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1. 发明授权

US11912805B2 Thermoplastic polymers synthesized from depolymerized lignin via free radical polymerization 有权
公开(公告)号：US11912805B2
公开(公告)日：2024-02-27
申请号：US16779018
申请日：2020-01-31
申请人： Iowa State University Research Foundation, Inc.
发明人： Eric W. Cochran , Xianglan Bai , Wangda Qu , Yuerui Huang , Yixin Luo
IPC分类号： C08F293/00 , C08J11/12 , C01B32/05 , D01F9/12 , D01F11/12
CPC分类号： C08F293/005 , C01B32/05 , C08J11/12 , D01F9/12 , D01F11/122 , D01F11/125 , C08F2438/01 , C08F2438/03 , C08J2397/02
摘要： One aspect of the present application relates to a method of synthesizing a thermoplastic polymer. This method includes providing a depolymerized lignin product comprising monomers and oligomers and producing lignin (meth)acrylate monomers and oligomers from the depolymerized lignin product. A thermoplastic lignin (meth)acrylate polymer is then formed by free radical polymerization of the lignin (meth)acrylate monomers and oligomers. The present application also relates to a branched chain thermoplastic lignin (meth)acrylate polymer which includes a chain transfer agent. The thermoplastic lignin based polymers of the present application can be used to prepare carbon fibers, and engineering thermoplastics. Mixtures of lignin (meth)acrylate monomers and oligomers are also disclosed.

2. 发明申请

US20180327935A1 PROCESS FOR GAS PHASE SURFACE TREATMENT 审中-公开
公开(公告)号：US20180327935A1
公开(公告)日：2018-11-15
申请号：US16045470
申请日：2018-07-25
申请人： CYTEC INDUSTRIES INC.
发明人： Shao C. Chiu
IPC分类号： D01F11/12 , D01F9/22 , D06M101/40
CPC分类号： D01F11/128 , D01F9/22 , D01F11/122 , D06M11/34 , D06M11/60 , D06M2101/40
摘要： A gas phase surface treatment for treating carbon fiber including (a) exposing a carbon fiber to a gaseous oxidizing atmosphere to form a modified carbon fiber with an oxidized fiber surface; followed by (b) exposing the oxidized fiber surface to a gaseous nitrogen-containing atmosphere to form a modified carbon fiber with a nitrogen-enriched surface, wherein the nitrogen-enriched surface exhibits an increase in surface nitrogen to surface carbon (N/C) ratio as compared to the surface of the carbon fiber prior to exposure at (a). Steps (a) and (b) are carried out continuously without any additional intervening surface treatment.

3. 发明申请

US20140234199A1 CARBON FIBER MANUFACTURING METHOD AND CARBON FIBER 有权
标题翻译：碳纤维制造方法和碳纤维
公开(公告)号：US20140234199A1
公开(公告)日：2014-08-21
申请号：US14235494
申请日：2012-08-02
申请人： Takayuki Kiriyama , Masahiro Hata , Hiroyuki Nakao , Nobuyuki Yamamoto , Masashi Shimahara , Kenichi Watanabe , Yasunori Murano , Hiroshi Tategaki
发明人： Takayuki Kiriyama , Masahiro Hata , Hiroyuki Nakao , Nobuyuki Yamamoto , Masashi Shimahara , Kenichi Watanabe , Yasunori Murano , Hiroshi Tategaki
IPC分类号： C01B31/02
CPC分类号： C01B32/05 , D01F11/122 , D06M11/34 , D06M23/06 , D06M2101/40 , D06M2200/50
摘要： Provided is a carbon fiber manufacturing method including a surface treatment step of ejecting an ozone solution in which ozone is dissolved in solvent from a fluid ejecting port toward a carbon fiber bundle and causing the ozone solution to pass between single fibers of the carbon fiber bundle so as to contact surfaces of the single fibers so that the surfaces of carbon fibers are treated by the ozone solution. Also, provided is a carbon fiber subjected to a surface treatment by the carbon fiber manufacturing method.
摘要翻译：本发明提供一种碳纤维的制造方法，其特征在于，包括将从溶液中溶解有臭氧的臭氧溶液从流体喷出口向碳纤维束排出并使臭氧溶液通过碳纤维束的单个纤维之间的表面处理工序，接触单个纤维的表面，使得碳纤维的表面被臭氧溶液处理。此外，提供了通过碳纤维制造方法进行表面处理的碳纤维。

