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1. 发明授权

US07708805B2 Method of producing carbon fibers, and methods of making protective clothing and a filter module 失效
标题翻译：生产碳纤维的方法，以及制作防护服的方法和过滤器模块
公开(公告)号：US07708805B2
公开(公告)日：2010-05-04
申请号：US11656259
申请日：2007-01-22
申请人： Michael Heine , Richard Neuert , Rainer Zimmermann-Chopin
发明人： Michael Heine , Richard Neuert , Rainer Zimmermann-Chopin
IPC分类号： D01F9/12
CPC分类号： D01F9/22
摘要： Porous carbon fibers, whose active centers are formed by pores that are filled at least in part by carbon and/or metal and/or metal carbide, obtainable by carbonization of organic or inorganic polymers, the use thereof for the adsorption or separation of gaseous substances, in particular of CO2, and also a method for the production thereof. First, a spinning mixture containing polyacrylonitrile-based polymer A and an organic or metallo-organic polymer B is produced. Next, the spinning mixture is spun to form mixed fibers of polymer A and polymer B. The mixed fiber is stabilized by oxidation. This is followed by carbonization or graphitization of the mixed fiber under non-oxidizing conditions in such a way that the polymer B forms a carbon and/or metal and/or metal carbide residue of at least 22 wt %, the residue forming active centers.
摘要翻译：多孔碳纤维，其活性中心由至少部分由碳和/或金属和/或金属碳化物填充的孔形成，可通过有机或无机聚合物的碳化获得，其用于吸附或分离气态物质，特别是二氧化碳，以及其制备方法。首先，制备含有聚丙烯腈类聚合物A和有机或金属有机聚合物B的纺丝混合物。接下来，将纺丝混合物纺丝以形成聚合物A和聚合物B的混合纤维。混合纤维通过氧化而稳定。接着在非氧化条件下使混合纤维碳化或石墨化，使得聚合物B形成至少22重量％的碳和/或金属和/或金属碳化物残余物，残余物形成活性中心。

2. 发明授权

US07309609B2 Detection of oxidation of carbon-containing fibers or fiber bundles in composites 有权
标题翻译：检测复合材料中含碳纤维或纤维束的氧化
公开(公告)号：US07309609B2
公开(公告)日：2007-12-18
申请号：US10624697
申请日：2003-07-22
申请人： Martin Christ , Michael Heine
发明人： Martin Christ , Michael Heine
IPC分类号： G01N25/18 , G01N27/00 , G01R31/26 , G01R31/28 , H01L23/58 , H01L29/10
CPC分类号： C04B35/83 , C04B35/565 , C04B35/573 , C04B2235/404 , C04B2235/405 , C04B2235/428 , C04B2235/5248 , C04B2235/526 , C04B2235/5264 , C04B2235/728 , C04B2235/80 , G01N27/9046
摘要： The invention relates to the detection of oxidation of carbon-containing fibers or fiber bundles embedded in a nonconductive or semiconducting ceramic matrix in composites wherein use is made of the eddy current method.
摘要翻译：本发明涉及检测复合材料中嵌入非导电或半导体陶瓷基体中的含碳纤维或纤维束的氧化，其中使用涡流法。

3. 发明授权

US07011785B2 Process for producing hollow bodies comprising fiber-reinforced ceramic materials 有权
公开(公告)号：US07011785B2
公开(公告)日：2006-03-14
申请号：US10328413
申请日：2002-12-23
申请人： Moritz Bauer , Michael Heine , Andreas Kienzle , Ronald Huener , Andreas Rahn , Rainer Zimmermann-Chopin
发明人： Moritz Bauer , Michael Heine , Andreas Kienzle , Ronald Huener , Andreas Rahn , Rainer Zimmermann-Chopin
IPC分类号： B29C35/08 , B29C67/00 , B28B7/28 , C01B31/00
CPC分类号： C04B41/87 , C04B35/565 , C04B35/573 , C04B35/83 , C04B41/009 , C04B41/5059 , C04B2111/00362 , C04B2111/00982 , C04B2235/404 , C04B2235/405 , C04B2235/428 , C04B2235/48 , C04B2235/5248 , C04B2235/6028 , C04B2235/728 , C04B2235/80 , C04B2235/94 , C04B2235/96 , F16D69/023 , C04B41/4523 , C04B41/4556
摘要： Process for producing hollow bodies comprising fiber-reinforced ceramic materials, where mold cores whose shape corresponds to that of the hollow spaces are produced in a first step, at least one mold core together with a press moulding composition or formable fiber composition are introduced into a mold, where the press moulding composition comprises carbon fibers and/or carbon filaments and thermally curable carbonizable binders, in such a way that the position of the cores corresponds to the desired position of the hollow spaces to be formed in a second step, the composition is cured in a third step by heating to a temperature of from 120° C. to 280° C., to give a green body, the strengthened green body is carbonized and or graphitized in a fourth step by heating in a nonoxidizing atmosphere to a temperature of from about 750° C. to about 2400° C. to form a C/C body, wherein heating in the third and/or fourth step is at least partly effected by an electric current being passed through the pressable composition or the green body and through at least one mold core, hollow bodies produced in this way and their use for producing clutch disks or brake disks, in particular for automobiles

