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1. 发明申请

US20090202869A1 CARBON PARTICLE HAVING DEPOSITED FINE PARTICLES, PROCESS FOR PRODUCING THE SAME, AND ELECTRODE FOR FUEL CELL 审中-公开
标题翻译：具有沉积精细颗粒的碳颗粒，其生产方法和用于燃料电池的电极
公开(公告)号：US20090202869A1
公开(公告)日：2009-08-13
申请号：US12304462
申请日：2007-06-12
申请人： Yuko Sawaki , Mikio Kishimoto , Haruyuki Nakanishi , Shigeaki Murata , Masahiro Imanishi
发明人： Yuko Sawaki , Mikio Kishimoto , Haruyuki Nakanishi , Shigeaki Murata , Masahiro Imanishi
IPC分类号： H01M4/02 , B05D7/24 , B32B5/16
CPC分类号： C01G49/0054 , B82Y30/00 , C01B32/05 , C01G51/003 , C01G51/006 , C01P2002/34 , C01P2002/60 , C01P2002/72 , C01P2002/74 , C01P2002/80 , C01P2002/85 , C01P2004/04 , C01P2004/64 , C01P2004/80 , C01P2006/40 , H01M4/8647 , H01M4/885 , H01M4/9033 , H01M4/92 , H01M4/921 , H01M4/923 , H01M4/925 , H01M4/926 , H01M2008/1095 , Y10T428/2991
摘要： Carbon particles having fine particles deposited thereon which can be used as a substitute for the carbon particles having platinum deposited thereon and metallic platinum particles which are presently in general use as, e.g., a catalyst for electrodes in fuel cells. Compared to the conventional carbon particles having platinum deposited thereon, etc., the carbon particles are effective in greatly reducing the amount of platinum to be used. The carbon particles are characterized by comprising carbon particles and, deposited on the surface of the carbon particles, fine particles of a perovskite type composite metal oxide in each of which fine noble-metal particles are present throughout the whole particle. Also provided is a process for producing the carbon particles.The carbon particles having deposited fine particles have a constitution in which fine particles of a perovskite type composite metal oxide each having fine noble-metal particles present throughout the whole perovskite type oxide particle and having a crystallite size of 1-20 nm are deposited on carbon particles. The process for producing such carbon particles having fine particles deposited thereon comprises preparing a solution containing fine perovskite type composite oxide particles and complex ions of a metal for constituting fine noble-metal particles, subsequently repeating the step of impregnating the solution into carbon particles and dried the particles to thereby adsorb complex ions of the metal onto the carbon particles, and then subjecting the resultant particles to heat treatment.
摘要翻译：具有沉积在其上的细颗粒的碳颗粒可以用作其上沉积有铂的碳颗粒的替代物和目前通常用作燃料电池中的电极催化剂的金属铂颗粒。与其上沉积有铂的常规碳颗粒相比，碳颗粒有效地大大降低了所用的铂的量。碳颗粒的特征在于包含碳颗粒，并且在碳颗粒的表面上沉积有细小的贵金属颗粒存在于整个颗粒中的钙钛矿型复合金属氧化物的细颗粒。还提供了用于生产碳颗粒的方法。具有沉积细小颗粒的碳颗粒具有这样一种构造，即，在整个钙钛矿型氧化物颗粒中存在细小的贵金属微粒并且具有1-20nm的微晶尺寸的钙钛矿型复合金属氧化物的微粒沉积在碳上粒子。制备这种沉积有微细颗粒的碳颗粒的方法包括制备含有细钙钛矿型复合氧化物颗粒和用于构成细贵金属颗粒的金属的配合离子的溶液，随后重复将溶液浸渍到碳颗粒中并干燥从而将金属的复合离子吸附到碳颗粒上，然后对所得颗粒进行热处理。

