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1. 发明授权

US09527768B2 Method of making inorganic, metal oxide spheres using microstructured molds 有权
公开(公告)号：US09527768B2
公开(公告)日：2016-12-27
申请号：US14788863
申请日：2015-07-01
申请人： 3M INNOVATIVE PROPERTIES COMPANY
发明人： David C. Kramlich , John L. Vandenberg , Matthew H. Frey , Scott R. Culler , Kathleen M. Schakel-Carlson
IPC分类号： C03C12/02 , C03B19/10 , G02B5/128 , C08K3/22 , C08K3/26 , C08K3/34 , C08K3/36 , C08K3/38
CPC分类号： C03C12/02 , C03B19/10 , C03B19/102 , C03B19/108 , C08K3/22 , C08K3/26 , C08K3/34 , C08K3/36 , C08K3/38 , C08K2003/2241 , C08K2003/265 , C08K2003/387 , G02B5/128 , Y10T428/24421
摘要： A process for making inorganic, metal oxide spheres that includes exposing solidified, molded microparticles that include a glass precursor composition to a temperature sufficient to transform the molded microparticles into molten glass and cooling the molten glass to form inorganic, metal oxide spheres.

2. 发明申请

US20070099786A1 Tumbled, Polished, Vibrated Broken Tempered Glass Pieces 审中-公开
标题翻译：翻滚，抛光，振动破碎的钢化玻璃片
公开(公告)号：US20070099786A1
公开(公告)日：2007-05-03
申请号：US11625195
申请日：2007-01-19
申请人： Edgar Jaunzemis , Claudia Jaunzemis
发明人： Edgar Jaunzemis , Claudia Jaunzemis
IPC分类号： C03C3/00 , B24B1/00
CPC分类号： B24B31/10 , B24B31/06 , C03B19/10 , C03B27/04 , C03C1/002 , C03C19/00 , F24B1/1808 , F24B1/191 , Y10T428/315
摘要： An invention is provided for creating smoothed, heat-treated glass fragments. The invention includes placing a plurality of heat-treated glass fragments into a tumbling or vibrating apparatus. Each heat-treated glass fragment is formed from glass that has been heated to a temperature of at least 1000° Fahrenheit and rapidly cooled to a temperature below 700° Fahrenheit. The plurality of glass fragments are then tumbled or vibrated for a predetermined period of time such that surfaces of the heat-treated glass fragments are smoother than prior to tumbling. The glass fragments are thereafter removed from the tumbling apparatus, resulting in smoothed, heat-treated glass fragments that are suitable for direct handling without hand protection.
摘要翻译：提供了一种用于产生平滑的经热处理的玻璃碎片的发明。本发明包括将多个经热处理的玻璃碎片放置在翻滚或振动装置中。每个经热处理的玻璃碎片由已被加热至至少1000华氏度的温度并快速冷却至低于700华氏度的玻璃形成。然后将多个玻璃碎片翻滚或振动预定时间段，使得经热处理的玻璃碎片的表面比翻滚前更平滑。玻璃碎片此后从转动装置中取出，产生平滑的，经热处理的玻璃碎片，适合直接处理而无需手部保护。

3. 发明授权

US4902450A Multi-element spherical shell generation 失效
标题翻译：多元素球壳产生
公开(公告)号：US4902450A
公开(公告)日：1990-02-20
申请号：US250195
申请日：1988-09-28
申请人： Andrew D. Morrison
发明人： Andrew D. Morrison
IPC分类号： A61J3/07 , B01J13/04 , B22F1/00 , B22F9/08 , C03B19/10
CPC分类号： B22F1/0051 , A61J3/07 , B01J13/04 , B22F9/08 , C03B19/10 , Y10S425/804
摘要： A nozzle assembly in a multi-element spherical shell generation system includes first and second side-by-side spaced apart nozzles and a web portion extending between and connecting the nozzles. The first nozzle has an inner orifice adapted to discharge a first filler material and an outer annular orifice separated from and defined in concentric relation about the inner orifice and adapted to discharge a first shell material. The second nozzle has an inner orifice adapted to discharge a second filler material and an outer annular orifice separated from and defined in concentric relation about the inner orifice and adapted to discharge a second shell material. A multi-element spherical shell can be formed through employment of the nozzle assembly by merger with one another after discharge from the outer orifices of the nozzles of a pair of adjacent annular streams of liquid or molten shell wall material of different compositions and encapsulation by the mixed shell wall materials of a common encapsulated core fluids also simultaneously discharged by the inner orifices nozzles. On the other hand, the pair of encapsulating streams of shell wall material can be of the same material which merge together and encapsulate core fluids of different compositions which will merge together after discharge from the nozzles.
摘要翻译：多元件球形壳体生成系统中的喷嘴组件包括第一和第二并排间隔开的喷嘴和在喷嘴之间延伸并连接喷嘴的腹板部分。第一喷嘴具有适于排出第一填充材料的内孔和从内孔分离并以同心关系限定的外环形孔，并适于排出第一壳材料。第二喷嘴具有适于排出第二填充材料的内孔和从内孔分离并且以同心关系限定的外环形孔，并适于排出第二壳材料。多元件球形壳体可以通过在从一对相邻的不同组成的液体或熔融壳体壁材料的环形流的喷嘴的外部喷嘴排出之后彼此并入而通过使用喷嘴组件而形成，并且由共同封装的核心流体的混合壳壁材料也同时由内孔喷嘴排出。另一方面，壳壁材料的一对封装流可以是相同的材料，其合并在一起并且包封不同组成的芯流体，其在从喷嘴排出后将合并在一起。

