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1. 发明授权

US07713506B2 Metal aminoboranes 失效
标题翻译：金属氨基硼烷
公开(公告)号：US07713506B2
公开(公告)日：2010-05-11
申请号：US12151575
申请日：2008-05-07
申请人： Anthony K. Burrell , Benjamin J. Davis , David L. Thorn , John C. Gordon , R. Thomas Baker , Troy Allen Semelsberger , William Tumas , Himashinie Vichalya Kaviraj Diyabalanage , Roshan P. Shrestha
发明人： Anthony K. Burrell , Benjamin J. Davis , David L. Thorn , John C. Gordon , R. Thomas Baker , Troy Allen Semelsberger , William Tumas , Himashinie Vichalya Kaviraj Diyabalanage , Roshan P. Shrestha
IPC分类号： C01B35/00 , C07F5/02
CPC分类号： H01M8/0606 , C01B3/0026 , C01B3/0031 , C01B6/19 , Y02E60/327
摘要： Metal aminoboranes of the formula M(NH2BH3)n have been synthesized. Metal aminoboranes are hydrogen storage materials. Metal aminoboranes are also precursors for synthesizing other metal aminoboranes. Metal aminoboranes can be dehydrogenated to form hydrogen and a reaction product. The reaction product can react with hydrogen to form a hydrogen storage material. Metal aminoboranes can be included in a kit.
摘要翻译：已经合成了式M（NH 2 BH 3）n的金属氨基硼烷。金属氨基硼烷是储氢材料。金属氨基硼烷也是合成其它金属氨基硼烷的前体。金属氨基硼烷可以脱氢形成氢气和反应产物。反应产物可与氢反应形成储氢材料。金属氨基硼烷可以包含在试剂盒中。

2. 发明申请

US20090297423A1 ENERGY EFFICIENT SYNTHESIS OF BORANES 失效
标题翻译：能量有效地合成硼
公开(公告)号：US20090297423A1
公开(公告)日：2009-12-03
申请号：US12533736
申请日：2009-07-31
申请人： David L. Thorn , William Tumas , Daniel E. Schwarz , Anthony K. Burrell
发明人： David L. Thorn , William Tumas , Daniel E. Schwarz , Anthony K. Burrell
IPC分类号： C01B6/10 , C08F8/42 , C08G77/00 , C08G79/02 , C08G79/08 , C08G73/00
CPC分类号： C01B6/15 , C01B6/19 , C01B35/061
摘要： The reaction of halo-boron compounds (B—X compounds, compounds having one or more boron-halogen bonds) with silanes provides boranes (B—H compounds, compounds having one or more B—H bonds) and halosilanes. Inorganic hydrides, such as surface-bound silane hydrides (Si—H) react with B—X compounds to form B—H compounds and surface-bound halosilanes. The surface bound halosilanes are converted back to surface-bound silanes electrochemically. Halo-boron compounds react with stannanes (tin compounds having a Sn—H bond) to form boranes and halostannanes (tin compounds having a Sn—X bond). The halostannanes are converted back to stannanes electrochemically or by the thermolysis of Sn-formate compounds. When the halo-boron compound is BCl3, the B—H compound is B2H6, and where the reducing potential is provided electrochemically or by the thermolysis of formate.
摘要翻译：卤代硼化合物（B-X化合物，具有一个或多个硼 - 卤键的化合物）与硅烷的反应提供硼烷（B-H化合物，具有一个或多个B-H键的化合物）和卤代硅烷。无机氢化物，例如表面结合的硅烷氢化物（Si-H）与B-X化合物反应以形成B-H化合物和表面结合的卤代硅烷。表面结合的卤代硅烷在电化学上转化回表面结合的硅烷。卤代硼化合物与锡烷（具有Sn-H键的锡化合物）反应形成硼烷和卤代烷（具有Sn-X键的锡化合物）。卤代烷腈通过电化学方法或通过Sn-甲酸酯化合物的热解转化回锡烷。当卤代硼化合物为BCl 3时，B-H化合物为B 2 H 6，并且其电还原电位或通过甲酸盐的热解提供还原电位。