2. 发明授权

US08007691B2 Fine particle of perovskite oxide, particle having deposited perovskite oxide, catalyst material, catalyst material for oxygen reduction, catalyst material for fuel cell, and electrode for fuel cell 有权
标题翻译：钙钛矿氧化物的细颗粒，具有沉积的钙钛矿氧化物的颗粒，催化剂材料，用于氧还原的催化剂材料，用于燃料电池的催化剂材料和用于燃料电池的电极
公开(公告)号：US08007691B2
公开(公告)日：2011-08-30
申请号：US12304452
申请日：2007-06-12
申请人： Yuko Sawaki , Mikio Kishimoto , Haruyuki Nakanishi , Shigeaki Murata , Masahiro Imanishi , Shinichi Matsumoto
发明人： Yuko Sawaki , Mikio Kishimoto , Haruyuki Nakanishi , Shigeaki Murata , Masahiro Imanishi , Shinichi Matsumoto
IPC分类号： H01B1/08
CPC分类号： H01M4/925 , C01G49/0018 , C01G49/009 , C01P2002/34 , C01P2002/77 , H01M4/9016 , H01M4/9033 , H01M4/9083 , H01M4/92 , H01M8/1007 , H01M2008/1095
摘要： A catalyst for electrodes in solid-polymer fuel cells which comprises metal oxide particles themselves. The catalyst contains fine transition-metal oxide particles having, in the main phase, a perovskite structure represented by the general formula ABO3 (wherein A represents one or more elements selected among lanthanum, strontium, cerium, calcium, yttrium, erbium, praseodymium, neodymium, samarium, europium, silicon, magnesium, barium, niobium, lead, bismuth, and antimony; and B represents one or more elements selected among iron, cobalt, manganese, copper, titanium, chromium, nickel, and molybdenum), the fine oxide particles having lattice constants satisfying the following relationship (1): 1.402
摘要翻译：固体聚合物燃料电池中用于电极的催化剂，其包含金属氧化物颗粒本身。该催化剂含有在主相中具有由通式ABO 3表示的钙钛矿结构的细过渡金属氧化物颗粒（其中A表示选自镧，锶，铈，钙，钇，铒，镨，钕中的一种或多种元素，钐，铕，硅，镁，钡，铌，铅，铋和锑; B表示选自铁，钴，锰，铜，钛，铬，镍和钼中的一种或多种元素）具有满足以下关系式（1）的晶格常数的粒子：1.402 <2b /（a + c）<1.422（1）其中a和c表示钙钛矿型晶格的短轴长度，b表示长轴长度其中。

3. 发明授权

US07829061B2 Zirconium oxide hydrate particles and method for producing the same 失效
标题翻译：氧化锆水合物颗粒及其制备方法
公开(公告)号：US07829061B2
公开(公告)日：2010-11-09
申请号：US12167110
申请日：2008-07-02
申请人： Yuko Sawaki , Kazutaka Matsuo , Mikio Kishimoto , Takayuki Hirashige , Makoto Morishima
发明人： Yuko Sawaki , Kazutaka Matsuo , Mikio Kishimoto , Takayuki Hirashige , Makoto Morishima
IPC分类号： C01G25/02
CPC分类号： C01G25/02 , B82Y30/00 , C01P2002/72 , C01P2002/76 , C01P2004/04 , C01P2004/64 , C01P2006/82 , Y10T428/2982
摘要： The zirconium oxide hydrate particles of the present invention are represented by the formula ZrO2.nH2O and have a mean primary particle size of 0.5 nm or more and 5 nm or less, and “n” in the formula represents a number greater than 2.5. Moreover, the method for producing of zirconium oxide hydrate particles of the present invention includes the step of preparing zirconium oxide hydrate particles by adding an aqueous zirconium salt solution to an aqueous alkaline solution while controlling the pH to 7.0 or more and 13.0 or less, and the step of subjecting the zirconium oxide hydrate particles to a hydrothermal treatment in the presence of water at a temperature of 50° C. or more and less than 110° C. for 3 hours or more.
摘要翻译：本发明的氧化锆水合物颗粒由式ZrO 2·nH 2 O表示，平均一次粒径为0.5nm以上且5nm以下，式中“n”表示大于2.5的数。此外，本发明的氧化锆水合物颗粒的制造方法包括通过向碱性水溶液中添加锆盐水溶液，同时将pH控制在7.0以上且13.0以下，制备氧化锆水合物颗粒的工序，以及在水存在下，在50℃以上且小于110℃的温度下对氧化锆水合物颗粒进行水热处理3小时以上的步骤。

