least two shells of graphitized carbon which have been obtained by impregnation with carbonizable impregnating agents and subsequent carbonization. The shell closest to the graphite fibers contains no cracks. The outermost shell is partially converted into silicon carbide. The starting material used comprises long or short fiber prepregs, which are first carbonized, then subjected at least once to an operation consisting of impregnation with a carbonizable impregnating agent and recarbonization, then graphitized at a temperature of up to a maximum of 2400° C. and then comminuted to yield a dry material for the production of a precursor article. This dry material is then mixed with a binder having a high carbon content and the mixture is compression molded to yield a green article. The green molding is then carbonized and afterwards infiltrated with liquid silicon, with the carbon matrix of the carbonized precursor article being converted into silicon carbide.
摘要翻译：制备用高强度短石墨纤维增强并具有基本上由碳化硅组成的基体的复合材料制品，其具有0.25至0.5％的断裂伸长率，因此显示出准韧性破坏行为。短的增强石墨纤维被至少两个石墨化碳壳包围，这些石墨化碳通过用可碳化浸渍剂浸渍并随后进行碳化而获得。最靠近石墨纤维的壳体不含裂纹。最外壳被部分转化为碳化硅。使用的起始原料包括长纤维或短纤维预浸料，其首先被碳化，然后至少进行一次操作，其中包括用可碳化浸渍剂的浸渍和再碳化，然后在最高达2400℃的温度下石墨化。然后粉碎以产生用于制备前体制品的干燥材料。然后将该干燥材料与具有高碳含量的粘合剂混合，并将该混合物压塑以产生绿色制品。然后将绿色模制品碳化，然后用液态硅渗透，碳化前体制品的碳基体转化为碳化硅。

4. 发明授权

US06187123B1 Method for producing a lightened SiC sandwich type structure with a honeycomb-shaped core and structure obtained by said method 失效
标题翻译：用于制造具有蜂窝状芯的减轻的SiC夹层结构的方法和通过所述方法获得的结构
公开(公告)号：US06187123B1
公开(公告)日：2001-02-13
申请号：US09176915
申请日：1998-10-22
申请人： Jean-Pascal Chenier , Gérard Rousseau , Frédéric Boursereau
发明人： Jean-Pascal Chenier , Gérard Rousseau , Frédéric Boursereau
IPC分类号： C04B3556
CPC分类号： B32B3/12 , B32B9/005 , B32B9/047 , B32B18/00 , B32B2305/024 , C04B35/632 , C04B35/634 , C04B35/63476 , C04B38/0006 , C04B38/0022 , C04B41/009 , C04B41/5059 , C04B2111/00612 , C04B2235/656 , C04B2237/363 , C04B2237/365 , C04B2237/38 , C04B2237/704 , G02B5/08 , G02B7/183 , C04B35/565 , C04B41/4531 , C04B35/52 , C04B41/4556
摘要： The present invention concerns a method for producing a lightened SiC structure, especially for the production of a lightened mirror, with the following stages: cutting of a preform with a honeycomb-shaped structure whose voiles have an organic matrix and a fibrous reinforcement, pyrolysis of this honeycomb-shaped structural preform so as to solely preserve the carbon, silicidation of the carbon of the preform so as to obtain a microporous SiC core, infiltrating type reinforcement by means of a SiC chemical vapor phase depositing of the voiles of the honeycomb structure of the core, embodiment of a felt sheet and assembling on at least one face of the core of the embodied sheet and densification of this sheet so as to obtain at least one SiC skin on the surface of the core. The invention also concerns the structure obtained.
摘要翻译：本发明涉及一种用于制造减轻SiC结构的方法，特别是用于生产减光镜的方法，具有以下阶段：用具有有机基体和纤维增强物的蜂窝状结构切割预成型体，热解该蜂窝状结构预成型件仅仅保留预成型体的碳的碳化硅化物，从而获得微孔SiC芯，通过SiC化学气相沉积蜂窝状结构体的蜂窝结构体芯片，毡片的实施例，并且在所实施的片材的芯部的至少一个表面上的组装和该片材的致密化，以便在芯部的表面上获得至少一个SiC表面。本发明还涉及获得的结构。

