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1. 发明申请

US20190017873A1 PROCESS AND SYSTEM FOR SAMPLE ANALYSIS 审中-公开
公开(公告)号：US20190017873A1
公开(公告)日：2019-01-17
申请号：US16051904
申请日：2018-08-01
申请人： MLS ACQ, Inc D/B/A Max Analytical Technology
发明人： Martin L. Spartz , Anthony S. Bonanno , Peter P. Behnke
IPC分类号： G01J3/42 , G01N30/74 , G01N21/3504 , G01N21/03 , G01N30/86 , G01N21/3581 , G01N21/33 , G01N21/65 , G01N21/64 , G01N21/35 , G01N30/00 , G01N30/02 , G01N21/359
CPC分类号： G01J3/42 , G01N21/031 , G01N21/33 , G01N21/3504 , G01N21/3581 , G01N21/359 , G01N21/64 , G01N21/65 , G01N30/74 , G01N30/8606 , G01N30/8641 , G01N2021/3595 , G01N2030/008 , G01N2030/025 , G01N2030/743
摘要： Components resolved in time by a separator accumulate in a sample cell and are analyzed by electromagnetic radiation-based spectroscopic techniques. The sample cell can be configured for multiple path absorption and can be heated. The separator can be a gas chromatograph or another suitable device, for example a distillation-based separator. The method and system described herein can include other mechanical elements, controls, procedures for handling background and sample data, protocols for species identification and/or quantification, automation, computer interfaces, algorithms, software or other features.

2. 发明申请

US20040035183A1 Method and apparatus for sample analysis 有权
标题翻译：样品分析方法和装置
公开(公告)号：US20040035183A1
公开(公告)日：2004-02-26
申请号：US10438517
申请日：2003-05-14
申请人： The State of Oregon acting and through the State Board of Higher Education on behalf of Portl
发明人： Robert J. O'Brien , Thomas R. Smith
IPC分类号： G01N030/78 , G01N030/60 , G01N030/02 , G01N021/49 , G01D011/24
CPC分类号： G01N30/22 , G01N1/2202 , G01N1/24 , G01N1/40 , G01N30/08 , G01N30/8606 , G01N30/8641 , G01N2001/2223 , G01N2001/2238 , G01N2001/2282 , G01N2001/4027 , G01N2015/0046 , G01N2015/0092 , G01N2030/025 , G01N2030/207 , G01N2030/328 , G01N2030/625 , G01N2030/626 , G01N30/06 , G01N30/32
摘要： Methods and systems for analyzing samples, such as gas samples, are described. One method comprises providing a gas sample, increasing pressure applied to the gas sample to compress the sample to a smaller volume and provide a pneumatically focused gas sample, and analyzing the pneumatically focused gas sample using any of a variety of analytical techniques. Also disclosed are systems for gas analysis, including systems for analysis of pneumatically focused, and thereby concentrated, gas samples and for analysis of particulate matter in gas samples. Analytical systems constructed within personal computer cases also are disclosed.
摘要翻译：描述了用于分析样品（如气体样品）的方法和系统。一种方法包括提供气体样品，增加施加到气体样品的压力以将样品压缩到更小的体积并提供气动聚焦的气体样品，以及使用各种分析技术中的任何一种分析气动聚焦的气体样品。还公开了用于气体分析的系统，包括用于气动聚焦的分析系统，从而分析气体样品，从而分析气体样品中的颗粒物质。在个人计算机机箱内构建的分析系统也被公开。

