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1. 发明授权

US09757769B2 Composition and method to form a self decontaminating surface 有权
公开(公告)号：US09757769B2
公开(公告)日：2017-09-12
申请号：US13448325
申请日：2012-04-16
申请人： Craig Grossman , Mai Ngo , Ronald Wysocki
发明人： Craig Grossman , Mai Ngo , Ronald Wysocki
IPC分类号： B05D7/00 , D06M11/46 , D06M13/51 , D06M13/513 , C09D5/00 , D06M23/00 , B05D5/00 , B05D1/02 , B05D1/04
CPC分类号： C09D5/14 , A01N55/00 , A01N55/02 , B05D1/02 , B05D1/04 , B05D5/00 , B05D7/52 , B05D2425/01 , B05D2601/24 , C07F7/28 , C08G77/26 , C08G79/00 , C09D5/00 , C09D7/63 , C09D183/08 , C09D185/00 , D06M11/46 , D06M13/51 , D06M13/513 , D06M15/423 , D06M23/005
摘要： A method to prepare a self-decontaminating surface, where that method includes disposing a first coating on a surface, where that first coating comprises an organosilane, and disposing a second coating over the first coating, where the second coating comprises TiO2.

2. 发明申请

US20170158873A1 COATING COMPOSITIONS COMPRISING POLYMERS HAVING TITANIUM/OXYGEN OR SILICON/OXYGEN BACKBONES 审中-公开
公开(公告)号：US20170158873A1
公开(公告)日：2017-06-08
申请号：US15432352
申请日：2017-02-14
申请人： Allied Bioscience, Inc.
发明人： Craig Grossman , Mai Ngo , Ronald Wysocki
IPC分类号： C09D5/14 , A01N55/02 , A01N55/00 , C09D7/12 , C09D185/00
CPC分类号： C09D5/14 , A01N55/00 , A01N55/02 , B05D1/02 , B05D1/04 , B05D5/00 , B05D7/52 , B05D2425/01 , B05D2601/24 , C07F7/28 , C08G77/26 , C08G79/00 , C09D5/00 , C09D7/63 , C09D183/08 , C09D185/00 , D06M11/46 , D06M13/51 , D06M13/513 , D06M15/423 , D06M23/005
摘要： A method to prepare a self-decontaminating surface, where that method includes disposing a first coating on a surface, where that first coating comprises an organosilane, and disposing a second coating over the first coating, where the second coating comprises TiO2.

3. 发明授权

US08679197B2 Conformal particle coatings on fibrous materials 有权
标题翻译：纤维材料上的保形颗粒涂层
公开(公告)号：US08679197B2
公开(公告)日：2014-03-25
申请号：US13945015
申请日：2013-07-18
申请人： Cornell University
发明人： Juan P. Hinestroza , Hong Dong
IPC分类号： D06M15/423 , B32B5/16
CPC分类号： D06M23/08 , D06M10/025 , D06M16/00 , D06M23/005
摘要： Methods are provided for uniform deposition of particles on curved surfaces such as fibers and coatings formed by the particles. Particles in the size range of 10-2000 nm are deposited onto a fibrous material via electrostatic interaction between charge modified fiber material surfaces and oppositely charged particles or metal ions. Various nonmetallic, bimetallic or other charged particles are deposited onto a fibrous material via electrostatic interaction between charged modified fibrous material surfaces and oppositely charged particles. Particles can be directly assembled onto a surface of a fibrous material by controlling hydrogen bonding interactions between interfaces of fibers and functionalized particles. Metal particles can also be deposited by in situ synthesis. A method is also provided for layer-by-layer deposition of particles over a fibrous material.
摘要翻译：提供了用于在诸如由颗粒形成的纤维和涂层的曲面上均匀沉积颗粒的方法。尺寸范围为10-2000nm的颗粒通过电荷改性纤维材料表面和带相反电荷的颗粒或金属离子之间的静电相互作用沉积到纤维材料上。各种非金属，双金属或其他带电粒子通过带电的改性纤维材料表面和带相反电荷的颗粒之间的静电相互作用沉积到纤维材料上。通过控制纤维和功能化颗粒的界面之间的氢键相互作用，可以将颗粒直接组装到纤维材料的表面上。金属颗粒也可以通过原位合成沉积。还提供了一种用于在纤维材料上逐层沉积颗粒的方法。