4. 发明申请

US20120309887A1 CARBON NANOFIBER, METHOD FOR PRODUCTION THEREOF, METHOD FOR PRODUCTION OF CARBON FIBER COMPOSITE MATERIAL USING CARBON NANOFIBER, AND CARBON FIBER COMPOSITE MATERIAL 有权
标题翻译：碳纳米纤维，其制造方法，使用碳纳米纤维生产碳纤维复合材料的方法和碳纤维复合材料
公开(公告)号：US20120309887A1
公开(公告)日：2012-12-06
申请号：US13566577
申请日：2012-08-03
申请人： Toru NOGUCHI , Hiroyuki UEKI , Shigeki INUKAI , Kenji TAKEUCHI , Satoshi IINOU
发明人： Toru NOGUCHI , Hiroyuki UEKI , Shigeki INUKAI , Kenji TAKEUCHI , Satoshi IINOU
IPC分类号： C08K3/04 , C08L27/16 , C23C16/52 , C08L23/16 , B82Y40/00
CPC分类号： C08J3/203 , B82Y30/00 , B82Y40/00 , C01B32/16 , C01B32/168 , C01P2004/03 , C08J5/005 , C08J2321/00 , D01F11/122 , Y10T428/298
摘要： A method of producing a carbon fiber composite material includes a first step and a second step. The first step includes oxidizing first carbon nanofibers produced by a vapor growth method to obtain second carbon nanofibers having an oxidized surface. The second step includes mixing the second carbon nanofibers into an elastomer, and uniformly dispersing the carbon nanofibers in the elastomer by applying a shear force to obtain the carbon fiber composite material. The second carbon nanofibers obtained by the first step have a surface oxygen concentration measured by X-ray photoelectron spectroscopy (XPS) of 2.6 to 4.6 atm %.
摘要翻译：碳纤维复合材料的制造方法包括第一工序和第二工序。第一步包括氧化通过气相生长法产生的第一碳纳米纤维，得到具有氧化表面的第二碳纳米纤维。第二步包括将第二碳纳米纤维混合成弹性体，并通过施加剪切力将碳纳米纤维均匀分散在弹性体中以获得碳纤维复合材料。通过第一步获得的第二碳纳米纤维具有通过X射线光电子能谱（XPS）测量的2.6至4.6atm％的表面氧浓度。

5. 发明授权

US08263698B2 Carbon nanofiber, method for production thereof, method for production of carbon fiber composite material using carbon nanofiber, and carbon fiber composite material 有权
标题翻译：碳纳米纤维，其制造方法，使用碳纳米纤维的碳纤维复合材料的制造方法以及碳纤维复合材料
公开(公告)号：US08263698B2
公开(公告)日：2012-09-11
申请号：US12937415
申请日：2009-04-08
申请人： Toru Noguchi , Hiroyuki Ueki , Shigeki Inukai , Kenji Takeuchi , Satoshi Iinou
发明人： Toru Noguchi , Hiroyuki Ueki , Shigeki Inukai , Kenji Takeuchi , Satoshi Iinou
IPC分类号： C08K3/04 , C08K3/00
CPC分类号： C08J3/203 , B82Y30/00 , B82Y40/00 , C01B32/16 , C01B32/168 , C01P2004/03 , C08J5/005 , C08J2321/00 , D01F11/122 , Y10T428/298
摘要： A method of producing a carbon fiber composite material includes a first step and a second step. The first step includes oxidizing first carbon nanofibers produced by a vapor growth method to obtain second carbon nanofibers having an oxidized surface. The second step includes mixing the second carbon nanofibers into an elastomer, and uniformly dispersing the carbon nanofibers in the elastomer by applying a shear force to obtain the carbon fiber composite material. The second carbon nanofibers obtained by the first step have a surface oxygen concentration measured by X-ray photoelectron spectroscopy (XPS) of 2.6 to 4.6 atm %.
摘要翻译：碳纤维复合材料的制造方法包括第一工序和第二工序。第一步包括氧化通过气相生长法产生的第一碳纳米纤维，得到具有氧化表面的第二碳纳米纤维。第二步包括将第二碳纳米纤维混合成弹性体，并通过施加剪切力将碳纳米纤维均匀分散在弹性体中以获得碳纤维复合材料。通过第一步获得的第二碳纳米纤维具有通过X射线光电子能谱（XPS）测量的2.6至4.6atm％的表面氧浓度。