4. 发明申请

US20090011239A1 ZIRCONIUM OXIDE HYDRATE PARTICLES AND METHOD FOR PRODUCING THE SAME 失效
标题翻译：氧化锆水合物颗粒及其生产方法
公开(公告)号：US20090011239A1
公开(公告)日：2009-01-08
申请号：US12167110
申请日：2008-07-02
申请人： Yuko SAWAKI , Kazutaka Matsuo , Mikio Kishimoto , Takayuki Hirashige , Makoto Morishima
发明人： Yuko SAWAKI , Kazutaka Matsuo , Mikio Kishimoto , Takayuki Hirashige , Makoto Morishima
IPC分类号： C01G25/02 , B32B5/16
CPC分类号： C01G25/02 , B82Y30/00 , C01P2002/72 , C01P2002/76 , C01P2004/04 , C01P2004/64 , C01P2006/82 , Y10T428/2982
摘要： The zirconium oxide hydrate particles of the present invention are represented by the formula ZrO2.nH2O and have a mean primary particle size of 0.5 nm or more and 5 nm or less, and “n” in the formula represents a number greater than 2.5. Moreover, the method for producing of zirconium oxide hydrate particles of the present invention includes the step of preparing zirconium oxide hydrate particles by adding an aqueous zirconium salt solution to an aqueous alkaline solution while controlling the pH to 7.0 or more and 13.0 or less, and the step of subjecting the zirconium oxide hydrate particles to a hydrothermal treatment in the presence of water at a temperature of 50° C. or more and less than 110° C. for 3 hours or more.
摘要翻译：本发明的氧化锆水合物颗粒由式ZrO 2·nH 2 O表示，平均一次粒径为0.5nm以上且5nm以下，式中“n”表示大于2.5的数。此外，本发明的氧化锆水合物颗粒的制造方法包括通过向碱性水溶液中添加锆盐水溶液，同时将pH控制在7.0以上且13.0以下，制备氧化锆水合物颗粒的工序，以及在水存在下，在50℃以上且小于110℃的温度下对氧化锆水合物颗粒进行水热处理3小时以上的步骤。

5. 发明申请

US20080141594A1 NON-MAGNETIC PLATE-FORM PARTICLES, METHOD FOR PRODUCING THE SAME, AND ABRASIVE, ABRASIVE MEMBER AND ABRASIVE LIQUID COMPRISING THE SAME 审中-公开
标题翻译：非磁性板形颗粒，其制造方法和磨料磨料组分和包含其的磨料液
公开(公告)号：US20080141594A1
公开(公告)日：2008-06-19
申请号：US11946694
申请日：2007-11-28
申请人： Mikio Kishimoto , Nobuko Kasajima , Yuko Sawaki , Kimihiko Kaneno , Yasumori Maeda
发明人： Mikio Kishimoto , Nobuko Kasajima , Yuko Sawaki , Kimihiko Kaneno , Yasumori Maeda
IPC分类号： B24D3/02
CPC分类号： B24D3/00 , C09K3/1409
摘要： An aqueous solution of a metal salt to an alkaline aqueous solution to forma hydroxide or a hydrate of a metal, and the hydroxide or hydrate of the metal is heated at a temperature of 110 to 300° C. in the presence of water. Then, the hydroxide or hydrate of the metal is filtered and dried and then further heated at a temperature of 300 to 1200° C. in an air to form oxide particles such as the particles of cerium oxide, zirconium oxide, aluminum oxide silicon oxide, iron oxide, etc. Thereby the particles of cerium oxide, zirconium oxide, aluminum oxide silicon oxide, iron oxide, etc. having a plate-form shape and a particle size of from 10 nm to 100 nm in the plate direction of the particle are obtained. The non-magnetic particles, in particular, plate-form oxide particles of the present invention have a uniform particle size distribution, are less sintered or agglomerated, and have good crystallinity.
摘要翻译：将金属盐的水溶液与碱性水溶液形成氢氧化物或金属的水合物，以及金属的氢氧化物或水合物在水存在下在110〜300℃的温度下加热。然后，将金属的氢氧化物或水合物过滤并干燥，然后在空气中在300至1200℃的温度下进一步加热以形成氧化物颗粒，例如氧化铈，氧化锆，氧化铝氧化硅颗粒，氧化铁等。由此，粒子的板方向上的板状，粒径为10nm〜100nm的氧化铈，氧化锆，氧化铝，氧化铁等的粒子为获得。非磁性颗粒，特别是本发明的板状氧化物颗粒具有均匀的粒度分布，较少烧结或附聚，并且具有良好的结晶度。