4. 发明授权

US4670035A Method and apparatus for generating microshells of refractory materials 失效
$Method and apparatus for generating microshells of refractory materials$
标题翻译：用于生成耐火材料微壳的方法和装置
公开(公告)号：US4670035A
公开(公告)日：1987-06-02
申请号：US751077
申请日：1985-07-02
申请人： Mark C. Lee , Christopher Schilling , George O. Ladner, Jr. , Taylor G. Wang
发明人： Mark C. Lee , Christopher Schilling , George O. Ladner, Jr. , Taylor G. Wang
IPC分类号： B01J13/04 , B22D25/02 , B22F1/00 , B22F9/08 , C03B19/10
CPC分类号： B22F1/0051 , B01J13/04 , B22D25/02 , B22F9/08 , C03B19/10
摘要： A system is described for forming accurately spherical and centered fluid-filled shells, especially of high melting temperature material. Material which is to form the shells is placed in a solid form in a container, and the material is rapidly heated to a molten temperature to avoid recrystallization and the possible generation of unwanted microbubbles in the melt. Immediately after the molten shells are formed, they drop through a drop tower whose upper end is heated along a distance of at least one foot to provide time for dissipation of surface waves on the shells while they cool to a highly viscous, or just above melting temperature so that the bubble within the shell will not rise and become off centered. The rest of the tower is cryogenically cooled to cool the shell to a solid state.
摘要翻译：描述了一种系统，用于形成精确的球形和居中的流体填充的壳，特别是高熔点材料。将形成壳的材料以固体形式放置在容器中，并将材料快速加热至熔融温度，以避免重结晶并在熔体中产生不想要的微泡。在熔融壳形成之后，它们立即通过一个下塔，它的上端被加热至少一英尺的距离，以便在壳体上散发表面波的时间，同时它们冷却到高粘度或刚好高于熔化使得壳内的气泡不会升高而变得偏心。塔的其余部分被低温冷却以将壳冷却至固态。

5. 发明授权

US09108874B2 Method of making inorganic, metal oxide spheres using microstructured molds 有权
标题翻译：使用微结构模具制备无机，金属氧化物球体的方法
公开(公告)号：US09108874B2
公开(公告)日：2015-08-18
申请号：US14228790
申请日：2014-03-28
申请人： 3M INNOVATIVE PROPERTIES COMPANY
发明人： David C. Kramlich , John L. Vandenberg , Matthew H. Frey , Scott R. Culler , Kathleen M. Schakel-Carlson
IPC分类号： C03C11/00 , C03C12/00 , C03B19/06 , C03B19/10 , C03C12/02 , G02B5/128
CPC分类号： C03C12/02 , C03B19/10 , C03B19/102 , C03B19/108 , C08K3/22 , C08K3/26 , C08K3/34 , C08K3/36 , C08K3/38 , C08K2003/2241 , C08K2003/265 , C08K2003/387 , G02B5/128 , Y10T428/24421
摘要： A process for making inorganic, metal oxide spheres that includes exposing solidified, molded microparticles that include a glass precursor composition to a temperature sufficient to transform the molded microparticles into molten glass and cooling the molten glass to form inorganic, metal oxide spheres.
摘要翻译：一种制备无机金属氧化物球体的方法，其包括使包含玻璃前体组合物的固化的模塑微粒暴露于足以将模制的微粒转化为熔融玻璃的温度，并冷却熔融玻璃以形成无机的金属氧化物球体。

