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1. 发明授权

US08703986B1 Process for preparing 10-chloro-9, 10-dihydro-9-oxa-10-phosphaphenanthrene-10-oxide compound 有权
标题翻译：制备10-氯-9,10-二氢-9-氧杂-10-磷杂菲-10-氧化物化合物的方法
公开(公告)号：US08703986B1
公开(公告)日：2014-04-22
申请号：US13932111
申请日：2013-07-01
申请人： UFC Corporation
发明人： Yu-Chin Lee , Jen-Hai Liao , Sung-Chen Lo , Chu-Chun Wu
IPC分类号： C07F9/02
CPC分类号： C07F9/657181 , C07F9/65719
摘要： Provided is a process for preparing 10-chloro-9,10-dihydro-9-oxa-10-phosphaphenanthrene-10-oxide (DOPO-C) compound, the process having steps of: reacting a liquid chlorinating agent and 9,10-dihydro-10-hydroxy-9-oxa 10-phosphaphenanthrene 10-oxide compound represented by formula (B) to form a mixture, the mixture comprises DOPO-C compound represented by formula (A) and an unreacted liquid chlorinating agent, separating the DOPO-C compound and the unreacted liquid chlorinating agent from the mixture to obtain the DOPO-C compound; wherein X1, X2, and X3 are each independently selected from the group consisting of hydrogen atom, hydroxyl group, cyano group, sulfonic acid group, sulfonate ester group represented by —SO3R1, halogen atom, alkoxy group represented by —OR2, acyclic hydrocarbon group having 1 to 8 carbon atoms, cyclic alkyl group having 3 to 8 carbon atoms, aryl group, heteroaryl group, and arylalkyl group, wherein R1 and R2 are each an acyclic hydrocarbon group having 1 to 8 carbon atoms.
摘要翻译：本发明提供一种制备10-氯-9,10-二氢-9-氧杂-10-磷杂菲-10-氧化物（DOPO-C）化合物的方法，该方法具有以下步骤：使液体氯化剂与9,10- 由式（B）表示的二氢-10-羟基-9-氧杂10-磷杂菲10氧化物化合物以形成混合物，该混合物包含由式（A）表示的DOPO-C化合物和未反应的液体氯化剂，将DOPO -C化合物和未反应的液体氯化剂，得到DOPO-C化合物; 其中X 1，X 2和X 3各自独立地选自氢原子，羟基，氰基，磺酸基，-SO 3 R 1表示的磺酸酯基，卤素原子，-OR 2表示的烷氧基，无环烃基具有1至8个碳原子，具有3至8个碳原子的环状烷基，芳基，杂芳基和芳基烷基，其中R 1和R 2各自是具有1至8个碳原子的无环烃基。

2. 发明授权

US07655805B2 Method for synthesizing benzotriazole 失效
标题翻译：苯并三唑合成方法
公开(公告)号：US07655805B2
公开(公告)日：2010-02-02
申请号：US12081983
申请日：2008-04-24
申请人： Ling Lu , Po-Hsuan Wei , Chung-Ning Fan , Yu-Cheng Lee , Hui-Ling Yang , Yu-Chin Lee
发明人： Ling Lu , Po-Hsuan Wei , Chung-Ning Fan , Yu-Cheng Lee , Hui-Ling Yang , Yu-Chin Lee
IPC分类号： C07D249/20
CPC分类号： C07D249/18
摘要： A method for synthesizing benzotriazole comprises acts of: preparing a first solvent comprising 2-(2-hydroxy-5-methylphenyl) benzotriazole, a basic agent and molecular sieves and a second solvent comprising 3-chloro-2-alkyl propylene; mixing the solvents; and heating the solvents. This method requires only one reaction vessel and produces few by-products, therefore is simpler and cheaper to produce. Furthermore, the molecular sieves are cheaper than catalysts in conventional reactions and may be recycled, giving even greater economic benefits.
摘要翻译：合成苯并三唑的方法包括以下作用：制备包含2-（2-羟基-5-甲基苯基）苯并三唑，碱性试剂和分子筛的第一溶剂和包含3-氯-2-烷基丙烯的第二溶剂; 混合溶剂; 并加热溶剂。该方法仅需要一个反应容器并产生很少的副产物，因此生产更简单和便宜。此外，分子筛比常规反应中的催化剂便宜，可以再循环，给予更大的经济效益。