6. 发明申请

US20100151362A1 PARTICULATE CARBON CARRYING FINE PARTICLE THEREON, PROCESS FOR PRODUCTION THEREOF, AND ELECTRODES FOR FUEL CELLS 审中-公开
标题翻译：颗粒状碳颗粒，其生产方法和燃料电极
公开(公告)号：US20100151362A1
公开(公告)日：2010-06-17
申请号：US12088064
申请日：2006-09-25
申请人： Yuko Sawaki , Mikio Kishimoto , Haruyuki Nakanishi , Masahiro Imanishi
发明人： Yuko Sawaki , Mikio Kishimoto , Haruyuki Nakanishi , Masahiro Imanishi
IPC分类号： H01M4/02 , B32B9/00 , B05D7/24 , B32B1/00
CPC分类号： B01J23/002 , B01J21/18 , B01J23/58 , B01J23/63 , B01J23/894 , B01J35/0013 , B01J2523/00 , H01M4/8605 , H01M4/8814 , H01M4/8875 , H01M4/8882 , H01M4/8896 , H01M4/9016 , H01M4/923 , H01M4/926 , H01M2008/1095 , Y10T428/2991 , B01J2523/24 , B01J2523/3706 , B01J2523/842 , B01J2523/821 , B01J2523/828 , B01J2523/3712 , B01J2523/845
摘要： There are provided carbon particles supporting thereon fine particles of a perovskite type composite oxide, which can be used as a substitute for the existing platinum-supporting carbon particles or platinum metal particles commonly used in electrocatalysts for fuel cells, and which are significantly reduced in the amount of platinum to be used in comparison with the existing platinum-supporting carbon particles, and a process for manufacturing the same carbon particles.The fine particles of a perovskite type composite metal oxide which contains a noble metal element in its crystal lattice and has an average crystallite size of from 1 to 20 nm are supported on carbon particles. To manufacture such fine particle-supporting carbon particles, a solution containing complex ions of a metal which constitutes the fine perovskite type composite oxide particle is firstly prepared; then, carbon particles are dispersed in the resulting solution to adsorb the complex ions of the metal onto the carbon particles; and the resulting dispersion is subjected to a heat treatment.
摘要翻译：提供了碳粒子，其上附着有钙钛矿型复合氧化物的细颗粒，其可以用作代替用于燃料电池的电极催化剂中通常使用的现有的铂负载碳颗粒或铂金属颗粒，并且在与现有的铂负载碳粒子相比较使用的铂量以及制造相同碳粒子的方法。含有贵金属元素的晶格中的平均微晶尺寸为1〜20nm的钙钛矿型复合金属氧化物的微粒被负载在碳粒子上。为了制造这种微粒子载体碳粒子，首先制备含有构成微细钙钛矿型复合氧化物粒子的金属的配合离子的溶液，然后将碳颗粒分散在所得溶液中以将金属的复合离子吸附到碳颗粒上; 对所得到的分散体进行热处理。

