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1. 发明授权

US06582667B1 Shell-and-tube reactor 失效
标题翻译：管壳式反应器
公开(公告)号：US06582667B1
公开(公告)日：2003-06-24
申请号：US09394087
申请日：1999-09-13
申请人： Yousuke Ogata , Takehiro Takashima , Osamu Dodo , Hidefumi Haramaki
发明人： Yousuke Ogata , Takehiro Takashima , Osamu Dodo , Hidefumi Haramaki
IPC分类号： B01J806
CPC分类号： C07C51/252 , B01J8/067 , B01J2208/00212 , B01J2208/00221 , B01J2208/00256 , B01J2219/00777 , C07C45/35 , C07C51/313 , Y02P20/123 , Y02P20/51 , C07C47/22 , C07C57/04 , C07C63/16
摘要： A shell-and-tube reactor has a plurality of reaction tubes incorporated therein, a circulation path for the heating medium formed outside the reaction tubes, a heating medium introducing section provided on the upper part of the shell in the reactor and a heating medium discharge section provided on the lower part of the shell in the reactor, a back pressure applying means for the heating medium is further provided in the heating medium discharge section.
摘要翻译：管壳式反应器内装有多个反应管，形成在反应管外侧的加热介质的循环路径，设置在反应器壳体上部的加热介质导入部和加热介质排出口在反应器的壳体的下部设置有用于加热介质的背压施加装置的加热介质排出部。

2. 发明授权

US5872288A Process for producing (meth) acrylic acid 失效
标题翻译：（甲基）丙烯酸的制造方法
公开(公告)号：US5872288A
公开(公告)日：1999-02-16
申请号：US990522
申请日：1997-12-15
申请人： Hidefumi Haramaki , Osamu Dodo , Mamoru Takamura
发明人： Hidefumi Haramaki , Osamu Dodo , Mamoru Takamura
IPC分类号： C07C57/07 , C07C51/42
CPC分类号： C07C51/42 , Y10S203/22
摘要： The present invention provides a process for producing (meth)acrylic acid by gas-phase catalytic oxidation, which comprises cooling and condensing a (meth)acrylic acid-containing reaction product gas to obtain a crude aqueous (meth)acrylic acid solution; cooling the aqueous solution to deposit the impurities contained in the aqueous solution, as solid matter; separating the solid matter; and then extracting and separating (meth)acrylic acid from the purified aqueous (meth)acrylic acid solution obtained. Unlike the conventional processes in which (meth)acrylic acid is extracted and separated from a crude aqueous (meth)acrylic acid solution, the present process can avoid various troubles caused by the impurities contained in the crude aqueous (meth)acrylic acid solution, for example, generation of scum and the like, and therefore can produce (meth)acrylic acid at a higher purity than in the conventional processes.
摘要翻译：本发明提供一种通过气相催化氧化制备（甲基）丙烯酸的方法，其包括冷却并冷凝含（甲基）丙烯酸的反应产物气体，得到粗的（甲基）丙烯酸水溶液; 冷却水溶液以沉积包含在水溶液中的杂质，作为固体物质; 分离固体物质; 然后从得到的纯化的（甲基）丙烯酸水溶液中萃取分离（甲基）丙烯酸。与从（甲基）丙烯酸粗水溶液中提取（甲基）丙烯酸并分离的常规方法不同，本方法可以避免由粗制的（甲基）丙烯酸水溶液中所含的杂质引起的各种麻烦，例如，生成浮渣等，因此可以以比常规方法更高的纯度生产（甲基）丙烯酸。