3. 发明授权

US08362303B2 Process for producing aromatic aldehyde compound 失效
标题翻译：芳香醛化合物的制备方法
公开(公告)号：US08362303B2
公开(公告)日：2013-01-29
申请号：US13084653
申请日：2011-04-12
申请人： Yu-Chin Lee , Hsien-Yu Chang , Han-Hsu Chen , Yu-Sen Hou , Rong-Yi Liao
发明人： Yu-Chin Lee , Hsien-Yu Chang , Han-Hsu Chen , Yu-Sen Hou , Rong-Yi Liao
IPC分类号： C07C45/61
CPC分类号： C07C45/68 , C07C47/228
摘要： A process for producing an aromatic aldehyde compound has steps of converting alkyl-substituted or non-substituted benzene into a compound of formula I by halomethylation, and allowing the compound of formula I and alkyl aldehyde to react in presence of phase transfer catalyst at a reaction temperature under alkaline condition to obtain the aromatic aldehyde compound.
摘要翻译：芳族醛化合物的制造方法具有以下步骤：通过卤代甲基化将烷基取代或未取代的苯转化为式I化合物，并使式I化合物和烷基醛在相转移催化剂存在下在反应中反应温度在碱性条件下得到芳族醛化合物。

4. 发明授权

US08981014B2 Phosphorus-containing phenolic resin, method for manufacturing the same, and use of the same 有权
标题翻译：含磷酚醛树脂及其制造方法及其用途
公开(公告)号：US08981014B2
公开(公告)日：2015-03-17
申请号：US14279673
申请日：2014-05-16
申请人： Meiwa Plastic Industries, Ltd. , UFC Corporation
发明人： Masato Takenouchi , Tadatoshi Fujinaga , Erina Kimura , Yu-Chin Lee , Jen-Hai Liao , Sung-Chen Lo
IPC分类号： C08G65/32 , C08G61/10 , C08L63/00 , C08L65/00 , C08L71/02
CPC分类号： C08L65/00 , C08G8/36 , C08G59/4071 , C08G59/621 , C08G61/02 , C08G2261/135 , C08G2261/142 , C08G2261/147 , C08G2261/148 , C08G2261/3424 , C08G2261/76 , C08J5/24 , C08J2363/02 , C08L61/14 , C09K21/14 , C08L63/00
摘要： The present invention provides a novel phosphorus-containing phenolic resin. When the phosphorus-containing phenolic resin is used as an epoxy resin curing agent, the cured product thereof has various excellent properties such as excellent moisture resistance, low permittivity, a low dissipation factor, and excellent adhesion in addition to improved flame retardation. Specifically, the phosphorus-containing phenolic resin of the invention is represented by formula (1). The invention also provides a method for manufacturing the novel phosphorus-containing phenolic resin, a phenolic resin composition including the phosphorus-containing phenolic resin, an epoxy resin curing agent including the phenolic resin composition, an epoxy resin composition including the epoxy resin curing agent and an epoxy resin, a cured product obtained by curing the epoxy resin composition, and a copper-clad laminated plate obtained by using the epoxy resin composition as a matrix resin.
摘要翻译：本发明提供一种新型含磷酚醛树脂。当含磷酚醛树脂用作环氧树脂固化剂时，其固化产物具有优异的耐湿性，低介电常数，低耗散因子以及优异的粘合性以及阻燃性的优异性能。具体地，本发明的含磷酚醛树脂由式（1）表示。本发明还提供一种制造新型含磷酚醛树脂的方法，包含含磷酚醛树脂的酚醛树脂组合物，包含酚醛树脂组合物的环氧树脂固化剂，包含环氧树脂固化剂的环氧树脂组合物和环氧树脂，通过使环氧树脂组合物固化而得到的固化物，以及使用该环氧树脂组合物作为基质树脂而得到的覆铜层压板。