7. 发明申请

US20060266980A1 Composite indium oxide particle, method for producing same, conductive coating material, conductive coating film, and conductive sheet 失效
标题翻译：复合氧化铟粒子，其制造方法，导电性涂料，导电性涂膜，导电片等
公开(公告)号：US20060266980A1
公开(公告)日：2006-11-30
申请号：US10551188
申请日：2004-03-31
申请人： Yuko Sawaki , Mikio Kishimoto
发明人： Yuko Sawaki , Mikio Kishimoto
IPC分类号： H01B1/12
CPC分类号： B82Y30/00 , C01G19/006 , C01P2002/72 , C01P2004/64 , H01B1/08 , Y10T428/256 , Y10T428/2982 , Y10T428/2991
摘要： An aqueous alkaline solution containing a tin salt dissolved therein is mixed with a zinc compound, and an aqueous solution of an indium salt is added to the mixture. The resultant hydroxide or hydrate containing tin, indium and zinc is treated by heating at a temperature of 110 to 300° C. in the present of water. Then, the resultant product is filtered, dried and treated by heating at a temperature of 300 to 1,000° C. in an air and further reduced at a temperature of 150 to 400° C. under a reducing atmosphere to obtain composite indium oxide particles of zinc oxide and tin-containing indium oxide, which have an average particle size of 5 to 100 nm. The resultant composite particles of zinc oxide and tin-containing indium oxide are suitably used to form a transparent conductive coating film having a UV-shielding effect.
摘要翻译：将含有锡盐的碱性水溶液与锌化合物混合，向该混合物中加入铟盐水溶液。所得到的含有锡，铟和锌的氢氧化物或水合物在水中在110〜300℃的温度下进行加热处理。然后，将所得产物过滤，干燥并在空气中在300至1000℃的温度下加热处理，并在还原气氛下在150至400℃的温度下还原，得到复合氧化铟颗粒氧化锌和含锡的氧化铟，其平均粒度为5〜100nm。所得到的氧化锌和含锡氧化铟的复合颗粒适合用于形成具有UV屏蔽作用的透明导电涂膜。

8. 发明申请

US20050008847A1 Indium particle containing tin, method for producing the same and electroconductive sheet comprising the same 失效
标题翻译：含锡的锡颗粒，其制造方法以及包含该锡的含导电性片材
公开(公告)号：US20050008847A1
公开(公告)日：2005-01-13
申请号：US10495527
申请日：2002-11-14
申请人： Mikio Kishimoto , Nobuko Kasajima , Yuko Sawaki , Noriaki Otani
发明人： Mikio Kishimoto , Nobuko Kasajima , Yuko Sawaki , Noriaki Otani
IPC分类号： C01G15/00 , C01G19/00 , H01B1/02 , H01B1/08 , B32B27/18
CPC分类号： B82Y30/00 , C01G15/00 , C01G19/00 , C01P2004/62 , C01P2004/64 , H01B1/02 , H01B1/08 , Y10T428/12007 , Y10T428/256 , Y10T428/265
摘要： An aqueous solution of a tin salt and an indium salt is added to an aqueous alkaline solution to form a hydroxide or a hydrate comprising tin and indium, the hydroxide or hydrate is heated at a temperature of 110 to 300° C. in the presence of water, filtered and dried, and then the hydroxide or hydrate is heated at a temperature of 200 to 1000° C. to form the tin-containing indium oxide particles. Thereby, tin-containing indium oxide particles which have a plate-form shape and an average particle size in the plane direction of 10 to 200 nm are obtained. The tin-containing indium oxide particles are suitable for forming an electrically conductive transparent coating film.
摘要翻译：将锡盐和铟盐的水溶液加入到碱性水溶液中以形成包含锡和铟的氢氧化物或水合物，氢氧化物或水合物在110〜300℃的温度下，在水，过滤并干燥，然后将氢氧化物或水合物在200至1000℃的温度下加热以形成含锡氧化铟颗粒。由此，得到平面形状的板状，平均粒径为10〜200nm的含锡氧化铟粒子。含锡氧化铟粒子适合于形成导电性透明涂膜。