6. 发明授权

US07485678B2 Process for producing carbon nanotube reinforced composite material 失效
标题翻译：生产碳纳米管增强复合材料的工艺
公开(公告)号：US07485678B2
公开(公告)日：2009-02-03
申请号：US11088328
申请日：2005-03-23
申请人： Toshiyuki Ohashi , Keiichi Sato , Kazuhiro Miura
发明人： Toshiyuki Ohashi , Keiichi Sato , Kazuhiro Miura
IPC分类号： C08J3/20 , C08L101/00 , C08K7/24
CPC分类号： C08J5/04 , B82Y30/00 , C08J3/2053 , C08J5/005 , C08K7/24 , D01F11/122
摘要： An object is to provide a process for producing a carbon nanotube (CNT) reinforced composite material, wherein CNT is homogeneously dispersed in a resin to obtain the composite material having an excellent mechanical strength. Hydrophilic CNTs 12 are dispersed in a first solvent 11 to prepare a first dispersion liquid 13. The dispersion liquid 13 and a synthetic resin raw material 15 are added to a second solvent 14 and the resulting mixture is stirred to prepare a third dispersion liquid 17 where a second dispersion liquid 16 in which the synthetic resin raw material 15 is dissolved in the dispersion liquid 13 is dispersed in the solvent 14. The solvents 11 and 14 are removed from the dispersion liquid 17 to obtain a mixture of the hydrophilic CNTs 12 and the synthetic resin raw material 15. The mixture is molded to obtain the composite material in which the synthetic resin is reinforced with the hydrophilic CNTs 12. The second solvent 14 has smaller solubility of the synthetic resin raw material 15 than that of the solvent 11, is substantially not compatible to the solvent 11, and has volume larger than that of the solvent 11. The dispersion liquid 17 is sprayed on a substrate and the solvents 11 and 14 are removed to obtain the mixture and simultaneously to conduct molding of the mixture.
摘要翻译：本发明的目的是提供一种碳纳米管（CNT）增强复合材料的制造方法，其中，CNT均匀地分散在树脂中，得到机械强度优异的复合材料。将亲水性CNT 12分散在第一溶剂11中以制备第一分散液13.将分散液13和合成树脂原料15加入到第二溶剂14中，并将所得混合物搅拌以制备第三分散液17，将合成树脂原料15溶解在分散液13中的第二分散液16分散在溶剂14中。从分散液17中除去溶剂11和14，得到亲水性CNT 12和合成树脂原料15.将该混合物成形，得到合成树脂用亲水性CNT 12增强的复合材料。第二溶剂14的合成树脂原料15的溶解度比溶剂11的溶解度小，为与溶剂11基本上不相容，并且体积大于溶剂11的体积。将分散液17喷涂在基材上，并将溶剂11和14 e去除以获得混合物并同时进行混合物的模制。