3. 发明申请

US20070034363A1 Shell-and-tube type heat exchanger and method for production of (meth) acrylic acid by use of the exchange 有权
标题翻译：壳管型热交换器和通过使用交换生产（甲基）丙烯酸的方法
公开(公告)号：US20070034363A1
公开(公告)日：2007-02-15
申请号：US11584233
申请日：2006-10-20
申请人： Tetsuji Mitsumoto , Takeshi Nishimura , Sei Nakahara , Osamu Dodo
发明人： Tetsuji Mitsumoto , Takeshi Nishimura , Sei Nakahara , Osamu Dodo
IPC分类号： F28F9/22
CPC分类号： B01J8/067 , B01J2208/0015 , F28D7/1615 , F28F9/22 , F28F2009/029 , F28F2009/224
摘要： A shell-and-tube type heat exchanger of the smallest possible length necessary for heat exchange is disclosed which is capable of obtaining uniform distribution of flow of a shell side fluid and substantially eliminating the structural restriction imposed on the shell side. This shell-and-tube type heat exchanger is provided with one annular conduit furnished with not less than two partitions concurrently serving as an expansion joint for introducing and discharging a shell side fluid and allowing the flow path for said shell side fluid to be separated into an introducing part and a discharging part and which comprises a place having no array of heat-transfer tubes in the flow path for said shell side fluid. It prevents the equipment from necessitating an unnecessary enlargement due to the structural restriction on the shell side and enables the shell side fluid to produce a uniform flow.
摘要翻译：公开了一种能够获得壳侧流体的均匀流动分布并且基本上消除了对壳体侧面的结构限制的壳体管式热交换器，其具有热交换所需的尽可能小的长度。这种管壳型热交换器设置有一个环形导管，其具有不少于两个隔板，同时用作用于引入和排出壳侧流体的膨胀接头，并且允许将所述壳侧流体的流动路径分离成引入部分和排出部分，并且包括在用于所述壳侧流体的流动路径中不具有热传递管阵列的位置。它防止了由于壳体侧面的结构限制而使设备不必要地增大，并且使得壳侧流体能够产生均匀的流动。

4. 发明授权

US06431261B1 Shell and tube type heat exchanger 有权
公开(公告)号：US06431261B1
公开(公告)日：2002-08-13
申请号：US09733679
申请日：2000-12-08
申请人： Takeshi Nishimura , Yukihiro Matsumoto , Daisuke Nakamura , Masakatsu Mori , Osamu Dodo
发明人： Takeshi Nishimura , Yukihiro Matsumoto , Daisuke Nakamura , Masakatsu Mori , Osamu Dodo
IPC分类号： F28D700
摘要： The temperature distribution in a shell and tube type heat exchanger having an expansion joint is uniformized by improving the circulation efficiency of fluid in the shell side. The uniformization is attained by the heat exchanger having an invasion-preventing plate against the fluid in the shell side attached to the expansion joint installed around the periphery of the shell, and a method of catalytic gas phase oxidation reaction that uses the heat exchanger.

5. 发明授权

US07541490B2 Method for production of acrylic acid and apparatus for production of acrylic acid 有权
标题翻译：制备丙烯酸的方法和生产丙烯酸的设备
公开(公告)号：US07541490B2
公开(公告)日：2009-06-02
申请号：US11601417
申请日：2006-11-17
申请人： Kazuto Okazaki , Yukihiro Matsumoto , Kazuhiko Sakamoto , Osamu Dodo
发明人： Kazuto Okazaki , Yukihiro Matsumoto , Kazuhiko Sakamoto , Osamu Dodo
IPC分类号： C07C51/16 , C07C51/235
CPC分类号： C07C51/215 , B01J19/0013 , B01J2219/00087 , B01J2219/00103 , B01J2219/00108 , B01J2219/0011 , B01J2219/00126 , B01J2219/00128 , C07C51/252 , C07C57/04
摘要： Chilled coolant is prepared by liquid coolant utilizing the latent heat generated by a gasification of liquefied propylene, for example, and this chilled coolant is used in heat exchangers which are used in a process for production of acrylic acid or acrolein. This method allows effective utilization of the latent heat which used to be discarded and permits a reduction of energy consumption of cooling required separately in the step for production. By recovering the chilled coolant with the liquid coolant, it makes possible to stabilize the gasification of propylene, etc. and consequently stabilize the production of acrylic acid. This invention consists of providing the method for the production of acrylic acid, etc. and the apparatus which make effective use of the latent heat generated in the steps of production.
摘要翻译：例如，通过液化丙烯气化产生的潜热的液体冷却剂制备冷冻冷却剂，并且该冷却的冷却剂用于用于生产丙烯酸或丙烯醛的方法中的热交换器。该方法允许有效利用以前被废弃的潜热，并且可以在生产步骤中单独地降低需要的冷却能量消耗。通过用液体冷却剂回收冷却的冷却剂，可以稳定丙烯等的气化，从而稳定丙烯酸的生产。本发明提供了生产丙烯酸等的方法和有效利用在生产步骤中产生的潜热的装置。