4. 发明申请

US20120269973A1 Automated Layer By Layer Spray Technology 有权
标题翻译：自动层叠喷涂技术
公开(公告)号：US20120269973A1
公开(公告)日：2012-10-25
申请号：US13543105
申请日：2012-07-06
申请人： Kevin C. Krogman , Paula T. Hammond , Nicole S. Zacharia
发明人： Kevin C. Krogman , Paula T. Hammond , Nicole S. Zacharia
IPC分类号： B05D3/10 , B05B17/00 , B05D1/36 , B05B1/00
CPC分类号： B05D1/02 , B01D67/0088 , B01D2323/02 , B01D2323/26 , B05D7/50 , D06M15/233 , D06M15/263 , D06M15/3562 , D06M15/3566 , D06M15/61 , D06M23/005 , D06M23/06
摘要： The present invention comprises an automated apparatus capable of spray depositing polyelectrolytes via the LbL mechanism with minimal or no human interaction. In certain embodiments, the apparatus sprays atomized polyelectrolytes onto a vertically oriented substrate. To counteract the effects of irregular spray patterns, the substrate is preferably slowly rotated about a central axis. In certain embodiments, the apparatus also includes a forced pathway for the droplets, such as a pathway created by using a vacuum. In this way, a thicker or three-dimensional substrate can be coated. In certain embodiments, the apparatus is designed so as to be scalable. Thus, through the use of multiple instantiations of the apparatus, a large or irregularly shaped substrate can be coated. Rolls of textile can therefore be coated using the apparatus. Additionally, the present invention includes a method to uniformly coat a substrate, such as a hydrophobic textile material, using aqueous solutions of polyelectrolytes.
摘要翻译：本发明包括能够通过LbL机制以最少或没有人类相互作用喷射沉积聚电解质的自动化装置。在某些实施方案中，该装置将雾化的聚电解质喷射到垂直取向的基底上。为了抵消不规则喷雾图案的影响，衬底优选地围绕中心轴缓慢旋转。在某些实施例中，该装置还包括用于液滴的强制通道，例如通过使用真空产生的通路。以这种方式，可以涂覆较厚或三维的基底。在某些实施例中，设备被设计成可伸缩的。因此，通过使用设备的多个实例，可以涂覆大或不规则形状的基底。因此可以使用该装置涂布纺织品卷。此外，本发明包括使用聚电解质的水溶液均匀地涂覆基底如疏水纺织材料的方法。

5. 发明授权

US07906177B2 Method for making an article hydrophobic and oleophobic as well as articles made therefrom and their use 有权
标题翻译：制造疏水性和疏油性物品的方法以及由其制成的制品及其用途
公开(公告)号：US07906177B2
公开(公告)日：2011-03-15
申请号：US11317036
申请日：2005-12-22
申请人： Edgar A. O'Rear , Nantaya Yanumet
发明人： Edgar A. O'Rear , Nantaya Yanumet
IPC分类号： B05D3/10
CPC分类号： C09D5/00 , B05D5/083 , C08K5/41 , C08K5/42 , C09D4/00 , C09D7/63 , D06M13/256 , D06M13/262 , D06M15/277 , D06M23/005 , D06M2200/11 , D06M2200/12 , D21H19/44 , D21H19/64 , D21H21/16 , Y10T428/31504 , Y10T428/3154 , Y10T428/31544 , Y10T442/20 , Y10T442/2164 , Y10T442/2213 , Y10T442/2238 , Y10T442/2262
摘要： The present invention relates in general to a method and variations thereof for making an article, such as cloth, water repellent and/or water resistant (i.e. hydrophobic) as well as oil repellent (i.e. oleophobic). In particular, the method involves the process of providing a thin-layer polymer coating on the article thereby rendering the article water repellent and/or water resistant. Articles made according to the method of the present invention are also disclosed and claimed herein as are the treated articles' use.
摘要翻译：本发明一般涉及用于制造诸如布，防水和/或防水（即疏水性）以及防油剂（即疏油性）的制品的方法和变型。特别地，该方法包括在制品上提供薄层聚合物涂层的过程，从而使制品防水和/或防水。根据本发明的方法制造的制品也在经处理制品的使用中公开和要求保护。