4. 发明授权

US06527092B2 Method for producing brake discs formed of ceramic parts with metal hubs and brake disc produced according to the method 有权
标题翻译：用于制造由具有金属毂的陶瓷部件和根据该方法制造的制动盘的制动盘的制造方法
公开(公告)号：US06527092B2
公开(公告)日：2003-03-04
申请号：US09793341
申请日：2001-02-26
申请人： Udo Gruber , Michael Heine , Andreas Kienzle
发明人： Udo Gruber , Michael Heine , Andreas Kienzle
IPC分类号： F16D6510
CPC分类号： F16D69/023 , F16D65/12 , F16D69/02 , F16D2065/132 , F16D2065/1328 , F16D2065/1344 , F16D2200/003 , F16D2200/0039 , F16D2200/0047 , F16D2250/0015 , Y10T428/30
摘要： A method for the production of brake discs having friction areas made of ceramic materials, in particular composite materials, includes placing at least one ceramic portion in a diecasting mold and joining the ceramic portion with molten metals by casting under pressure into a rotationally symmetrical body which contains at least one ceramic (composite) segment that is disposed symmetrically relative to the axis of rotation of the metal body and juts out over at least one surface of the metal body perpendicular to the axis. A brake disc produced according to the method is also provided.
摘要翻译：一种用于制造具有由陶瓷材料制成的摩擦区域，特别是复合材料的制动盘的方法，包括将至少一个陶瓷部分放置在压铸模具中，并将陶瓷部分与熔融金属通过在压力下铸造成旋转对称的主体，包含至少一个相对于金属体的旋转轴线对称设置的陶瓷（复合）部分，并且突出在垂直于该轴线的金属体的至少一个表面上。还提供了根据该方法制造的制动盘。

5. 发明授权

US06030913A Silicon carbide articles reinforced with short graphite fibers 失效
标题翻译：用短石墨纤维增强的碳化硅制品
公开(公告)号：US06030913A
公开(公告)日：2000-02-29
申请号：US26347
申请日：1998-02-19
申请人： Michael Heine , Udo Gruber
发明人： Michael Heine , Udo Gruber
IPC分类号： C04B35/565 , C04B35/573 , C04B35/65 , C04B35/80 , F16D69/02 , C04B35/56
CPC分类号： F16D69/023 , C04B35/573 , C04B35/806 , F16D2200/0047
摘要： A composite material article reinforced with high strength short graphite fibers and having a matrix substantially consisting of silicon carbide is prepared which has an elongation at break of 0.25 to 0.5% and thus exhibits quasi-ductile failure behavior. The short reinforcing graphite fibers are enclosed by at least two shells of graphitized carbon which have been obtained by impregnation with carbonizable impregnating agents and subsequent carbonization. The shell closest to the graphite fibers contains no cracks. The outermost shell is partially converted into silicon carbide. The starting material used comprises long or short fiber prepregs, which are first carbonized, then subjected at least once to an operation consisting of impregnation with a carbonizable impregnating agent and recarbonization, then graphitized at a temperature of up to maximum of 2400.degree. C. and then comminuted to yield a dry material for the production of a precursor article. This dry material is then mixed with a binder having a high carbon content and the mixture is compression molded to yield a green article. The green molding is then carbonized and afterwards infiltrated with liquid silicon, with the carbon matrix of the carbonized precursor article being converted into silicon carbide.
摘要翻译：制备用高强度短石墨纤维增强并具有基本上由碳化硅组成的基体的复合材料制品，其具有0.25至0.5％的断裂伸长率，因此显示出准韧性破坏行为。短的增强石墨纤维被至少两个石墨化碳壳包围，这些石墨化碳通过用可碳化浸渍剂浸渍并随后进行碳化而获得。最靠近石墨纤维的壳体不含裂纹。最外壳被部分转化为碳化硅。使用的起始原料包括长纤维或短纤维预浸料，其首先被碳化，然后至少进行一次操作，其中包括用可碳化浸渍剂的浸渍和再碳化，然后在最高达2400℃的温度下石墨化，然后粉碎以产生用于制备前体制品的干材料。然后将该干燥材料与具有高碳含量的粘合剂混合，并将该混合物压塑以产生绿色制品。然后将绿色模制品碳化，然后用液态硅渗透，碳化前体制品的碳基体转化为碳化硅。