6. 发明授权

US06891061B1 Packed column and polymerizable compound treating method using the same 有权
标题翻译：填充柱和使用其的可聚合化合物处理方法
公开(公告)号：US06891061B1
公开(公告)日：2005-05-10
申请号：US09688169
申请日：2000-10-16
申请人： Takeshi Nishimura , Yukihiro Matsumoto , Sei Nakahara , Osamu Dodo
发明人： Takeshi Nishimura , Yukihiro Matsumoto , Sei Nakahara , Osamu Dodo
IPC分类号： B01D3/16 , B01D3/14 , B01D3/32 , B01J10/00 , B01J19/30 , B01J19/32 , C07C51/44 , C07C57/07 , C07C67/54 , C07C69/54 , C07C67/48 , C07C51/42
CPC分类号： B01J19/305 , B01D3/324 , B01D3/326 , B01J19/325 , B01J2219/185 , B01J2219/3221 , B01J2219/32213 , B01J2219/32272 , B01J2219/32275 , B01J2219/3325
摘要： Provided are a packed column arranged so as to be capable of effectively preventing polymerization of a polymerizable compound such as a (meth)acrylic acid in treating the compound, and a method for treating a polymerizable compound using the packed column. The packed column, which is provided with a packing support plate and is filled with a packing on the packing support plate, is arranged so as to include a packing layer (B) having a greater percentage of voids than that of a packing layer (A), between the packing support plate and the packing layer (A).
摘要翻译：提供了一种填充柱，其布置成能够有效地防止在处理该化合物时诸如（甲基）丙烯酸之类的可聚合化合物的聚合，以及使用填充柱处理可聚合化合物的方法。填充柱设置有填充支撑板并且填充在填料支撑板上的填料，以包括具有比填充层（A（A））更大百分比的空隙的填充层（B）），在包装支撑板和包装层（A）之间。