6. 发明授权

US08419505B2 Tumbled, polished, vibrated broken tempered glass pieces 失效
标题翻译：翻滚，抛光，振动破碎的钢化玻璃片
公开(公告)号：US08419505B2
公开(公告)日：2013-04-16
申请号：US13180434
申请日：2011-07-11
申请人： Edgar Edward Jaunzemis , Claudia Sue Jaunzemis
发明人： Edgar Edward Jaunzemis , Claudia Sue Jaunzemis
IPC分类号： B24B1/00
CPC分类号： B24B31/10 , B24B31/06 , C03B19/10 , C03B27/04 , C03C1/002 , C03C19/00 , F24B1/1808 , F24B1/191 , Y10T428/315
摘要： An invention is provided for creating smoothed, heat-treated glass fragments. The invention includes placing a plurality of heat-treated glass fragments into a tumbling or vibrating apparatus. Each heat-treated glass fragment is formed from glass that has been heated to a temperature of at least 1000° Fahrenheit and rapidly cooled to a temperature below 700° Fahrenheit. The plurality of glass fragments are then tumbled or vibrated for a predetermined period of time such that surfaces of the heat-treated glass fragments are smoother than prior to tumbling. The glass fragments are thereafter removed from the tumbling apparatus, resulting in smoothed, heat-treated glass fragments that are suitable for direct handling without hand protection.
摘要翻译：提供了一种用于产生平滑的经热处理的玻璃碎片的发明。本发明包括将多个经热处理的玻璃碎片放置在翻滚或振动装置中。每个经热处理的玻璃碎片由已被加热至至少1000华氏度的温度并快速冷却至低于700华氏度的玻璃形成。然后将多个玻璃碎片翻滚或振动预定时间段，使得经热处理的玻璃碎片的表面比翻转前更平滑。玻璃碎片此后从转动装置中取出，产生平滑的，经热处理的玻璃碎片，适合直接处理而无需手部保护。

7. 发明申请

US20080041103A1 METHOD OF MAKING INORGANIC, METAL OXIDE SPHERES USING MICROSTRUCTURED MOLDS 有权
标题翻译：使用微结构的方法制造无机，金属氧化物球体的方法
公开(公告)号：US20080041103A1
公开(公告)日：2008-02-21
申请号：US11465848
申请日：2006-08-21
申请人： David C. Kramlich , John L. Vandenberg , Matthew H. Frey , Scott R. Culler , Kathleen M. Schakel-Carlson
发明人： David C. Kramlich , John L. Vandenberg , Matthew H. Frey , Scott R. Culler , Kathleen M. Schakel-Carlson
IPC分类号： C03B19/09 , C03B19/06 , C03B19/01
CPC分类号： C03C12/02 , C03B19/10 , C03B19/102 , C03B19/108 , C08K3/22 , C08K3/26 , C08K3/34 , C08K3/36 , C08K3/38 , C08K2003/2241 , C08K2003/265 , C08K2003/387 , G02B5/128 , Y10T428/24421
摘要： A process for making inorganic, metal oxide spheres that includes exposing solidified, molded microparticles that include a glass precursor composition to a temperature sufficient to transform the molded microparticles into molten glass and cooling the molten glass to form inorganic, metal oxide spheres.
摘要翻译：一种制备无机金属氧化物球体的方法，其包括使包含玻璃前体组合物的固化的模塑微粒暴露于足以将模制的微粒转化为熔融玻璃的温度，并冷却熔融玻璃以形成无机的金属氧化物球体。

8. 发明申请

US20060101854A1 Tumbled, polished, vibrated broken tempered glass pieces 无效
公开(公告)号：US20060101854A1
公开(公告)日：2006-05-18
申请号：US11319957
申请日：2005-12-28
申请人： Edgar Jaunzemis , Claudia Jaunzemis
发明人： Edgar Jaunzemis , Claudia Jaunzemis
IPC分类号： C03B23/00
CPC分类号： B24B31/10 , B24B31/06 , C03B19/10 , C03B27/04 , C03C1/002 , C03C19/00 , F24B1/1808 , F24B1/191 , Y10T428/315
摘要： An invention is provided for creating smoothed, heat-treated glass fragments. The invention includes placing a plurality of heat-treated glass fragments into a tumbling or vibrating apparatus. Each heat-treated glass fragment is formed from glass that has been heated to a temperature of at least 1000° Fahrenheit and rapidly cooled to a temperature below 700° Fahrenheit. The plurality of glass fragments are then tumbled or vibrated for a predetermined period of time such that surfaces of the heat-treated glass fragments are smoother than prior to tumbling. The glass fragments are thereafter removed from the tumbling apparatus, resulting in smoothed, heat-treated glass fragments that are suitable for direct handling without hand protection.

