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1. 发明授权

US07147048B2 Shell-and-tube type heat exchanger and method for production of (meth) acrylic acid by use of the exchange 失效
公开(公告)号：US07147048B2
公开(公告)日：2006-12-12
申请号：US10254379
申请日：2002-09-25
申请人： Tetsuji Mitsumoto , Takeshi Nishimura , Sei Nakahara , Osamu Dodo
发明人： Tetsuji Mitsumoto , Takeshi Nishimura , Sei Nakahara , Osamu Dodo
IPC分类号： F28D7/10 , F28D7/00 , F28F9/02 , C07C51/16
CPC分类号： B01J8/067 , B01J2208/0015 , F28D7/1615 , F28F9/22 , F28F2009/029 , F28F2009/224
摘要： A shell-and-tube type heat exchanger of the smallest possible length necessary for heat exchange is disclosed which is capable of obtaining uniform distribution of flow of a shell side fluid and substantially eliminating the structural restriction imposed on the shell side. This shell-and-tube type heat exchanger is provided with one annular conduit furnished with not less than two partitions concurrently serving as an expansion joint for introducing and discharging a shell side fluid and allowing the flow path for said shell side fluid to be separated into an introducing part and a discharging part and which comprises a place having no array of heat-transfer tubes in the flow path for said shell side fluid. It prevents the equipment from necessitating an unnecessary enlargement due to the structural restriction on the shell side and enables the shell side fluid to produce a uniform flow.

2. 发明申请

US20070034363A1 Shell-and-tube type heat exchanger and method for production of (meth) acrylic acid by use of the exchange 有权
标题翻译：壳管型热交换器和通过使用交换生产（甲基）丙烯酸的方法
公开(公告)号：US20070034363A1
公开(公告)日：2007-02-15
申请号：US11584233
申请日：2006-10-20
申请人： Tetsuji Mitsumoto , Takeshi Nishimura , Sei Nakahara , Osamu Dodo
发明人： Tetsuji Mitsumoto , Takeshi Nishimura , Sei Nakahara , Osamu Dodo
IPC分类号： F28F9/22
CPC分类号： B01J8/067 , B01J2208/0015 , F28D7/1615 , F28F9/22 , F28F2009/029 , F28F2009/224
摘要： A shell-and-tube type heat exchanger of the smallest possible length necessary for heat exchange is disclosed which is capable of obtaining uniform distribution of flow of a shell side fluid and substantially eliminating the structural restriction imposed on the shell side. This shell-and-tube type heat exchanger is provided with one annular conduit furnished with not less than two partitions concurrently serving as an expansion joint for introducing and discharging a shell side fluid and allowing the flow path for said shell side fluid to be separated into an introducing part and a discharging part and which comprises a place having no array of heat-transfer tubes in the flow path for said shell side fluid. It prevents the equipment from necessitating an unnecessary enlargement due to the structural restriction on the shell side and enables the shell side fluid to produce a uniform flow.
摘要翻译：公开了一种能够获得壳侧流体的均匀流动分布并且基本上消除了对壳体侧面的结构限制的壳体管式热交换器，其具有热交换所需的尽可能小的长度。这种管壳型热交换器设置有一个环形导管，其具有不少于两个隔板，同时用作用于引入和排出壳侧流体的膨胀接头，并且允许将所述壳侧流体的流动路径分离成引入部分和排出部分，并且包括在用于所述壳侧流体的流动路径中不具有热传递管阵列的位置。它防止了由于壳体侧面的结构限制而使设备不必要地增大，并且使得壳侧流体能够产生均匀的流动。