7. 发明授权

US06848501B2 Method for preventing plate type heat exchanger from blockage 失效
标题翻译：防止板式换热器堵塞的方法
公开(公告)号：US06848501B2
公开(公告)日：2005-02-01
申请号：US10356428
申请日：2003-01-31
申请人： Harunori Hirao , Yukihiro Matsumoto , Sei Nakahara , Osamu Dodo , Tetsuji Mitsumoto , Takeshi Nishimura , Kazuhiko Sakamoto , Hiroo Iwato
发明人： Harunori Hirao , Yukihiro Matsumoto , Sei Nakahara , Osamu Dodo , Tetsuji Mitsumoto , Takeshi Nishimura , Kazuhiko Sakamoto , Hiroo Iwato
IPC分类号： B01J19/00 , F28D7/16 , F28D9/00 , F28F19/00 , F28F27/02
CPC分类号： F28D9/0068 , B01J19/002 , B01J2219/00252 , F28D7/1607 , F28D7/1623 , F28D9/0062 , F28F9/0278 , F28F19/00 , F28F2250/102
摘要： In an apparatus provided with a plate type heat exchanger as a heater and/or a cooler and operated to treat a gas containing an easily blocking substance, a method for preventing the plate type heat exchanger from being blocked is disclosed which is characterized by i) setting the width of a flow path on a plate of the plate type heat exchanger in the apparatus in a range of 6-25 mm and ii) setting the average flow rate of the gas passing the plate type heat exchanger in the apparatus per unit cross-sectional area of the flow path on the plate in the range of 3-15 m/s. In the exchange of heat of an easily blocking substance by the use of a plate type heat exchanger, a method for preventing the plate type heat exchanger from blockage is disclosed which has the plate type heat exchanger provided in the port for introducing a gas containing an easily blocking substance with a gas dispersion plate. This invention, in the heat exchange of an effluent gas emanating from a process for the production of (meth)acrylic acid or an ester thereof or the disposal of the gas, significantly allays blockage of the interior of the plate type heat exchanger.
摘要翻译：在设置有作为加热器和/或冷却器的板式热交换器并且被操作以处理含有易阻塞物质的气体的装置中，公开了一种防止板式热交换器被堵塞的方法，其特征在于i）将设备中板式热交换器的板上的流路宽度设置在6-25mm的范围内，以及ii）将通过板式热交换器的气体的平均流量设置在每单位十字的装置中板上流路的截面面积在3-15 m / s的范围内。在通过使用板式热交换器交换容易堵塞物质的热的情况下，公开了一种防止板式热交换器堵塞的方法，其具有设置在用于引入含有用气体分散板容易地堵塞物质。本发明在从（甲基）丙烯酸或其酯的制备方法产生的流出气体的热交换或气体的处理中显着地阻止了板式热交换器的内部堵塞。

8. 发明授权

US06808689B1 Reactor for catalytic gas phase oxidation 有权
标题翻译：催化气相氧化反应器
公开(公告)号：US06808689B1
公开(公告)日：2004-10-26
申请号：US09652209
申请日：2000-08-30
申请人： Yukihiro Matsumoto , Masakatsu Mori , Masatsuga Kitaura , Osamu Dodo , Michio Tanimoto
发明人： Yukihiro Matsumoto , Masakatsu Mori , Masatsuga Kitaura , Osamu Dodo , Michio Tanimoto
IPC分类号： B01J804
CPC分类号： C07C45/35 , B01J8/067 , B01J2208/00212 , B01J2208/00221 , B01J2208/0023 , C07C51/252 , C07C47/22 , C07C57/04
摘要： The temperature distribution of a heating medium in the reactor is allayed and the occurrence of hot spots is repressed. In a shell-and-tube type reactor provided with donut type and disc type baffle plates, reaction tubes are disposed even in the holes formed in the donut type baffle plates and an empty space devoid of a configuration of the reaction tubes is formed at the center of the shell. According to this invention, (meth)acrylic acid and/or (meth)acrolein can be produced at a low energy by catalytic gas phase oxidation of propylene- or isobutylene-containing gas.
摘要翻译：反应器中加热介质的温度分布被消除，并且热点的发生被抑制。在设置有环形型和盘式挡板的管壳型反应器中，反应管甚至设置在形成于环形挡板中的孔中，并且在反应管的形成空间处形成反应管的形状壳的中心。根据本发明，通过催化气相氧化含丙烯或异丁烯的气体，可以在低能量下生产（甲基）丙烯酸和/或（甲基）丙烯醛。