6. 发明授权

US06967059B2 METHOD OF REFORMING ELEMENT SURFACE, ELEMENT WITH REFORMED SURFACE, METHOD OF MANUFACTURING ELEMENT WITH REFORMED SURFACE, SURFACE TREATMENT LIQUID FOR FORMING REFORMED SURFACE, AND METHOD OF MANUFACTURING SURFACE TREATMENT LIQUID 失效
标题翻译：改性元件表面的方法，具有改性表面的元件，用改性表面制造元件的方法，用于形成改性表面的表面处理液以及制造表面处理液的方法
公开(公告)号：US06967059B2
公开(公告)日：2005-11-22
申请号：US09725032
申请日：2000-11-29
申请人： Mikio Sanada , Sadayuki Sugama , Hiroki Hayashi
发明人： Mikio Sanada , Sadayuki Sugama , Hiroki Hayashi
IPC分类号： C08J7/12 , B05D1/18 , C08F8/42 , C08J7/04 , C08J7/14 , C09D183/00 , C09D183/04 , C09D183/08 , C09D183/12 , D06M13/507 , D06M15/647 , D06M23/00 , C08G77/12 , C08L75/00
CPC分类号： B82Y30/00 , B05D1/185 , B82Y40/00 , C08F8/42 , C08J7/047 , C08J7/14 , C08J2323/02 , C08J2483/00 , C09D183/04 , C09D183/08 , C09D183/12 , D06M15/647 , D06M23/005 , Y10T428/2995 , Y10T428/2998 , Y10T428/31663 , Y10T428/31855 , Y10T428/8305
摘要： A surface reforming method capable of efficiently carrying out a sustainable, even reforming treatment on a prescribed surface part of an element, a surface treatment liquid to be employed for the above-described method, and an element having a reformed surface treated by the above-described method. A part of the surface of an element is subjected to the reforming treatment by providing the object surface with a polymer, which is different from a constituent material of the objet surface and comprises a first part having a functional group and a second part having an interfacial energy different from that of the functional group and approximately equal to the surface energy of the object surface and orienting the second part of the polymer toward the object surface and orienting the first part in a direction different from the object surface.
摘要翻译：一种表面改性方法，能够有效地对元素的规定表面部分进行可持续均匀的重整处理，用于上述方法的表面处理液，以及通过上述方法处理的具有重整表面的元件，描述方法。通过为物体表面提供不同于对象表面的构成材料的聚合物，对元件表面的一部分进行重整处理，并且包括具有官能团的第一部分和具有界面的第二部分能量与功能组的能量不同，大致等于物体表面的表面能，并将聚合物的第二部分朝向物体表面定向，并使第一部分沿与物体表面不同的方向取向。

7. 发明申请

US20030051295A1 Modified textiles and other materials and methods for their proparation 失效
标题翻译：改性纺织品及其其他材料和方法的推荐
公开(公告)号：US20030051295A1
公开(公告)日：2003-03-20
申请号：US10198415
申请日：2002-07-17
申请人： Nano- Tex, LLC
发明人： David S. Soane , David A. Offord
IPC分类号： D06P001/00
CPC分类号： C08B3/12 , C08B3/10 , C08B3/14 , C08B15/00 , D06M13/184 , D06M13/513 , D06M15/03 , D06M15/05 , D06M15/11 , D06M15/227 , D06M15/263 , D06M15/277 , D06M15/285 , D06M15/333 , D06M15/347 , D06M15/3562 , D06M15/643 , D06M23/00 , D06M23/005 , D06M2101/06 , D06M2101/12 , D06M2101/34 , D06M2400/01 , D06P1/653 , D06P5/04 , Y10T442/2164
摘要： Provided are compounds and methods for modifying a material to change properties of the material, as well as a variety of products obtained using the methods. In one embodiment, a material comprising one or more modifiable functional groups is reacted with an activated hydrophobic acyl group in the presence of a hindered base, thereby to covalently attach the hydrophobic acyl group to the modifiable functional groups on the material. The material which is modified may be, for example, a carbohydrate, and the modifiable functional groups on the material may be hydroxyls. For example, materials such as cellulose may be modified by reacting it with a acid chloride or acid anhydride including a hydrophobic acyl group, in the presence of a hindered base, such as tripentylamine, to attach the hydrophobic acyl groups to the hydroxyls on the cellulose, thereby to increase the hydrophobicity of the cellulose. The methods and compounds disclosed herein may be used to modify materials to improve properties such as resistance, grease repellency, soil resistance and permanent press properties.
摘要翻译：提供了用于改变材料以改变材料性质的化合物和方法，以及使用这些方法获得的各种产品。在一个实施方案中，包含一个或多个可修饰的官能团的材料在受阻碱的存在下与活化的疏水性酰基反应，从而将疏水性酰基共价连接到材料上的可修饰官能团上。被修饰的材料可以是例如碳水化合物，并且材料上的可修饰的官能团可以是羟基。例如，纤维素等材料可以通过使其与含有疏水性酰基的酰基氯或酸酐在受阻碱例如三戊胺的存在下反应而进行改性，以将疏水性酰基与纤维素上的羟基连接，从而增加纤维素的疏水性。本文公开的方法和化合物可用于改性材料以改善诸如电阻，拒油性，耐土壤性和永久性冲击性能的性能。