7. 发明授权

US07470417B2 Ozonation of carbon nanotubes in fluorocarbons 有权
标题翻译：碳纳米管在碳氟化合物中的臭氧化
公开(公告)号：US07470417B2
公开(公告)日：2008-12-30
申请号：US11285232
申请日：2005-11-22
申请人： Kirk J. Ziegler , Jonah Shaver , Robert H. Hauge , Irene Morin Marek, legal representative
发明人： Richard E. Smalley
IPC分类号： C09C1/56 , B82B3/00
CPC分类号： B82Y30/00 , B82Y40/00 , C01B32/174 , C01B2202/02 , D01F11/122 , Y10S977/847
摘要： The present invention is generally directed to methods of ozonating CNTs in fluorinated solvents (fluoro-solvents), wherein such methods provide a less dangerous alternative to existing ozonolysis methods. In some embodiments, such methods comprise the steps of: (a) dispersing carbon nanotubes in a fluoro-solvent to form a dispersion; and (b) reacting ozone with the carbon nanotubes in the dispersion to functionalize the sidewalls of the carbon nanotubes and yield functionalized carbon nanotubes with oxygen-containing functional moieties. In some such embodiments, the fluoro-solvent is a fluorocarbon solvent, such as a perfluorinated polyether.
摘要翻译：本发明一般涉及在氟化溶剂（氟溶剂）中臭氧化碳纳米管的方法，其中这些方法对现有的臭氧分解方法提供了较不危险的替代方法。在一些实施方案中，这些方法包括以下步骤：（a）将碳纳米管分散在氟溶剂中以形成分散体; 和（b）使臭氧与分散体中的碳纳米管反应，使碳纳米管的侧壁官能化，并产生具有含氧官能团的官能化碳纳米管。在一些这样的实施方案中，氟 - 溶剂是氟烃溶剂，例如全氟化聚醚。

8. 发明申请

US20080152573A1 METHOD FOR PRODUCING CARBON NANOTUBES, METHOD FOR PRODUCING LIQUID DISPERSION THEREOF AND OPTICAL PRODUCT 审中-公开
标题翻译：生产碳纳米管的方法，生产液体分散体的方法和光学产品
公开(公告)号：US20080152573A1
公开(公告)日：2008-06-26
申请号：US11613895
申请日：2006-12-20
申请人： Noriyuki Juni , Amane Mochizuki , Toshitaka Nakamura , Bin Gu , Hiroaki Miyagawa
发明人： Noriyuki Juni , Amane Mochizuki , Toshitaka Nakamura , Bin Gu , Hiroaki Miyagawa
IPC分类号： D01F9/12
CPC分类号： D01F11/122 , B01J19/123 , B01J2219/0886 , B82Y10/00 , B82Y30/00 , B82Y40/00 , C01B32/174 , C01B2202/02 , C01B2202/28 , C01B2202/34 , C01B2202/36 , D01F11/16 , H01L51/0049
摘要： A method for producing dispersible carbon nanotubes of the invention comprises subjecting single-walled carbon nanotubes to UV treatment in the presence of ozone such that carboxyl groups are introduced into the single-walled carbon nanotubes and that the single-walled carbon nanotubes are fragmented. A carbon nanotubes obtained by the method has a good dispersibility.
摘要翻译：本发明的分散性碳纳米管的制造方法包括在臭氧存在下对单壁碳纳米管进行紫外线处理，使得羧基被引入到单壁碳纳米管中，并且单壁碳纳米管被分散。通过该方法获得的碳纳米管具有良好的分散性。