5. 发明申请

US20090246077A1 CONTAINER ASSEMBLY FOR SUBLIMATION 审中-公开
标题翻译：集装箱集装箱
公开(公告)号：US20090246077A1
公开(公告)日：2009-10-01
申请号：US12059890
申请日：2008-03-31
申请人： Ling LU , Kai-Chiang HUANG , Kang-Wei HSUEH , Ching-Hung CHEN , Yu-Sen HOU , Yu-Chin LEE
发明人： Ling LU , Kai-Chiang HUANG , Kang-Wei HSUEH , Ching-Hung CHEN , Yu-Sen HOU , Yu-Chin LEE
IPC分类号： G01D13/12
CPC分类号： B65D25/56 , B01D7/00 , B01D7/02
摘要： A container assembly has a raw-material container and a product-collection container, which are heat resistant and pressure resistant and have graduations formed on a sidewall thereof and a joint protruding therefrom. The product-collection container is detachably mounted on the raw-material container and communicates with the raw-material container through the joint. Since the raw-material container has graduations, an amount of raw materials can be consistently added in each batch, therefore, conditions of sublimation such as pressure, temperature or the like do not require adjustment and may just be monitored to ensure maximum yield is attained. Therefore, a sublimation procedure is simple, saves time and decreases product costs. Since, the product-collection container has graduations, an amount of product can be observed easily by the graduations and the product is easily removed without removing impure byproducts. Therefore, purity of the product can be increased.
摘要翻译：容器组件具有耐热和耐压的原料容器和产品收集容器，并且具有形成在其侧壁上的刻度和从其突出的接头。产品收集容器可拆卸地安装在原料容器上，并通过接头与原料容器连通。由于原材料容器具有刻度，因此可以一批添加一批原料，因此，升压条件如压力，温度等不需要调整，可以进行监控，以确保达到最大的收率。因此，升华程序简单，节省时间，降低产品成本。由于产品收集容器具有刻度，因此可以容易地观察到一定量的产品，并且容易地除去产品而不除去不纯的副产物。因此，可以提高产品的纯度。

6. 发明申请

US20140378622A1 PHOSPHORUS-CONTAINING PHENOLIC RESIN, METHOD FOR MANUFACTURING THE SAME, AND USE OF THE SAME 有权
标题翻译：含有PHOSPHOR的含酚树脂，其制造方法及其用途
公开(公告)号：US20140378622A1
公开(公告)日：2014-12-25
申请号：US14279673
申请日：2014-05-16
申请人： MEIWA PLASTIC INDUSTRIES, LTD. , UFC CORPORATION
发明人： Masato Takenouchi , Tadatoshi Fujinaga , Erina Kimura , Yu-Chin Lee , Jen-Hai Liao , Sung-Chen Lo
IPC分类号： C08G61/10 , C08L65/00 , C08L63/00
CPC分类号： C08L65/00 , C08G8/36 , C08G59/4071 , C08G59/621 , C08G61/02 , C08G2261/135 , C08G2261/142 , C08G2261/147 , C08G2261/148 , C08G2261/3424 , C08G2261/76 , C08J5/24 , C08J2363/02 , C08L61/14 , C09K21/14 , C08L63/00
摘要： The present invention provides a novel phosphorus-containing phenolic resin. When the phosphorus-containing phenolic resin is used as an epoxy resin curing agent, the cured product thereof has various excellent properties such as excellent moisture resistance, low permittivity, a low dissipation factor, and excellent adhesion in addition to improved flame retardation. Specifically, the phosphorus-containing phenolic resin of the invention is represented by formula (1). The invention also provides a method for manufacturing the novel phosphorus-containing phenolic resin, a phenolic resin composition including the phosphorus-containing phenolic resin, an epoxy resin curing agent including the phenolic resin composition, an epoxy resin composition including the epoxy resin curing agent and an epoxy resin, a cured product obtained by curing the epoxy resin composition, and a copper-clad laminated plate obtained by using the epoxy resin composition as a matrix resin.
摘要翻译：本发明提供一种新型含磷酚醛树脂。当含磷酚醛树脂用作环氧树脂固化剂时，其固化产物具有优异的耐湿性，低介电常数，低耗散因子以及优异的粘合性以及阻燃性的优异性能。具体地，本发明的含磷酚醛树脂由式（1）表示。本发明还提供一种制造新型含磷酚醛树脂的方法，包含含磷酚醛树脂的酚醛树脂组合物，包含酚醛树脂组合物的环氧树脂固化剂，包含环氧树脂固化剂的环氧树脂组合物和环氧树脂，通过使环氧树脂组合物固化得到的固化物，以及使用该环氧树脂组合物作为基质树脂而得到的覆铜层压板。