8. 发明授权

US06380336B1 Copolymers and oil-and water-repellent compositions containing them 失效
标题翻译：含有它们的共聚物和防油和疏水组合物
公开(公告)号：US06380336B1
公开(公告)日：2002-04-30
申请号：US09546199
申请日：2000-04-10
申请人： David S. Soane , David A. Offord
发明人： David S. Soane , David A. Offord
IPC分类号： C08F1820
CPC分类号： C08B3/10 , C08B3/12 , C08B3/14 , C08B15/00 , C08F220/22 , D06M13/184 , D06M13/513 , D06M15/03 , D06M15/05 , D06M15/11 , D06M15/227 , D06M15/248 , D06M15/263 , D06M15/273 , D06M15/277 , D06M15/285 , D06M15/333 , D06M15/347 , D06M15/3562 , D06M15/643 , D06M23/00 , D06M23/005 , D06M2101/06 , D06M2101/12 , D06M2101/34 , D06M2200/11 , D06M2200/12 , D06M2400/01 , D06P1/653 , D06P5/04
摘要： The present invention is directed to a copolymer capable of forming a water- and oil-repellent agent that enables binding to textiles and other materials without the production of formaldehyde. The copolymer according to the present invention comprises a) a fluoroaliphatic radical-containing agent, (b) stearyl (meth)acrylate; (c) a chlorine-containing compound; and (d) a monomer selected from those that contain an anhydride functional group or are capable of forming an anhydride functional group. The present invention further provides a water and oil repellency-imparting composition for fibrous and other substrates, the composition comprising the above copolymer together with a catalyst, such as sodium hypophosphite, for forming anhydrides from the acid-containing monomers in the copolymer. The composition can further optionally comprise other additives such as, e.g., poly(acrylic acid); an extender; a softener; an antioxidant; a surfactant; and/or a plasticizer.
摘要翻译：本发明涉及一种能够形成防水防油剂的共聚物，其能够在不产生甲醛的情况下与纺织品和其它材料结合。根据本发明的共聚物包含a）含氟脂族基团的试剂，（b）（甲基）丙烯酸硬脂酯; （c）含氯化合物; 和（d）选自含有酸酐官能团或能够形成酸酐官能团的单体的单体。本发明还提供了一种用于纤维和其它基材的拒油拒油剂组合物，该组合物包含上述共聚物以及诸如次磷酸钠的催化剂，用于从共聚物中的含酸单体形成酸酐。组合物还可任选地包含其它添加剂，例如聚（丙烯酸）; 增长剂软化剂抗氧化剂表面活性剂; 和/或增塑剂。