9. 发明授权

US06565927B1 Method for treatment of surfaces with ultraviolet light 有权
标题翻译：用紫外线处理表面的方法
公开(公告)号：US06565927B1
公开(公告)日：2003-05-20
申请号：US09287978
申请日：1999-04-07
申请人： Lawrence T. Drzal , Narasimharao Dontula , Richard L. Schalek , Alekh S. Bhurke , Michael J. Rich , Laura M. Fisher , Ming Xie
发明人： Lawrence T. Drzal , Narasimharao Dontula , Richard L. Schalek , Alekh S. Bhurke , Michael J. Rich , Laura M. Fisher , Ming Xie
IPC分类号： C08F246
CPC分类号： B29C59/16 , B05D3/062 , B05D3/063 , B05D3/064 , B05D3/101 , B05D3/102 , B05D3/104 , B29C2035/0827 , C03C25/6226 , C04B41/0045 , D01F11/122 , G21K5/10 , H01B1/04
摘要： A method using irradiation with optical light having a wavelength of 160 to 500 nanometers without higher wavelengths with cooling of the surface during the irradiation to modify the surface (12A, 104A, 202A, 304A, 402A, 502A) of a substrate (12, 104, 202, 304, 402, 502) is described. The light is filtered or the lamp (24, 106, 212, 306, 510) is restricted to the limited range to avoid the affects of the higher spectra. The light can be pulsed or continuous. The method is significantly enhanced by the presence of water (14, 124, 204, 306, 410, 508) on the surface, preferably also in the presence of ozone in the water. The treated surfaces are more paintable and bondable.
摘要翻译：一种在照射期间使用具有160-500纳米波长的光，而不具有更高波长并且冷却表面以改变基底（12,104）的表面（12A，104A，202A，304A，402A，502A）的方法的方法，202,304,402,502）。光被过滤或灯（24,106,212,306,510）被限制在有限的范围以避免较高光谱的影响。光可以是脉冲或连续的。该方法通过表面上存在水（14,124,204,306,410,508）而显着增强，优选地也存在于水中的臭氧存在下。经处理的表面更可涂漆和粘合。

10. 发明申请

US20030035769A1 Carbide and oxycarbide based compositions, rigid porous structures including the same, methods of making and using the same 失效
标题翻译：基于碳化物和碳氧化物的组合物，包括其的刚性多孔结构，制备和使用它们的方法
公开(公告)号：US20030035769A1
公开(公告)日：2003-02-20
申请号：US10170269
申请日：2002-06-11
申请人： Hyperion Catalysis International, Inc.
发明人： David Moy , Chunning Niu , Jun Ma , James M. Willey
IPC分类号： B01J027/22 , B01J021/18 , D01F009/12
CPC分类号： B82Y30/00 , B01J21/18 , B01J27/22 , B01J35/023 , B82Y40/00 , C01B32/168 , C01B32/907 , C01B2202/36 , C01P2002/72 , C01P2004/03 , C01P2004/04 , C01P2004/13 , C01P2004/50 , C01P2004/64 , C01P2004/80 , C01P2004/82 , C01P2006/10 , C01P2006/14 , C01P2006/60 , C01P2006/80 , C30B23/00 , C30B29/605 , D01F9/12 , D01F11/122 , Y10S977/737 , Y10S977/762 , Y10S977/895 , Y10T428/249962 , Y10T428/249967 , Y10T428/25 , Y10T428/2918 , Y10T428/292
摘要： Compositions including oxycarbide-based nanorods and/or carbide-based nanorods and/or carbon nanotubes bearing carbides and oxycarbides and methods of making the same are provided. Rigid porous structures including oxycarbide-based nanorods and/or carbide based nanorods and/or carbon nanotubes bearing carbides and oxycarbides and methods of making the same are also provided. The compositions and rigid porous structures of the invention can be used either as catalyst and/or catalyst supports in fluid phase catalytic chemical reactions. Processes for making supported catalyst for selected fluid phase catalytic reactions are also provided. The fluid phase catalytic reactions catalyzed include hydrogenation, hydrodesulfurisation, hydrodenitrogenation, hydrodemetallisation, hydrodeoxigenation, hydrodearomatization, dehydrogenation, hydrogenolysis, isomerization, alkylation, dealkylation and transalkylation.
摘要翻译：提供包括基于碳氧化物的纳米棒和/或碳化物基纳米棒和/或碳纳米管和碳氧化物的组合物及其制备方法。还提供了包括基于碳氧化物的纳米棒和/或碳化物基纳米棒和/或含有碳化物和碳氧化物的碳纳米管的刚性多孔结构及其制备方法。本发明的组合物和刚性多孔结构可用作流化相催化化学反应中的催化剂和/或催化剂载体。还提供了用于制备选择的流化相催化反应的负载型催化剂的方法。催化的流相催化反应包括氢化，加氢脱硫，加氢脱氮，加氢脱金属，加氢脱氧，氢化脱氢，脱氢，氢解，异构化，烷基化，脱烷基化和烷基转移。

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