7. 发明申请

US20120264975A1 Phase Transfer Catalyst for Producing Aromatic Aldehyde Compound 审中-公开
标题翻译：用于生产芳香醛化合物的相转移催化剂
公开(公告)号：US20120264975A1
公开(公告)日：2012-10-18
申请号：US13086470
申请日：2011-04-14
申请人： Yu-Chin Lee , Hsien-Yu Chang , Han-Hsu Chen , Yu-Sen Hou , Rong-Yi Liao
发明人： Yu-Chin Lee , Hsien-Yu Chang , Han-Hsu Chen , Yu-Sen Hou , Rong-Yi Liao
IPC分类号： C07C211/63
CPC分类号： C07C211/63 , C07C45/68 , C07C47/52
摘要： Provided is a phase transfer catalyst for producing an aromatic aldehyde compound, comprising a compound of formula I, wherein R1 is hydrogen, methyl, ethyl, isopropyl, isobutyl or tertbutyl; R4, R5 and R6 are independently selected from alkyl groups containing 1 to 6 carbon atoms; and X is fluorine, chlorine, bromine or iodine.
摘要翻译：本发明提供一种用于生产芳族醛化合物的相转移催化剂，其包含式I化合物，其中R 1是氢，甲基，乙基，异丙基，异丁基或叔丁基; R4，R5和R6独立地选自含1至6个碳原子的烷基; X是氟，氯，溴或碘。

8. 发明授权

US07964750B2 Method for synthesizing 9,10-dihydro-9-oxa-10-phosphaphenanthrene-10-oxide or a derivative thereof 有权
标题翻译：合成9,10-二氢-9-氧杂-10-磷杂菲-10-氧化物或其衍生物的方法
公开(公告)号：US07964750B2
公开(公告)日：2011-06-21
申请号：US12535897
申请日：2009-08-05
申请人： Ling Lu , Kai-Chiang Huang , Kuan-Chieh Tseng , Chung-Ning Fan , Yu-Cheng Lee , Tien-Wen Lo , Yu-Chin Lee
发明人： Ling Lu , Kai-Chiang Huang , Kuan-Chieh Tseng , Chung-Ning Fan , Yu-Cheng Lee , Tien-Wen Lo , Yu-Chin Lee
IPC分类号： C07F9/6571
CPC分类号： C07F9/657172 , C07F9/65719
摘要： A method for synthesizing 9,10-dihydro-9-oxa-10-phosphaphenanthrene-10-oxide or its derivatives has a step of introducing 6-chloro-6H-dibenz[c,e][1,2]oxaphosphorin or its derivative, an acid compound and water into a reacting chamber to form an organic layer having 9,10-dihydro-9-oxa-10-phosphaphenanthrene-10-oxide or its derivative and an aqueous layer. Because the acid compound is from an external source and has a catalyzing effect, employing the method can prevent side reaction from occurring and increase yield of 9,10-dihydro-9-oxa-10-phosphaphenanthrene-10-oxide or its derivative. Furthermore, the method is a one-pot operation of hydrolysis, dehydration and cyclization, so the method does not require purification of intermediates. Therefore, the method is time- and cost-saving and requires less organic solvent, resulting in less pollution to the environment.
摘要翻译：合成9,10-二氢-9-氧杂-10-磷杂菲-10-氧化物或其衍生物的方法具有引入6-氯-6H-二苯并[c，e] [1,2]氧杂磷杂环丁烷或其衍生物的步骤，酸化合物和水加入到反应室中以形成具有9,10-二氢-9-氧杂-10-磷杂菲-10-氧化物或其衍生物和水层的有机层。由于酸化合物来自外源并具有催化作用，所以采用该方法可以防止发生副反应，提高9,10-二氢-9-氧杂-10-磷杂菲-10-氧化物或其衍生物的产率。此外，该方法是水解，脱水和环化的一锅操作，因此该方法不需要中间体的纯化。因此，该方法节省时间并且需要更少的有机溶剂，从而减少对环境的污染。