5. 发明授权

US06248681B1 Ceramic cutting tool 有权
标题翻译：陶瓷切割工具
公开(公告)号：US06248681B1
公开(公告)日：2001-06-19
申请号：US09220752
申请日：1998-12-28
申请人： Hideki Kato
发明人： Hideki Kato
IPC分类号： C04B3556
CPC分类号： C04B35/645 , B23B27/148 , C04B35/5611 , C04B35/5626 , C04B35/58021 , C04B35/6455
摘要： Disclosed is a ceramic cutting tool comprising in its essential part a ceramic material comprising, in one aspect, a titanium carbonitride-based hard phase and an alumina-based phase, wherein the ceramic material satisfies the following relationships: 10 wt %≦weight of Al2O3≦45 wt %; 51 wt %≦weight of TiCN≦89.5 wt %; and 96 wt %≦weight of Al2O3+weight of TiCN≦99.5 wt % wherein the weight of Al2O3 indicates the weight content of aluminum as calculated in terms of Al2O3; and the weight of TiCN indicates the weight content of said titanium carbonitride hard phase,with the proviso that the weight of TiCN is defined by the weight of Ti+ the weight of C+ the weight of N, in which weight of Ti, C, and N are the weight contents of the titanium component, carbon component, and nitrogen component, respectively.
摘要翻译：公开了一种陶瓷切削工具，其主要部分包括陶瓷材料，其一方面包括基于碳氮化钛的硬质相和氧化铝基相，其中所述陶瓷材料满足以下关系：其中Al 2 O 3的重量表示以Al2O3计算的铝的重量含量; TiCN的重量表示碳氮化钛硬质合金的重量含量，条件是TiCN的重量由Ti +的重量定义，C +的重量为N的重量，其中Ti，C和N的重量分别为钛成分，碳成分和氮成分的重量含量。

6. 发明授权

US06225247B1 Polymer precursor composition, crosslinked polymers, thermosets and ceramics made with silyl and siloxyl substituted carboranes with unsaturated organic end groups 失效
标题翻译：聚合物前体组合物，交联聚合物，热固性材料和由具有不饱和有机端基的甲硅烷基和甲硅烷基取代的碳硼烷制成的陶瓷
公开(公告)号：US06225247B1
公开(公告)日：2001-05-01
申请号：US09336728
申请日：1999-06-21
申请人： Teddy M. Keller , Eric J. Houser
发明人： Teddy M. Keller , Eric J. Houser
IPC分类号： C04B3556
CPC分类号： C08L83/14 , C08G77/56
摘要： A precursor composition includes (1) at least one crosslinking compound represented by the formula: wherein: u and x are independently selected positive integers, v and w are independently selected integers greater than or equal to zero, R1, R2, R3, R4, R5, R6, R7 and R8 are independently selected from the group consisting of alkyl, aryl, alkylaryl, haloalkyl, haloaryl and mixtures thereof; A and E are independently selected from the group consisting of O, an aliphatic bridge, an aryl bridge and mixtures thereof; and R9 and R10 are unsubstituted or substituted vinyl or ethynyl groups, (2) at least one organosilicon compound containing at least two silicon hydride moieties per molecule, and (3) a hydrosilation catalyst, A cross-linked polymer is formed by reacting the crosslinking compound of formula I with the organosilicon compound via a hydrosilation reaction. A thermoset polymer is formed by thermally curing the crosslinked polymer. A boron-carbon-silicon ceramic formed by pyrolyzing the cross-linked polymer.
摘要翻译：前体组合物包括（1）至少一种由下式表示的交联化合物：其中：u和x独立选择正整数，v和w独立地选自大于或等于零的整数，R 1，R 2，R 3，R 4， R5，R6，R7和R8独立地选自烷基，芳基，烷基芳基，卤代烷基，卤代芳基及其混合物; A和E独立地选自O，脂族桥，芳基桥及其混合物; 并且R 9和R 10是未取代的或取代的乙烯基或乙炔基，（2）每分子含有至少两个氢化硅部分的至少一种有机硅化合物，和（3）硅氢化催化剂。交联聚合物通过使交联式I化合物与有机硅化合物通过硅氢化反应。通过热固化交联聚合物形成热固性聚合物。通过热解交联聚合物形成的硼 - 碳 - 硅陶瓷。