9. 发明授权

US06613940B1 Method for catalytic gas phase oxidation 失效
标题翻译：催化气相氧化方法
公开(公告)号：US06613940B1
公开(公告)日：2003-09-02
申请号：US09648950
申请日：2000-08-25
申请人： Takeshi Nishimura , Masakatsu Mori , Masatsugu Kitaura , Osamu Dodo , Daisuke Nakamura
发明人： Takeshi Nishimura , Masakatsu Mori , Masatsugu Kitaura , Osamu Dodo , Daisuke Nakamura
IPC分类号： C07C5116
CPC分类号： B01J8/008 , B01J8/067 , B01J2208/00212 , B01J2208/00221 , B01J2208/00256 , C07C45/35 , C07C51/215 , C07C51/252 , C07C51/255 , C07C51/265 , C07C47/22 , C07C57/145 , C07C63/16 , C07C57/02
摘要： In the reaction of catalytic gas phase oxidation by means of a shell-and-tube type reactor adapted to circulate a heating medium to the shell of the reactor through the medium of a circulation device connecting an annular conduit connected thereto, a method for the catalytic gas phase oxidation characterized by subjecting a part of the heating medium extracted from the shell of the reactor to heat exchange, introducing the heating medium resulting from the heat exchange into the proximity of a heating medium circulation inlet on the inlet side of the circulation device or the annular conduit on the outlet side of the reactor. The flow rate of the heating medium after the heat exchange is preferred to be in the range of 2-40 vol. % based on the flow rate of the heating medium within the shell of the reactor and the temperature difference of the heating medium at the inlet and the outlet to be in the range of 15-150° C. According to this invention, it is made possible to reduce evenly the hot spots in the reaction tubes, improve the yield of the product aimed at, and implement a reaction of catalytic gas phase oxidation of propylene or isobutylene.
摘要翻译：在通过壳管式反应器进行催化气相氧化的反应中，该反应器适于通过连接连接其的环形导管的循环装置的介质将加热介质循环到反应器的壳体，催化剂的方法气相氧化特征在于使从反应器壳体中提取的一部分加热介质进行热交换，将由热交换产生的加热介质引入循环装置入口侧的加热介质循环入口附近，或反应器出口侧的环形导管。热交换后的加热介质的流量优选为2-40体积％。基于反应器壳体内的加热介质的流量，入口和出口处的加热介质的温度差在15-150℃的范围内。根据本发明，制成可能均匀地减少反应管中的热点，提高目标产品的产率，并实现丙烯或异丁烯的催化气相氧化反应。

10. 发明授权

US07468167B2 Method for starting up reactor and reactor system 有权
标题翻译：启动反应堆和反应堆系统的方法
公开(公告)号：US07468167B2
公开(公告)日：2008-12-23
申请号：US11221213
申请日：2005-09-07
申请人： Yukihiro Matsumoto , Takeshi Nishimura , Hideki Sogabe , Kazuhiko Sakamoto , Osamu Dodo
发明人： Yukihiro Matsumoto , Takeshi Nishimura , Hideki Sogabe , Kazuhiko Sakamoto , Osamu Dodo
IPC分类号： F28D7/00 , F28D21/00 , F28D15/00 , C07C53/00
CPC分类号： F28D7/0066 , B01J8/067 , B01J2208/00212 , B01J2208/00256 , B01J2208/00716 , B01J2219/00006 , C07C45/35 , C07C51/252 , C07C47/22 , C07C57/04
摘要： A method for quickly starting up a reactor and a reactor system therefor are provided. A shell-and-tube reactor in the system is adapted to circulate a heat medium having a solid point in the range of 50-250° C. to the outside of the reaction tubes and characterized by initiating temperature elevation of the reactor by introducing a gas of a temperature in the range of 100-400° C. to the reaction tubes' side and then circulating the heat medium in a heated state to the outside of the reaction tubes. By introducing a gas of an elevated temperature preparatorily to the reaction tubes, it is made possible to prevent the heat medium after circulation from being solidified again and enable the reactor to be quickly started up.
摘要翻译：提供了一种用于快速启动反应器及其反应器系统的方法。系统中的管壳式反应器适于将具有在50-250℃范围内的固点的热介质循环到反应管的外部，并且其特征在于通过引入反应器的温度升高将温度在100-400℃范围内的气体加到反应管侧，然后将加热的热介质循环到反应管的外部。通过将升温的气体预先引入反应管，可以防止循环后的热介质再次固化，使反应器快速启动。

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