6. 发明授权

US5853429A Method for converting multidimensional sheet structures consisting of polyacrylonitrile fibres into the thermally stabilized stage 失效
标题翻译：将由聚丙烯腈纤维组成的多维片材结构转化为热稳定化阶段的方法
公开(公告)号：US5853429A
公开(公告)日：1998-12-29
申请号：US893737
申请日：1997-07-11
申请人： Michael Heine , Dieter Kompalik
发明人： Michael Heine , Dieter Kompalik
IPC分类号： D01F9/22
CPC分类号： D01F9/225
摘要： Method for converting two-dimensional or three-dimensional sheet structures consisting of polyacrylonitrile fibres or substantially of polyacrylonitrile fibres, such as woven fabrics, layered materials, knitted fabrics, felts, or non-woven fabrics, into the thermally stabilized but non-carbonized state, by means of an oxygen-containing or oxygen-yielding gas flowing through the respective sheet fibre structure. This gas or gas mixture is used as a medium for the temperature control in the sheet fibre structure and as a means for supplying the oxygen carrier and also removing the gaseous reaction products. Temperature and flow velocity of the gas/gas mixture are matched to the stabilization characteristic of the respective sheet fibre structure and are controlled precisely. The device used for carrying out the method consists of a furnace (23) which consists of at least one chamber, through which furnace a web of the sheet fibre structure (18) is moved continuously. During this transportation the oxygen-containing or oxygen-emitting gas flows through the sheet fibre structure (18) in a controlled manner.
摘要翻译：将由聚丙烯腈纤维或基本上由纺织织物，层状材料，针织物，毡或无纺织物组成的聚丙烯腈纤维组成的二维或三维片材结构转化成热稳定但非碳化状态的方法，通过流过各个片材纤维结构的含氧或产氧气体。该气体或气体混合物用作片材纤维结构中温度控制的介质，并用作供应氧载体并除去气态反应产物的方法。气体/气体混合物的温度和流速匹配于各个片材纤维结构的稳定特性，并被精确地控制。用于执行该方法的装置包括由至少一个室组成的炉（23），片状纤维结构（18）的纤维网通过该炉连续移动。在该输送期间，含氧或发氧气体以受控的方式流过片状纤维结构（18）。

7. 发明授权

US07445095B2 Brake system having a composite-material brake disc 有权
标题翻译：具有复合材料制动盘的制动系统
公开(公告)号：US07445095B2
公开(公告)日：2008-11-04
申请号：US10171591
申请日：2002-06-14
申请人： Moritz Bauer , Udo Gruber , Michael Heine , Andreas Kienzle , Rainer Zimmermann-Chopin
发明人： Moritz Bauer , Udo Gruber , Michael Heine , Andreas Kienzle , Rainer Zimmermann-Chopin
IPC分类号： F16D65/10
CPC分类号： C04B35/522 , C04B35/521 , C04B35/524 , C04B35/565 , C04B35/573 , C04B35/63 , C04B35/63492 , C04B35/63496 , C04B35/806 , C04B2235/3217 , C04B2235/3272 , C04B2235/3279 , C04B2235/3813 , C04B2235/3821 , C04B2235/3826 , C04B2235/3839 , C04B2235/386 , C04B2235/3886 , C04B2235/3891 , C04B2235/402 , C04B2235/404 , C04B2235/405 , C04B2235/407 , C04B2235/421 , C04B2235/425 , C04B2235/428 , C04B2235/446 , C04B2235/526 , C04B2235/728 , C04B2235/75 , C04B2235/80 , F16D69/02 , F16D69/023
摘要： A brake system includes a friction coupling having organically or inorganically bound metal-containing, sintered-metal-containing and/or CFC-containing brake linings and a brake disc of fiber-reinforced C/SiC ceramic composite material. A friction layer and/or a surface of the brake disc subject to friction has a proportion of SiC greater than 65% and material compositions in a core region and a surface region of the brake disc are different. The brake system may be used in motor vehicles, rail vehicles or aircraft.
摘要翻译：制动系统包括具有有机或无机结合的含金属，含烧结金属和/或含CFC的制动衬片和纤维增强C / SiC陶瓷复合材料的制动盘的摩擦联接器。摩擦层和/或经受摩擦的制动盘的表面具有大于65％的SiC比例，并且芯区域和制动盘的表面区域中的材料成分不同。制动系统可用于机动车辆，轨道车辆或飞机。