3. 发明授权

US07837852B2 Energy efficient synthesis of boranes 失效
标题翻译：能量高效合成硼烷
公开(公告)号：US07837852B2
公开(公告)日：2010-11-23
申请号：US12533736
申请日：2009-07-31
申请人： David L. Thorn , William Tumas , Daniel E. Schwarz , Anthony K. Burrell
发明人： David L. Thorn , William Tumas , Daniel E. Schwarz , Anthony K. Burrell
IPC分类号： C01B6/00
CPC分类号： C01B6/15 , C01B6/19 , C01B35/061
摘要： The reaction of halo-boron compounds (B—X compounds, compounds having one or more boron-halogen bonds) with silanes provides boranes (B—H compounds, compounds having one or more B—H bonds) and halosilanes. Inorganic hydrides, such as surface-bound silane hydrides (Si—H) react with B—X compounds to form B—H compounds and surface-bound halosilanes. The surface bound halosilanes are converted back to surface-bound silanes electrochemically. Halo-boron compounds react with stannanes (tin compounds having a Sn—H bond) to form boranes and halostannanes (tin compounds having a Sn—X bond). The halostannanes are converted back to stannanes electrochemically or by the thermolysis of Sn-formate compounds. When the halo-boron compound is BCl3, the B—H compound is B2H6, and where the reducing potential is provided electrochemically or by the thermolysis of formate.
摘要翻译：卤代硼化合物（B-X化合物，具有一个或多个硼 - 卤键的化合物）与硅烷的反应提供硼烷（B-H化合物，具有一个或多个B-H键的化合物）和卤代硅烷。无机氢化物，例如表面结合的硅烷氢化物（Si-H）与B-X化合物反应以形成B-H化合物和表面结合的卤代硅烷。表面结合的卤代硅烷在电化学上转化回表面结合的硅烷。卤代硼化合物与锡烷（具有Sn-H键的锡化合物）反应形成硼烷和卤代烷（具有Sn-X键的锡化合物）。卤代烷腈通过电化学方法或通过Sn-甲酸酯化合物的热解转化回锡烷。当卤代硼化合物为BCl 3时，B-H化合物为B 2 H 6，并且其还原电位通过电化学方法或通过甲酸盐的热解提供。

4. 发明申请

US20070189950A1 Energy efficient synthesis of boranes 审中-公开
标题翻译：能量高效合成硼烷
公开(公告)号：US20070189950A1
公开(公告)日：2007-08-16
申请号：US11704494
申请日：2007-02-08
申请人： David Thorn , William Tumas , Daniel Schwarz , Anthony Burrell
发明人： David Thorn , William Tumas , Daniel Schwarz , Anthony Burrell
IPC分类号： C01B35/14 , C01B35/06
CPC分类号： C01B6/15 , C01B6/19 , C01B35/061
摘要： The reaction of halo-boron compounds (B—X compounds, compounds having one or more boron-halogen bonds) with silanes provides boranes (B—H compounds, compounds having one or more B—H bonds) and halosilanes. Inorganic hydrides, such as surface-bound silane hydrides (Si—H) react with B—X compounds to form B—H compounds and surface-bound halosilanes. The surface bound halosilanes are converted back to surface-bound silanes electrochemically. Halo-boron compounds react with stannanes (tin compounds having a Sn—H bond) to form boranes and halostannanes (tin compounds having a Sn—X bond). The halostannanes are converted back to stannanes electrochemically or by the thermolysis of Sn-formate compounds. When the halo-boron compound is BCl3, the B—H compound is B2H6, and where the reducing potential is provided electrochemically or by the thermolysis of formate.
摘要翻译：卤代硼化合物（B-X化合物，具有一个或多个硼 - 卤键的化合物）与硅烷的反应提供硼烷（B-H化合物，具有一个或多个B-H键的化合物）和卤代硅烷。无机氢化物，例如表面结合的硅烷氢化物（Si-H）与B-X化合物反应以形成B-H化合物和表面结合的卤代硅烷。表面结合的卤代硅烷在电化学上转化回表面结合的硅烷。卤代硼化合物与锡烷（具有Sn-H键的锡化合物）反应形成硼烷和卤代烷（具有Sn-X键的锡化合物）。卤代烷腈通过电化学方法或通过Sn-甲酸酯化合物的热解转化回锡烷。当卤代硼化合物为BCl 3时，BH化合物是B 2 H 6 N，并且其中还原电位是电化学或由甲酸盐的热解。