3. 发明申请

US20030015019A1 Method and apparatus for concentrating samples for analysis 有权
标题翻译：用于浓缩样品进行分析的方法和装置
公开(公告)号：US20030015019A1
公开(公告)日：2003-01-23
申请号：US09770942
申请日：2001-01-25
申请人： The State of Oregon Acting by and through the State Board of Higher Education on behalf of Portl
发明人： Robert O'Brien
IPC分类号： G01N001/00
CPC分类号： G01N1/2202 , G01N1/24 , G01N1/40 , G01N30/06 , G01N30/22 , G01N30/78 , G01N30/8606 , G01N30/8641 , G01N2001/2223 , G01N2001/4027 , G01N2015/0046 , G01N2015/0092 , G01N2030/025 , G01N2030/328 , G01N2030/625 , G01N2030/626 , G01N30/32
摘要： A method for analyzing a gas sample is described. The method comprises providing a gas sample, increasing pressure applied to the gas sample to compress the sample to a smaller volume and provide a pneumatically focused gas sample, and analyzing the pneumatically focused gas sample using any of a variety of analytical techniques. Pneumatic Focusing generally means increasing the pressure of the sample, column or cell to a pressure of from about 100 psi to about 15,000 psi, more typically from about 200 psi to about 2,000 psi. Examples including gas chromatography and absorption spectroscopy are illustrated herein. Numerous other examples could be given. The method is well suited for analyzing gaseous samples, such as ambient air samples, both continuously, and remotely, using computer control. Continuously sampling ambient air provides a method for real-time monitoring of air quality. Continuous monitoring allows for pollutant exposure and allows for the identification of emission sources. The method is also well suited for analysis of breath exhalations from respiring organisms useful in metabolic studies or disease diagnosis.
摘要翻译：对气体样品的分析方法进行说明。该方法包括提供气体样品，增加施加到气体样品的压力以将样品压缩到更小的体积并提供气动聚焦的气体样品，以及使用各种分析技术中的任何一种来分析气动聚焦的气体样品。气动聚焦通常意味着将样品，柱或细胞的压力提高到约100psi至约15,000psi，更典型地约200psi至约2,000psi的压力。本文说明了包括气相色谱和吸收光谱的实例。可以给出很多其他例子。该方法非常适用于使用计算机控制连续和远程分析气态样品，如环境空气样品。连续采样环境空气提供了一种实时监测空气质量的方法。连续监测允许污染物暴露并允许识别排放源。该方法也非常适用于分析代谢研究或疾病诊断中有用的呼吸生物的呼吸呼气。

4. 发明授权

US6112161A Method, apparatus, and article of manufacture for enhanced intergration of signals 失效
标题翻译：用于增强信号整合的方法，装置和制造
公开(公告)号：US6112161A
公开(公告)日：2000-08-29
申请号：US932150
申请日：1997-09-17
申请人： Paul C. Dryden , Bruce D. Quimby
发明人： Paul C. Dryden , Bruce D. Quimby
IPC分类号： G01N30/86
CPC分类号： G01N30/8603 , G01N30/8624 , G01N2030/8854 , G01N30/8606 , G01N30/8641
摘要： A method, apparatus, and article of manufacture for enhanced integration of signals, such as those generated by chromatographs. In one embodiment an approximate baseline used for integration of a signal is improved to reduce error. Alternate embodiments filter drift, noise, or both from a signal prior to integration or simulated distillation. The signals are processed according to a computer program stored in a memory. The methods include steps for subtracting an approximate baseline from the signal, defining a noise band in the resulting difference, and forming a composite baseline by substituting signal data for baseline data wherever the difference does not exceed the threshold, thus leaving the parts of the approximate baseline that correspond to signal peaks unchanged.
摘要翻译：用于增强信号集成的方法，装置和制品，例如由色谱仪产生的信号。在一个实施例中，用于信号积分的近似基线被改进以减少误差。替代实施例在集成或模拟蒸馏之前从信号滤波漂移，噪声或二者。信号根据存储在存储器中的计算机程序进行处理。这些方法包括从信号中减去近似基线的步骤，在所得到的差值中定义噪声带，并通过将信号数据代入基线数据形成复合基线，无论差值不超过阈值，因此留下近似的部分对应于信号峰的基线不变。

5. 发明授权

US5352585A System for benzodiazepine detection 失效
标题翻译：苯二氮卓检测系统
公开(公告)号：US5352585A
公开(公告)日：1994-10-04
申请号：US084845
申请日：1993-06-29
申请人： Steven R. Binder , David L. King
发明人： Steven R. Binder , David L. King
IPC分类号： G01N30/02 , G01N30/06 , G01N30/08 , G01N30/14 , G01N30/34 , G01N30/46 , G01N30/74 , G01N30/86 , G01N30/88
CPC分类号： G01N30/461 , G01N30/88 , G01N2030/027 , G01N2030/085 , G01N2030/8804 , G01N2030/8813 , G01N2030/8831 , G01N30/02 , G01N30/06 , G01N30/14 , G01N30/34 , G01N30/468 , G01N30/74 , G01N30/8606 , G01N30/8679 , Y10S436/901 , Y10T436/14 , Y10T436/145555 , Y10T436/17 , Y10T436/25 , Y10T436/25125 , Y10T436/255
摘要： Biological samples are analyzed for benzodiazepines in a single isocratic analysis using a chromatographic column system containing an immobilized enzyme reactor which cleaves glucuronic acid-conjugated benzodiazepines, an anion exchange column, a hydrophobic cation exchange column and a reverse-phase analytical column. Preferred methods of performing the analysis further involve the use of a hydrophobic cation exchange precolumn prior to the anion exchange column. The system readily lends itself to automation, automatic periodic sampling and benzodiazepine identification and quantification. The system is particularly well adapted to the determination and identification of benzodiazepines in urine samples.
摘要翻译：在使用含有固定化酶反应器的色谱柱系统的单一等度分析中分析生物样品中的苯并二氮杂，所述固定化酶反应器切割葡糖醛酸 - 共轭苯并二氮杂，阴离子交换柱，疏水性阳离子交换柱和反相分析柱。执行分析的优选方法还涉及在阴离子交换柱之前使用疏水性阳离子交换预柱。该系统易于自动化，自动定期取样和苯二氮卓鉴定和定量。该系统特别适用于尿液样品中苯二氮卓类的测定和鉴定。