9. 发明授权

US4485834A Atomization die and method for atomizing molten material 失效
标题翻译：雾化模具和雾化熔融材料的方法
公开(公告)号：US4485834A
公开(公告)日：1984-12-04
申请号：US327698
申请日：1981-12-04
申请人： Nicholas J. Grant
发明人： Nicholas J. Grant
IPC分类号： B22F9/08 , C03B19/01 , C03B19/10 , C03B37/06 , C23C4/12 , D04H1/56 , B22D23/00
CPC分类号： B22F9/082 , C03B19/01 , C03B19/10 , C03B37/06 , C23C4/123 , D04H1/56 , B22F2009/088 , B22F2998/00 , B22F2999/00
摘要： The die comprises at least one set of opposed linearly configurated die elements spaced in substantially parallel relationship to define a longitudinally configurated die space therebetween dimensioned to pass therethrough a sheet of the molten material, the die elements defining a nozzle assembly characterized by oppositely disposed orifice-bearing surfaces. Each of the linear die elements has a gas pressure manifold for receiving atomizing gas under superatmospheric pressure, each of the oppositely disposed nozzle-defining surfaces having at least one array of orifices extending therealong and embracing each side of the longitudinally configurated die space defined by the oppositely disposed linear die elements. Conduits are provided for communicating the orifices with the gas manifold, the array of orifices in each of the die elements being convergently directed towards the other through an included angle of, for example, 40.degree. for directing atomizing gas against a predetermined focal region on a sheet of molten material passing through the longitudinal die space, each of the orifice conduits connected to resonating cavities for generating ultrasonic, high frequency shock waves for one-step disintegration of the sheet of molten material at said focal region into fine atomized particles which later solidify. The uses include the production of dry powders and liquid dynamically densified shapes, such as ingots, forging and rolling preforms and highly dense compacts.
摘要翻译：模具包括至少一组相对的线性构造的模具元件，其基本平行的关系间隔开，以限定其间尺寸设计成穿过熔融材料片材的纵向配置的模具空间，模具元件限定喷嘴组件，其特征在于相对设置的孔口 - 轴承表面。每个线性模具元件具有用于在超大气压力下接收雾化气体的气体压力歧管，每个相对设置的喷嘴限定表面具有至少一个孔阵列，其沿着其延伸并且包围由所述纵向配置的模具空间的每一侧限定相对设置的线性模具元件。提供管道用于将孔与气体歧管连通，每个模具元件中的孔的阵列通过例如40°的夹角会聚地指向另一个，用于将雾化气体引导到预定焦点区域上熔融材料片通过纵向模具空间，每个孔口导管连接到谐振腔，用于产生超声波高频冲击波，用于在所述焦点区域将熔融材料片一步分解成稍微固化的细小雾化颗粒。这些用途包括生产干燥粉末和液体动态致密化的形状，例如锭，锻造和轧制预成型件以及高度致密的压坯。

10. 发明授权

US3617333A Process for flotation treatment of glass beads 失效
标题翻译：玻璃珠的浮选处理工艺
公开(公告)号：US3617333A
公开(公告)日：1971-11-02
申请号：US3617333D
申请日：1968-10-30
申请人： GEN STEEL IND INC
发明人： BROWN PERVIS
IPC分类号： C03B19/10 , C03C17/28 , C03C17/22
CPC分类号： C03C17/28 , C03B19/10 , Y10T428/2993 , Y10T428/2996
摘要： A process for surface treating or sizing glass beads and similar discrete particles such as silicon carbide, sand and the like, with a chemical adhesion promoter to provide the glass beads with water repellent and organic solvent repellent properties. The surface treatment improves adhesion of the bead to the substrate in which it is embedded, which may be paint or various types of organic binders. Because of the hydrophobic and oleophobic properties provided through repellent surface treatment, the beads do not sink through the binder but rather are floated thereon, and the top surfaces are exposed to provide for reflexreflective properties. The surface treating or sizing agent is an organo-titanium derivative, including alkyl-titanates, titaniumacylates, and titanium-chelates, in which between two and four of the coordination positions of the titanium are occupied by alkyl or aromatic groups.

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