8. 发明申请

US20060071373A1 PROCESS FOR PRODUCING HOLLOW BODIES COMPRISING FIBRE-REINFORCED CERAMIC MATERIALS 有权
标题翻译：生产包含纤维增强陶瓷材料的中空体的方法
公开(公告)号：US20060071373A1
公开(公告)日：2006-04-06
申请号：US10256492
申请日：2002-09-26
申请人： Moritz Bauer , Michael Heine , Udo Gruber , Ronald Huener , Andreas Kienzle , Andreas Rahn , Rainer Zimmermann-Chopin
发明人： Moritz Bauer , Michael Heine , Udo Gruber , Ronald Huener , Andreas Kienzle , Andreas Rahn , Rainer Zimmermann-Chopin
IPC分类号： C04B33/32
CPC分类号： F16D69/023 , B29C43/006 , B29C2043/3668 , C04B35/565 , C04B35/573 , C04B35/83 , C04B2235/404 , C04B2235/405 , C04B2235/428 , C04B2235/48 , C04B2235/5248 , C04B2235/526 , C04B2235/5268 , C04B2235/5272 , C04B2235/6028 , C04B2235/728 , C04B2235/80 , C04B2235/94 , F16D13/64 , F16D65/12 , F16D2200/0052
摘要： Process for producing hollow bodies comprising fibre-reinforced ceramic materials, where cores whose shape corresponds to that of the hollow spaces are produced in a first step, a green body is produced in a second step by introducing the abovementioned cores and a press moulding compound into a mould, where the press moulding compound comprises carbon fibres and/or carbon threads and pitch and/or resins, the green body is cured in a third step by heating under pressure, and then carbonised in a fourth step by heating in the absence of oxidants to form a C/C body, which latter can be infiltrated with liquid metal with retention of its shape in a fifth step, with at least partial formation of carbides, where the cores comprise a material which is non-meltable but undergoes at least sufficient shrinkage above the curing temperature of the shaping by pressing of the press moulding compound for the shrunken core to be able to be taken out from the carbonised body; hollow bodies produced by this process and also their use as brake disks, clutch disks and friction disks
摘要翻译：制造中空体的方法，其中纤维强化陶瓷材料的形状对应于中空空间的芯体在第一步骤中生产，在第二步骤中，通过将上述芯体和压模化合物引入模具，其中压模成型料包括碳纤维和/或碳线和沥青和/或树脂，生坯在第三步骤中通过在加压下加热固化，然后在第四步骤中通过在不存在氧化剂形成C / C体，后者可以用液态金属渗透，并在第五步中保持其形状，至少部分形成碳化物，其中芯包含不可熔化但经历至少通过压缩用于收缩芯的加压模塑料能够从碳化体中取出而使成形的固化温度以上的充分收缩; 通过该方法生产的中空体以及它们用作制动盘，离合器盘和摩擦盘