5. 发明授权

US08920760B2 Metal amidoborane compositions and processes for their preparation 有权
标题翻译：金属氨基硼烷组合物及其制备方法
公开(公告)号：US08920760B2
公开(公告)日：2014-12-30
申请号：US13392457
申请日：2010-04-13
申请人： Viktor Balema , Kanth Josyula , Guolin Xu , Nathaniel Wallock , Scott Batcheller , Peng Gao , Shashi Jasty
发明人： Viktor Balema , Kanth Josyula , Guolin Xu , Nathaniel Wallock , Scott Batcheller , Peng Gao , Shashi Jasty
IPC分类号： C01B35/14 , C01B21/092 , C01B6/21 , C01B6/19
CPC分类号： C01B6/21 , C01B6/19 , C01B6/34 , C01B21/0923 , C01B35/146 , C01P2002/86 , C01P2002/88 , Y02E60/364
摘要： The present invention provides compositions comprising a metal amidoborane and an amine, and processes for preparing the metal amidoborane compositions. In particular, the process comprises contacting ammonia borane with a metal amide in the presence of an amine solvent to form the metal amidoborane composition. The invention also provides methods for generating hydrogen, wherein the method comprises heating the metal amidoborane composition such that hydrogen is released.
摘要翻译：本发明提供了包含金属氨基硼烷和胺的组合物，以及制备金属氨基硼烷组合物的方法。特别地，该方法包括在胺溶剂存在下使氨硼烷与金属酰胺接触以形成金属氨基硼烷组合物。本发明还提供了产生氢气的方法，其中该方法包括加热金属氨基硼烷组合物以释放氢。

6. 发明申请

US20120301382A1 METAL AMIDOBORANE COMPOSITIONS AND PROCESSES FOR THEIR PREPARATION 有权
标题翻译：金属微生物组合物及其制备方法
公开(公告)号：US20120301382A1
公开(公告)日：2012-11-29
申请号：US13392457
申请日：2010-04-13
申请人： Viktor Balema , Kanth Josyula , Guolin Xu , Nathaniel Wallock , Scott Batcheller , Peng Gao , Shashi Jasty
发明人： Viktor Balema , Kanth Josyula , Guolin Xu , Nathaniel Wallock , Scott Batcheller , Peng Gao , Shashi Jasty
IPC分类号： C01B3/04 , C01B35/14
CPC分类号： C01B6/21 , C01B6/19 , C01B6/34 , C01B21/0923 , C01B35/146 , C01P2002/86 , C01P2002/88 , Y02E60/364
摘要： The present invention provides compositions comprising a metal amidoborane and an amine, and processes for preparing the metal amidoborane compositions. In particular, the process comprises contacting ammonia borane with a metal amide in the presence of an amine solvent to form the metal amidoborane composition. The invention also provides methods for generating hydrogen, wherein the method comprises heating the metal amidoborane composition such that hydrogen is released.
摘要翻译：本发明提供了包含金属氨基硼烷和胺的组合物，以及制备金属氨基硼烷组合物的方法。特别地，该方法包括在胺溶剂存在下使氨硼烷与金属酰胺接触以形成金属氨基硼烷组合物。本发明还提供了产生氢气的方法，其中该方法包括加热金属氨基硼烷组合物以释放氢。

7. 发明申请

US20080311017A1 Metal aminoboranes 失效
标题翻译：金属氨基硼烷
公开(公告)号：US20080311017A1
公开(公告)日：2008-12-18
申请号：US12151575
申请日：2008-05-07
申请人： Anthony K. Burrell , Benjamin J. Davis , David L. Thorn , John C. Gordon , R. Thomas Baker , Troy Allen Semelsberger , William Tumas , Himashinie Vichalya Kaviraj Diyabalanage , Roshan P. Shrestha
发明人： Anthony K. Burrell , Benjamin J. Davis , David L. Thorn , John C. Gordon , R. Thomas Baker , Troy Allen Semelsberger , William Tumas , Himashinie Vichalya Kaviraj Diyabalanage , Roshan P. Shrestha
IPC分类号： C01F17/00 , C01B35/14
CPC分类号： H01M8/0606 , C01B3/0026 , C01B3/0031 , C01B6/19 , Y02E60/327
摘要： Metal aminoboranes of the formula M(NH2BH3)n have been synthesized. Metal aminoboranes are hydrogen storage materials. Metal aminoboranes are also precursors for synthesizing other metal aminoboranes. Metal aminoboranes can be dehydrogenated to form hydrogen and a reaction product. The reaction product can react with hydrogen to form a hydrogen storage material. Metal aminoboranes can be included in a kit.
摘要翻译：已经合成了式M（NH 2 BH 3）n的金属氨基硼烷。金属氨基硼烷是储氢材料。金属氨基硼烷也是合成其它金属氨基硼烷的前体。金属氨基硼烷可以脱氢形成氢气和反应产物。反应产物可与氢反应形成储氢材料。金属氨基硼烷可以包含在试剂盒中。