6. 发明授权

US4875169A Method for improving the limit of detection in a data signal 失效
标题翻译：用于提高数据信号中检测限的方法
公开(公告)号：US4875169A
公开(公告)日：1989-10-17
申请号：US201304
申请日：1988-05-27
申请人： Robert E. Synovec , Edward S. Yueng
发明人： Robert E. Synovec , Edward S. Yueng
IPC分类号： G01N30/62 , G01N30/86
CPC分类号： G01N30/86 , G01N2030/621 , G01N30/8606 , G01N30/8641
摘要： A method for improving the limit of detection for a data set in which experimental noise is uncorrelated along a given abscissa and an analytical signal is correlated to the abscissa, the steps comprising collecting the data set, converting the data set into a data signal including an analytical portion and the experimental noise portion, designating and adjusting a baseline of the data signal to center the experimental noise numerically about a zero reference, and integrating the data signal preserving the corresponding information for each point of the data signal. The steps of the method produce an enhanced integrated data signal which improves the limit of detection of the data signal.
摘要翻译：一种用于改善沿着给定横坐标和实验噪声不相关的数据集的检测限的方法与横坐标相关，所述步骤包括收集数据集，将数据集转换为包括数据信号的数据信号分析部分和实验噪声部分，指定和调整数据信号的基线，使实验噪声以零参考为中心，并对保存数据信号的每个点的相应信息进行积分。该方法的步骤产生增强的集成数据信号，其改善了数据信号的检测限。

7. 发明授权

US3779069A Chromatographic apparatus and method 失效
标题翻译：色谱装置和方法
公开(公告)号：US3779069A
公开(公告)日：1973-12-18
申请号：US3779069D
申请日：1971-01-04
申请人： PETROCHEM KOM SCHWEDT VEB
发明人： BERTHOLD G
IPC分类号： G01N30/62 , G01N30/86 , G01N30/88 , G01N31/08
CPC分类号： G01N30/8651 , G01N30/62 , G01N30/8606 , G01N30/88 , Y10T137/86413
摘要： A gas chromatograph for analyzing specimens from a chemicalprocess line is triggered by a pneumatic sawtooth generator. The output signal is delivered to the recorder directly and through control, regulating and computing elements, all operating with pneumatic, rather than electrical, signals. The process regulator is likewise of the pneumatic type.
摘要翻译：用于分析来自化学处理线的样品的气相色谱仪由气动锯齿发生器触发。输出信号通过控制，调节和计算元件直接输送到记录仪，全部采用气动而不是电气信号运行。过程调节器同样是气动式的。

8. 发明授权

US08874381B2 Method of measuring destruction rate of refrigerant 有权
标题翻译：测量制冷剂破坏率的方法
公开(公告)号：US08874381B2
公开(公告)日：2014-10-28
申请号：US13172012
申请日：2011-06-29
申请人： Dae Sung Jung , Jun Young Lee , Jong Rae Cho , Han Seok Kim
发明人： Dae Sung Jung , Jun Young Lee , Jong Rae Cho , Han Seok Kim
IPC分类号： G01N1/22 , G01N30/88 , G06F17/40 , G06F19/00 , G01N30/72
CPC分类号： G01N30/8606 , G01N1/2258 , G01N30/7206 , G01N30/88 , G01N2030/8845 , G06F17/40 , G06F19/00
摘要： The present invention provides a method for calculating a destruction rate of refrigerant by establishing a calibration line using standard refrigerant gases and measuring the amount of refrigerant remaining in exhaust gas discharged after destruction of waste refrigerant. For this purpose, the present invention provides a method for calculating a destruction rate of refrigerant, the method including: establishing a calibration line using standard refrigerant gas samples whose concentrations are known; sampling exhaust gas finally discharged after decomposition of waste refrigerant; measuring the concentration of refrigerant remaining in the sampled exhaust gas; and calculating the amount of undestroyed refrigerant using the concentration of refrigerant remaining in the exhaust gas, the amount of exhaust gas discharged, and the known density of refrigerant.
摘要翻译：本发明提供了一种通过使用标准制冷剂气体建立校准线并测量废弃制冷剂破坏后排出的废气中剩余的制冷剂量来计算制冷剂破坏率的方法。为此，本发明提供一种计算制冷剂破坏率的方法，该方法包括：使用浓度已知的标准制冷剂气体样品建立校准线; 废气分解后排气最终排放; 测量取样废气中剩余的制冷剂的浓度; 以及使用残留在排气中的制冷剂的浓度，排出的排气量和已知的制冷剂密度来计算未破坏的制冷剂的量。