7. 发明授权

US06221479B1 Cemented carbide insert for turning, milling and drilling 有权
标题翻译：用于车削，铣削和钻孔的硬质合金刀片
公开(公告)号：US06221479B1
公开(公告)日：2001-04-24
申请号：US09214923
申请日：1999-04-20
申请人： Mats Waldenström , Åke Östlund , Ove Alm
发明人： Mats Waldenström , Åke Östlund , Ove Alm
IPC分类号： C04B3556
CPC分类号： C23C30/005 , B22F1/0003 , B22F1/0081 , B22F2998/00 , C22C1/051 , C22C29/08 , Y10T428/25 , Y10T428/252 , B22F9/026
摘要： There is disclosed a cemented carbide insert with excellent properties for machining of steels and stainless steels. The cemented carbide comprises WC and 4-25 wt-% Co. The WC-grains have an average grain size in the range 0.2-3.5 &mgr;m and a narrow grain size distribution in the range 0-4.5 &mgr;m. According to the method of the invention a cemented carbide cutting tool insert is made by mixing powders of WC, TiC, TaC and/or NbC, binder metal and pressing agent, drying preferably by spray drying, pressing to inserts and sintering. The method characterised in that a deagglomerated WC-powder with a narrow grain size distribution is used, that the powders of TiC, TaC and/or NbC are deagglomerated and that the mixing is wet mixing with no change in grain size or grain size distribution.
摘要翻译：公开了一种用于钢和不锈钢加工的优异性能的硬质合金刀片。硬质合金包括WC和4-25wt％的Co。WC-晶粒的平均晶粒尺寸在0.2-3.5μm的范围内，并且窄的粒度分布在0-4.5μm的范围内。根据通过混合WC，TiC，TaC和/或NbC，粘合剂金属和压制剂的粉末，优选通过喷雾干燥，压制成型和烧结来制备硬质合金刀具刀片。该方法的特征在于使用具有窄粒度分布的解团聚WC粉末，其中TiC，TaC和/或NbC的粉末被解团聚，并且混合是湿混合而不改变晶粒尺寸或晶粒尺寸分布。

8. 发明授权

US06660673B1 Use of particulate materials containing TiO2 in refractory products 有权
$Use of particulate materials containing TiO2 in refractory products$
标题翻译：在耐火产品中使用含有TiO2的颗粒材料
公开(公告)号：US06660673B1
公开(公告)日：2003-12-09
申请号：US09624571
申请日：2000-07-24
申请人： Djamschid Amirzadeh-Asl , Dieter Fünders
发明人： Djamschid Amirzadeh-Asl , Dieter Fünders
IPC分类号： C04B3556
CPC分类号： C09K21/02 , C04B35/66
摘要： In order to reduce wear on refractory linings due to corrosion and the infiltration of slags and molten metals, particulate materials containing TiO2 are added to the refractory products consisting of a mixture of aggregates and binding agents.
摘要翻译：为了减少由于腐蚀和炉渣和熔融金属的渗透引起的耐火材料衬里的磨损，将含有TiO 2的颗粒材料加入到由聚集体和粘合剂的混合物组成的耐火产品中。

9. 发明授权

US06617271B1 Tungsten carbide cutting tool materials 失效
标题翻译：碳化钨切削刀具材料
公开(公告)号：US06617271B1
公开(公告)日：2003-09-09
申请号：US10100488
申请日：2002-03-19
申请人： Vladimir Yurievich Kodash , Edwin Spartakovich Gevorkian
发明人： Vladimir Yurievich Kodash , Edwin Spartakovich Gevorkian
IPC分类号： C04B3556
CPC分类号： C04B35/645 , B23B27/148 , B23B2222/28 , B82Y30/00 , C04B35/5626 , C04B35/62655 , C04B35/6303 , C04B35/64 , C04B2235/3839 , C04B2235/3847 , C04B2235/3895 , C04B2235/5409 , C04B2235/5454 , C04B2235/6581 , C04B2235/6582 , C04B2235/6584 , C04B2235/666 , C04B2235/667 , C04B2235/72 , C04B2235/723 , C04B2235/725 , C04B2235/77 , C04B2235/784 , C04B2235/785 , C04B2235/786 , C04B2235/80 , C04B2235/96 , Y10T407/27
摘要： The disclosed invention describes a new high-performance binderless high purity tungsten carbide material, its manufacturing and applications as a cutting tool material.
摘要翻译：所公开的发明描述了一种新的高性能无粘合剂高纯度碳化钨材料，其制造和应用作为切削工具材料。

10. 发明授权

US06551954B1 WC-base composite ceramic sintered compact 失效
标题翻译： WC基复合陶瓷烧结体
公开(公告)号：US06551954B1
公开(公告)日：2003-04-22
申请号：US09869241
申请日：2001-07-18
申请人： Mitsuyoshi Nagano , Shigeya Sakaguchi , Norimitsu Mukae , Kouki Minamoto , Toyoshige Sasaki
发明人： Mitsuyoshi Nagano , Shigeya Sakaguchi , Norimitsu Mukae , Kouki Minamoto , Toyoshige Sasaki
IPC分类号： C04B3556
CPC分类号： C04B35/645 , C04B35/5603 , C04B35/5626 , C04B35/6455 , Y10T407/27
摘要： A WC-based composite ceramics sintered body consisting of 40 volume % to 90 volume % of WC including solid-solved oxygen represented by a chemical formula of WCxOy (where 0.005
摘要翻译： WC系复合陶瓷烧结体，其组成为40体积％〜90体积％的WC，其包含以化学式WCxOy表示的固溶氧（其中0.005

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