9. 发明申请

US20110034717A1 METHOD FOR SYNTHESIZING 9,10-DIHYDRO-9-OXA-10-PHOSPHAPHENANTHRENE-10-OXIDE AND DERIVATIVES THEREOF 有权
标题翻译：合成9,10-二氢-9-氧代-10-磷杂环戊烯-10-氧化物及其衍生物的方法
公开(公告)号：US20110034717A1
公开(公告)日：2011-02-10
申请号：US12535897
申请日：2009-08-05
申请人： Ling Lu , Kai-Chiang Huang , Kuan-Chieh Tseng , Chung-Ning Fan , Yu-Cheng Lee , Tien-Wen Lo , Yu-Chin Lee
发明人： Ling Lu , Kai-Chiang Huang , Kuan-Chieh Tseng , Chung-Ning Fan , Yu-Cheng Lee , Tien-Wen Lo , Yu-Chin Lee
IPC分类号： C07F9/32
CPC分类号： C07F9/657172 , C07F9/65719
摘要： A method for synthesizing 9,10-dihydro-9-oxa-10-phosphaphenanthrene-10-oxide or its derivatives has a step of introducing 6-chloro-6H-dibenz[c,e][1,2]oxaphosphorin or its derivative, an acid compound and water into a reacting chamber to form an organic layer having 9,10-dihydro-9-oxa-10-phosphaphenanthrene-10-oxide or its derivative and an aqueous layer. Because the acid compound is from an external source and has a catalyzing effect, employing the method can prevent side reaction from occurring and increase yield of 9,10-dihydro-9-oxa-10-phosphaphenanthrene-10-oxide or its derivative. Furthermore, the method is a one-pot operation of hydrolysis, dehydration and cyclization, so the method does not require purification of intermediates. Therefore, the method is time-and cost-saving and requires less organic solvent, resulting in less pollution to the environment.
摘要翻译：合成9,10-二氢-9-氧杂-10-磷杂菲-10-氧化物或其衍生物的方法具有引入6-氯-6H-二苯并[c，e] [1,2]氧杂磷杂环丁烷或其衍生物的步骤，酸化合物和水加入到反应室中以形成具有9,10-二氢-9-氧杂-10-磷杂菲-10-氧化物或其衍生物和水层的有机层。由于酸化合物来自外源并具有催化作用，所以采用该方法可以防止发生副反应，提高9,10-二氢-9-氧杂-10-磷杂菲-10-氧化物或其衍生物的产率。此外，该方法是水解，脱水和环化的一锅操作，因此该方法不需要中间体的纯化。因此，该方法节省时间并且需要更少的有机溶剂，导致对环境的污染较少。

10. 发明申请

US20120264981A1 Process for Producing Aromatic Aldehyde Compound 失效
标题翻译：生产芳香醛化合物的方法
公开(公告)号：US20120264981A1
公开(公告)日：2012-10-18
申请号：US13084653
申请日：2011-04-12
申请人： Yu-Chin Lee , Hsien-Yu Chang , Han-Hsu Chen , Yu-Sen Hou , Rong-Yi Liao
发明人： Yu-Chin Lee , Hsien-Yu Chang , Han-Hsu Chen , Yu-Sen Hou , Rong-Yi Liao
IPC分类号： C07C45/61
CPC分类号： C07C45/68 , C07C47/228
摘要： A process for producing an aromatic aldehyde compound has steps of converting alkyl-substituted or non-substituted benzene into a compound of formula I by halomethylation, and allowing the compound of formula I and alkyl aldehyde to react in presence of phase transfer catalyst at a reaction temperature under alkaline condition to obtain the aromatic aldehyde compound.
摘要翻译：芳族醛化合物的制造方法具有以下步骤：通过卤代甲基化将烷基取代或未取代的苯转化为式I化合物，并使式I化合物和烷基醛在相转移催化剂存在下在反应中反应温度在碱性条件下得到芳族醛化合物。

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