9. 发明授权

US06865926B2 Method and apparatus for sample analysis 有权
标题翻译：样品分析方法和装置
公开(公告)号：US06865926B2
公开(公告)日：2005-03-15
申请号：US10438517
申请日：2003-05-14
申请人： Robert J. O'Brien , Thomas R. Smith
发明人： Robert J. O'Brien , Thomas R. Smith
IPC分类号： G01N1/22 , G01N1/24 , G01N1/40 , G01N15/00 , G01N30/02 , G01N30/06 , G01N30/08 , G01N30/22 , G01N30/32 , G01N30/62 , G01N30/86 , G01N30/04
CPC分类号： G01N30/22 , G01N1/2202 , G01N1/24 , G01N1/40 , G01N30/08 , G01N30/8606 , G01N30/8641 , G01N2001/2223 , G01N2001/2238 , G01N2001/2282 , G01N2001/4027 , G01N2015/0046 , G01N2015/0092 , G01N2030/025 , G01N2030/207 , G01N2030/328 , G01N2030/625 , G01N2030/626 , G01N30/06 , G01N30/32
摘要： Methods and systems for analyzing samples, such as gas samples, are described. One method comprises providing a gas sample, increasing pressure applied to the gas sample to compress the sample to a smaller volume and provide a pneumatically focused gas sample, and analyzing the pneumatically focused gas sample using any of a variety of analytical techniques. Also disclosed are systems for gas analysis, including systems for analysis of pneumatically focused, and thereby concentrated, gas samples and for analysis of particulate matter in gas samples. Analytical systems constructed within personal computer cases also are disclosed.
摘要翻译：描述了用于分析样品（如气体样品）的方法和系统。一种方法包括提供气体样品，增加施加到气体样品的压力以将样品压缩到更小的体积并提供气动聚焦的气体样品，以及使用各种分析技术中的任何一种分析气动聚焦的气体样品。还公开了用于气体分析的系统，包括用于气动聚焦的分析系统，从而分析气体样品，从而分析气体样品中的颗粒物质。在个人计算机机箱内构建的分析系统也被公开。

10. 发明授权

US5416023A System for benzodiazepine detection 失效
标题翻译：苯二氮卓检测系统
公开(公告)号：US5416023A
公开(公告)日：1995-05-16
申请号：US271390
申请日：1994-07-06
申请人： Steven R. Binder , David L. King
发明人： Steven R. Binder , David L. King
IPC分类号： G01N30/02 , G01N30/06 , G01N30/08 , G01N30/14 , G01N30/34 , G01N30/46 , G01N30/74 , G01N30/86 , G01N30/88
CPC分类号： G01N30/461 , G01N30/88 , G01N2030/027 , G01N2030/085 , G01N2030/8804 , G01N2030/8813 , G01N2030/8831 , G01N30/02 , G01N30/06 , G01N30/14 , G01N30/34 , G01N30/468 , G01N30/74 , G01N30/8606 , G01N30/8679 , Y10S436/901 , Y10T436/14 , Y10T436/145555 , Y10T436/17 , Y10T436/25 , Y10T436/25125 , Y10T436/255
摘要： Biological samples are analyzed for benzodiazepines in a single isocratic analysis using a chromatographic column system containing an immobilized enzyme reactor which cleaves glucuronic acid-conjugated benzodiazepines, an anion exchange column, a hydrophobic cation exchange column and a reverse-phase analytical column. Preferred methods of performing the analysis further involve the use of a hydrophobic cation exchange precolumn prior to the anion exchange column. The system readily lends itself to automation, automatic periodic sampling and benzodiazepine identification and quantification. The system is particularly well adapted to the determination and identification of benzodiazepines in urine samples.
摘要翻译：在使用含有固定化酶反应器的色谱柱系统的单一等度分析中分析生物样品中的苯并二氮杂，所述固定化酶反应器切割葡糖醛酸 - 共轭苯并二氮杂，阴离子交换柱，疏水性阳离子交换柱和反相分析柱。执行分析的优选方法还涉及在阴离子交换柱之前使用疏水性阳离子交换预柱。该系统易于自动化，自动定期取样和苯二氮卓鉴定和定量。该系统特别适用于尿液样品中苯二氮卓类的测定和鉴定。

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