9. 发明授权

US07011786B2 Process for producing shaped bodies comprising fiber-reinforced ceramic materials 有权
标题翻译：包括纤维增强陶瓷材料的成形体的制造方法
公开(公告)号：US07011786B2
公开(公告)日：2006-03-14
申请号：US10328659
申请日：2002-12-23
申请人： Moritz Bauer , Michael Heine , Andreas Kienzle , Ronald Huener , Rainer Zimmermann-Chopin , Andreas Rahn
发明人： Moritz Bauer , Michael Heine , Andreas Kienzle , Ronald Huener , Rainer Zimmermann-Chopin , Andreas Rahn
IPC分类号： B29C35/08 , B29C59/00 , B29C67/00 , C01B31/00 , D01F9/12
CPC分类号： F16D65/125 , C04B35/573 , C04B35/806 , C04B35/83 , F16D69/023 , F16D2200/0039 , F16D2200/0052 , F16D2200/006 , Y10T428/249927 , Y10T428/249928
摘要： Process for producing shaped bodies comprising fiber-reinforced ceramic materials, where a green body is produced in a first step by introducing a press moulding composition into a mold, where the press moulding composition comprises carbon fibers and/or carbon filaments and pitch and/or resins which, when treated thermally and with the exclusion of oxidizing agents, form carbon-containing residues, the green body is cured in a second step by heating to a temperature of from 120° C. to 280° C. under pressure, the cured green body, also referred to as intermediate body, is carbonized in a third step by heating in a nonoxidizing atmosphere to a temperature of from about 750° C. to about 1100° C. to form a C/C body, wherein heating in the first, second and/or third step is at least partly effected by an electric current being passed through the pressable composition, the green body and/or the cured green body, shaped bodies produced according to this process and their use as brake disks, clutch disks and friction disks
摘要翻译：包括纤维增强陶瓷材料的成型体的制造方法，其中通过将压制成型组合物引入模具中，在第一步骤中生产生坯体，其中压制成型组合物包含碳纤维和/或碳丝，沥青和/或在热处理和排除氧化剂的情况下，形成含碳残留物的树脂在第二步骤中通过在压力下加热至120℃至280℃的温度而固化，固化也称为中间体的生坯通过在非氧化气氛中加热至约750℃至约1100℃的温度而在第三步骤中进行碳化以形成C / C体，其中在第一，第二和/或第三步骤至少部分地通过通过可挤压组合物，生坯和/或固化的生坯体的电流，根据该方法制造的成形体及其作为制动器的用途 ks，离合器盘和摩擦盘

10. 发明授权

US06759117B2 Multilayer ceramic composite and process for forming the composite 有权
标题翻译：多层陶瓷复合材料和复合材料的成型工艺
公开(公告)号：US06759117B2
公开(公告)日：2004-07-06
申请号：US10190821
申请日：2002-07-08
申请人： Moritz Bauer , Martin Christ , Udo Gruber , Michael Heine , Andreas Kienzle , Jens Rosenlöcher , Rainer Zimmermann-Chopin
发明人： Moritz Bauer , Martin Christ , Udo Gruber , Michael Heine , Andreas Kienzle , Jens Rosenlöcher , Rainer Zimmermann-Chopin
IPC分类号： B32B1800
CPC分类号： F16D69/023 , C04B35/571 , C04B35/573 , C04B35/584 , C04B35/62873 , C04B35/63492 , C04B37/005 , C04B37/008 , C04B2235/3201 , C04B2235/3205 , C04B2235/3217 , C04B2235/36 , C04B2235/3804 , C04B2235/3813 , C04B2235/3826 , C04B2235/3891 , C04B2235/404 , C04B2235/405 , C04B2235/421 , C04B2235/428 , C04B2235/5248 , C04B2235/526 , C04B2235/616 , C04B2235/80 , C04B2237/08 , C04B2237/083 , C04B2237/385 , C04B2237/61 , C04B2237/708 , F16D69/02 , Y10T156/10 , Y10T428/12562 , Y10T428/12681 , Y10T428/24099 , Y10T428/249928 , Y10T428/292
摘要： A multilayer ceramic composite is described which contains at least one supporting zone having oxidation-sensitive reinforcing fibers as well as a matrix. The matrix optionally contains oxidation-sensitive components. The composite further contains at least one surface layer, as well as at least one additional protective layer disposed between the supporting zone and surface layer, and whose matrix is composed substantially of at least one component of the matrix of the supporting zone or cover layer. The protective layer further contains additives that form self-healing layers.
摘要翻译：描述了包含至少一个具有氧化敏感性增强纤维的支撑区域以及基质的多层陶瓷复合体。该基质任选地含有氧化敏感组分。所述复合材料还包含至少一个表面层以及设置在所述支撑区域和表面层之间的至少一个附加保护层，并且其基质基本上由所述支撑区域或覆盖层的基质的至少一个组分组成。保护层还含有形成自愈层的添加剂。

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