9. 发明授权

US06379753B1 Modified textile and other materials and methods for their preparation 失效
标题翻译：改性纺织品等材料及其制备方法
公开(公告)号：US06379753B1
公开(公告)日：2002-04-30
申请号：US09274749
申请日：1999-03-23
申请人： David S. Soane , David A. Offord
发明人： David S. Soane , David A. Offord
IPC分类号： D06M1558
CPC分类号： C08B3/12 , C08B3/10 , C08B3/14 , C08B15/00 , D06M13/184 , D06M13/513 , D06M15/03 , D06M15/05 , D06M15/11 , D06M15/227 , D06M15/263 , D06M15/277 , D06M15/285 , D06M15/333 , D06M15/347 , D06M15/3562 , D06M15/643 , D06M23/00 , D06M23/005 , D06M2101/06 , D06M2101/12 , D06M2101/34 , D06M2400/01 , D06P1/653 , D06P5/04 , Y10T442/2164
摘要： Provided are compounds and methods for modifying a material to change properties of the material, as well as a variety of products obtained using the methods. The material which is modified may be, for example, a carbohydrate, and the modifiable functional groups on the material may be hydroxyls. Multifunctional molecules for use in modifying the surfaces of materials such as textile fibers, yarns and other fabrics made of or, including cotton, wool and nylon, are provided. The multifunctional molecules can include hydrophobic regions and/or hydrophilic regions. The multifunctional molecules also may include binding functional groups that permit either non-covalent or covalent binding to the material being modified, thus permitting the multifunctional molecule to form a non-covalent or covalent coating on the material. The methods and compounds disclosed herein may be used to modify materials to improve properties such as resistance, grease repellency, soil resistance permanent press properties, and quickness of drying.
摘要翻译：提供了用于改变材料以改变材料性质的化合物和方法，以及使用这些方法获得的各种产品。被修饰的材料可以是例如碳水化合物，并且材料上的可修饰的官能团可以是羟基。提供了用于改性材料表面的多功能分子，例如纺织纤维，纱线和由或由棉，羊毛和尼龙制成的其它织物。多官能分子可以包括疏水区和/或亲水区。多官能分子还可以包括结合官能团，其允许与被修饰的材料非共价或共价结合，从而允许多官能分子在材料上形成非共价或共价涂层。本文公开的方法和化合物可用于改性材料以改善诸如电阻，拒油性，耐土壤永久性压制性能和干燥速度等性能。

10. 发明授权

US5804252A Water- and oil repellent substrate and method of treatment 失效
标题翻译：拒水拒油基材和处理方法
公开(公告)号：US5804252A
公开(公告)日：1998-09-08
申请号：US625891
申请日：1996-04-01
申请人： Kazufumi Ogawa , Mamoru Soga
发明人： Kazufumi Ogawa , Mamoru Soga
IPC分类号： A61N1/365 , B05D1/18 , B05D5/08 , C09D4/00 , D06M15/657 , D06M23/00 , B05D3/02
CPC分类号： B82Y30/00 , A61N1/36514 , B05D1/185 , B82Y40/00 , C09D4/00 , D06M15/657 , D06M23/005 , B05D5/08 , Y10S428/913 , Y10T428/2918 , Y10T428/2933 , Y10T428/2962 , Y10T428/31663
摘要： A durable and extremely water- and oil repellent ultra thin film is formed on the surface of a substates such as glass, ceramics, fabrics, fur and cloth by a dehydrochlorination reaction between a functional group such as a hydroxyl group or an imino group on the surface of the substrate. The coating film of the material comprises a plurality of chlorosilyl groups was formed on the surface of the substrate by dipping and holding the substrate comprising functional groups on its surface in a solution prepared by dissolving a material comprising fluorocarbon groups and a plurality of chlorosilyl groups in a non-aqueous solvent and drying the substrate which is then taken out from the solution in a substantially moistureless or low moisture atomosphere and removing the non-aqueous solvent remaining on the substrate. Further, when the coating film is left in an atomosphere comprising moisture, i.e., humid air, the coating film is polymerized by a dehydrochlorination reaction between the coating film and the moisture in the atomosphere. The film is formed on the surface of the substrate containing hydroxyl groups, imino groups or carboxyl groups through --SiO-- bonds or --SiN
摘要翻译：通过在诸如羟基或亚氨基之类的官能团之间的脱氯化氢反应，在玻璃，陶瓷，织物，毛皮和布等基底的表面上形成耐久且极其防水和防油的超薄膜基板的表面。该材料的涂膜包括在基材的表面上形成多个氯甲硅烷基，在其表面上浸渍并保持包含官能团的基材，通过将包含氟烃基和多个氯代甲硅烷基的材料溶解在非水溶剂并干燥基材，然后将其从基本上无水或低湿气体的空气溶液中取出并除去残留在基材上的非水溶剂。此外，当涂膜留在包含湿气的空气即湿空气中时，涂膜通过涂膜和大气层中的水分之间的脱氯化氢反应而聚合。该薄膜通过-SiO键或-SiN <键在含有羟基，亚氨基或羧基的基材表面上形成。

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