8. 发明申请

US20090095615A1 UNIVERSAL LIGANDS FOR THE ISOTOPE SEPARATION OF ELEMENTS 审中-公开
标题翻译：用于同位素分离元素的通用配置
公开(公告)号：US20090095615A1
公开(公告)日：2009-04-16
申请号：US11870708
申请日：2007-10-11
申请人： Edward J. Lahoda , David L. Stucker
发明人： Edward J. Lahoda , David L. Stucker
IPC分类号： B01D59/34
CPC分类号： B01D59/22 , B01D59/04 , B01D59/12 , B01D59/20 , C01B6/19
摘要： The present invention is directed to a method of isotope separation of one or more isotopes of a metal having a valence of two or more, comprised of selecting a ligand, such as BH4, BD4, CH3BH3 or CD3BD3, for attachment to one or more isotopes of the metal, ionically attaching the ligand to the one or more isotopes of the metal, and separating the one or more isotopes of the metal by an isotope separation technique. Suitable isotope separation techniques that can be used in the methods of the present invention include centrifuge, gaseous diffusion, gaseous distillation or molecular laser isotope separation techniques.
摘要翻译：本发明涉及一种同位素分离方法，其中一种或多种具有两个或更多个化合价的金属的同位素，包括选择配体如BH4，BD4，CH3BH3或CD3BD3，以连接至一个或多个同位素的金属离子地将配体附着到金属的一种或多种同位素，并通过同位素分离技术分离金属的一种或多种同位素。可用于本发明方法的合适的同位素分离技术包括离心机，气体扩散，气态蒸馏或分子激光同位素分离技术。

9. 发明授权

US06670444B2 Processes for synthesizing borohydride compounds 失效
标题翻译：合成硼氢化合物的方法
公开(公告)号：US06670444B2
公开(公告)日：2003-12-30
申请号：US10331674
申请日：2002-12-27
申请人： Steven C. Amendola , Michael T. Kelly , Jeffrey V. Ortega , Ying Wu
发明人： Steven C. Amendola , Michael T. Kelly , Jeffrey V. Ortega , Ying Wu
IPC分类号： C08G7908
CPC分类号： C01B6/21 , C01B3/34 , C01B6/13 , C01B6/19 , C01B2203/0227 , C01B2203/0283 , F17C11/005 , Y02P20/582
摘要： The present invention relates to processes for producing borohydride compounds. In particular, the present invention provides efficient processes and compositions for the large-scale production of borohydride compounds of the formula YBH4 by the reaction of a boron-containing compound represented by the formula BX3 with hydrogen or an aldehyde to obtain diborane and HX, and reacting the diborane with a Y-containing base selected from those represented by the formula Y2O, YOH and Y2CO3 to obtain YBH4 and YBO2. Y is selected from the group consisting of the alkali metals, pseudo-alkali metals, alkaline earth metals, an ammonium ion, and quaternary amines of the formula NR4+, wherein each R is independently selected from hydrogen and a straight- or branched-chain C1-4 alkyl group, and X is selected from the group consisting of halide ions, —OH, —R′ and —OR′ groups, chalcogens, and chalcogenides, wherein R′ is a straight- or branched-chain C1-4 alkyl group.
摘要翻译：本发明涉及生产硼氢化合物的方法。特别地，本发明提供了通过式BX3表示的含硼化合物与氢或醛反应而大规模生产式YBH4的硼氢化合物的有效方法和组合物，以获得乙硼烷和HX，以及使乙硼烷与选自由式Y 2 O，YOH和Y 2 CO 3表示的Y含量碱反应，得到YBH 4和YBO 2。 Y选自碱金属，假碱金属，碱土金属，铵离子和式NR4 +的季胺，其中每个R独立地选自氢和直链或支链的 - 链C 1-4烷基，X选自卤离子，-OH，-R'和-OR'基，硫属元素和硫族化物，其中R'是直链或支链C1- 4烷基。

10. 发明授权

US06524542B2 Processes for synthesizing borohydride compounds 失效
标题翻译：合成硼氢化合物的方法
公开(公告)号：US06524542B2
公开(公告)日：2003-02-25
申请号：US09833904
申请日：2001-04-12
申请人： Steven C. Amendola , Michael T. Kelly , Ying Wu
发明人： Steven C. Amendola , Michael T. Kelly , Ying Wu
IPC分类号： C01B610
CPC分类号： C01B6/21 , C01B6/13 , C01B6/19 , F17C11/005 , Y02P20/582
摘要： Processes for synthesizing borohydride compounds with reduced energy requirements are disclosed.
摘要翻译：公开了减少能量需求合成硼氢化合物的方法。

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