9. 发明授权

US08163438B2 Composite electrolyte membrane, production method thereof, membrane-electrode assembly, and fuel cell 有权
标题翻译：复合电解质膜，其制造方法，膜 - 电极组件和燃料电池
公开(公告)号：US08163438B2
公开(公告)日：2012-04-24
申请号：US12155142
申请日：2008-05-30
申请人： Takayuki Hirashige , Makoto Morishima , Mikio Kishimoto , Yuko Sawaki , Kazutaka Matsuo
发明人： Takayuki Hirashige , Makoto Morishima , Mikio Kishimoto , Yuko Sawaki , Kazutaka Matsuo
IPC分类号： H01M8/10 , C01G25/02
CPC分类号： C08J5/2275 , C08J2381/02 , H01B1/122 , H01M8/04197 , H01M8/1011 , H01M8/1023 , H01M8/1039 , H01M8/1048 , H01M8/1072 , H01M2300/0071 , H01M2300/0082 , H01M2300/0091 , Y02E60/523 , Y02P70/56
摘要： A composite electrolyte membrane uses a metal-oxide hydrate which has a number of hydration water molecules of 2.7 or more and 10 or less and/or which is in the form of particles having a particle diameter of 1 nm or more and 10 nm or less. The composite electrolyte membrane exhibits its expected original performance, has both a high proton conductivity and a low methanol permeability, and provides a high-output membrane electrolyte assembly for a fuel cell.
摘要翻译：复合电解质膜使用水合水分子数为2.7以上且10以下的金属氧化物水合物和/或粒径为1nm以上且10nm以下的粒子的形式。复合电解质膜表现出其预期的原始性能，具有高质子传导性和低甲醇渗透性，并提供用于燃料电池的高输出膜电解质组件。

10. 发明申请

US20090246602A1 Microparticle-Supported Carbon Particle, Method for Production Thereof, and Fuel Cell Electrode 审中-公开
标题翻译：微颗粒载体碳颗粒，其制备方法和燃料电池电极
公开(公告)号：US20090246602A1
公开(公告)日：2009-10-01
申请号：US11992545
申请日：2006-09-25
申请人： Yuko Sawaki , Yoshinori Sato , Mikio Kishimoto , Haruyuki Nakanishi , Masahiro Imanishi
发明人： Yuko Sawaki , Yoshinori Sato , Mikio Kishimoto , Haruyuki Nakanishi , Masahiro Imanishi
IPC分类号： H01M4/90 , B05D7/00 , H01B1/08 , H01B1/06
CPC分类号： H01M4/8652 , H01M4/8842 , H01M4/8882 , H01M4/9016 , H01M4/9083
摘要： There are provided fine particle-carrying carbon particles, which can be used as a substitute for the existing platinum-carrying carbon particles or platinum metal particles commonly used in electrocatalysts for fuel cells or the like, and which are significantly reduced in the amount of platinum to be used in comparison with the existing platinum-carrying carbon particles, and an electrode for a fuel cell using the same carbon particles.The fine particle-carrying carbon particle comprises a carbon particle with an average particle diameter of from 20 to 70 nm, and fine particles of a metal oxide with an average crystallite size of from 1 to 20 nm, carried on the carbon particle, wherein the metal oxide contains a noble metal element such as a platinum element, and is represented by the formula: MOx in which the metal element M is partially substituted by the noble metal element. To manufacture such fine particle-carrying carbon particles, a solution containing complex ions of a metal which constitutes the fine metal oxide particle is firstly prepared; then, carbon particles are dispersed in the resulting solution to adsorb the complex ions of the metal onto the carbon particles; and the resulting dispersion is subjected to a hydrothermal treatment.
摘要翻译：提供了能够用于代替燃料电池等的电极催化剂中通常使用的现有的携带铂的碳粒子或铂金属粒子的微粒子载体碳粒子，其显着降低了铂与现有的携带铂的碳颗粒相比使用，以及使用相同碳颗粒的燃料电池用电极。所述微粒子载体碳粒子包含平均粒径为20〜70nm的碳粒子和平均微晶尺寸为1〜20nm的金属氧化物的微粒，承载在碳粒子上，其中，金属氧化物含有贵金属元素如铂元素，并且由金属元素M部分被贵金属元素取代的式为MOx表示。为了制造这种微粒子载体碳粒子，首先制备含有构成金属微细氧化物粒子的金属的络合离子的溶液，然后将碳颗粒分散在所得溶液中以将金属的复合离子吸附到碳颗粒上; 并将所得分散体进行水热处理。

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