3. 发明授权

US06848501B2 Method for preventing plate type heat exchanger from blockage 失效
标题翻译：防止板式换热器堵塞的方法
公开(公告)号：US06848501B2
公开(公告)日：2005-02-01
申请号：US10356428
申请日：2003-01-31
申请人： Harunori Hirao , Yukihiro Matsumoto , Sei Nakahara , Osamu Dodo , Tetsuji Mitsumoto , Takeshi Nishimura , Kazuhiko Sakamoto , Hiroo Iwato
发明人： Harunori Hirao , Yukihiro Matsumoto , Sei Nakahara , Osamu Dodo , Tetsuji Mitsumoto , Takeshi Nishimura , Kazuhiko Sakamoto , Hiroo Iwato
IPC分类号： B01J19/00 , F28D7/16 , F28D9/00 , F28F19/00 , F28F27/02
CPC分类号： F28D9/0068 , B01J19/002 , B01J2219/00252 , F28D7/1607 , F28D7/1623 , F28D9/0062 , F28F9/0278 , F28F19/00 , F28F2250/102
摘要： In an apparatus provided with a plate type heat exchanger as a heater and/or a cooler and operated to treat a gas containing an easily blocking substance, a method for preventing the plate type heat exchanger from being blocked is disclosed which is characterized by i) setting the width of a flow path on a plate of the plate type heat exchanger in the apparatus in a range of 6-25 mm and ii) setting the average flow rate of the gas passing the plate type heat exchanger in the apparatus per unit cross-sectional area of the flow path on the plate in the range of 3-15 m/s. In the exchange of heat of an easily blocking substance by the use of a plate type heat exchanger, a method for preventing the plate type heat exchanger from blockage is disclosed which has the plate type heat exchanger provided in the port for introducing a gas containing an easily blocking substance with a gas dispersion plate. This invention, in the heat exchange of an effluent gas emanating from a process for the production of (meth)acrylic acid or an ester thereof or the disposal of the gas, significantly allays blockage of the interior of the plate type heat exchanger.
摘要翻译：在设置有作为加热器和/或冷却器的板式热交换器并且被操作以处理含有易阻塞物质的气体的装置中，公开了一种防止板式热交换器被堵塞的方法，其特征在于i）将设备中板式热交换器的板上的流路宽度设置在6-25mm的范围内，以及ii）将通过板式热交换器的气体的平均流量设置在每单位十字的装置中板上流路的截面面积在3-15 m / s的范围内。在通过使用板式热交换器交换容易堵塞物质的热的情况下，公开了一种防止板式热交换器堵塞的方法，其具有设置在用于引入含有用气体分散板容易地堵塞物质。本发明在从（甲基）丙烯酸或其酯的制备方法产生的流出气体的热交换或气体的处理中显着地阻止了板式热交换器的内部堵塞。

4. 发明授权

US07326811B2 Method for production of (meth)acrylic acid by use of a shell-and-tube heat exchanger 有权
标题翻译：使用管壳式热交换器生产（甲基）丙烯酸的方法
公开(公告)号：US07326811B2
公开(公告)日：2008-02-05
申请号：US11584233
申请日：2006-10-20
申请人： Tetsuji Mitsumoto , Takeshi Nishimura , Sei Nakahara , Osamu Dodo
发明人： Tetsuji Mitsumoto , Takeshi Nishimura , Sei Nakahara , Osamu Dodo
IPC分类号： C07C51/42 , C07C51/16
CPC分类号： B01J8/067 , B01J2208/0015 , F28D7/1615 , F28F9/22 , F28F2009/029 , F28F2009/224
摘要： A shell-and-tube type heat exchanger of the smallest possible length necessary for heat exchange is disclosed which is capable of obtaining uniform distribution of flow of a shell side fluid and substantially eliminating the structural restriction imposed on the shell side. This shell-and-tube type heat exchanger is provided with one annular conduit furnished with not less than two partitions concurrently serving as an expansion joint for introducing and discharging a shell side fluid and allowing the flow path for said shell side fluid to be separated into an introducing part and a discharging part and which comprises a place having no array of heat-transfer tubes in the flow path for said shell side fluid. It prevents the equipment from necessitating an unnecessary enlargement due to the structural restriction on the shell side and enables the shell side fluid to produce a uniform flow.
摘要翻译：公开了一种能够获得壳侧流体的均匀流动分布并且基本上消除了对壳体侧面的结构限制的壳体管式热交换器，其具有热交换所需的尽可能小的长度。这种管壳型热交换器设置有一个环形导管，其具有不少于两个隔板，同时用作用于引入和排出壳侧流体的膨胀接头，并且允许将所述壳侧流体的流动路径分离成引入部分和排出部分，并且包括在用于所述壳侧流体的流动路径中不具有热传递管阵列的位置。它防止了由于壳体侧面的结构限制而使设备不必要地增大，并且使得壳侧流体能够产生均匀的流动。

5. 发明授权

US07048834B2 Method for purification of acrylic acid 有权
标题翻译：纯化丙烯酸的方法
公开(公告)号：US07048834B2
公开(公告)日：2006-05-23
申请号：US09745896
申请日：2000-12-21
申请人： Yoshitake Ishii , Kouji Ueno , Kazuhiko Sakamoto , Sei Nakahara , Masatoshi Ueoka , Tetsuji Mitsumoto , Takeshi Nishimura , Mamoru Takamura , Hisao Nakama
发明人： Yoshitake Ishii , Kouji Ueno , Kazuhiko Sakamoto , Sei Nakahara , Masatoshi Ueoka , Tetsuji Mitsumoto , Takeshi Nishimura , Mamoru Takamura , Hisao Nakama
IPC分类号： B01D3/34 , B01D3/42 , C07C51/44 , C07C51/487 , C07C57/07
CPC分类号： C07C51/44 , C07C51/487 , C07C57/04
摘要： The present invention provides an industrially easy and economical method for purification of acrylic acid which enables to efficiently eliminate impurities from a crude acrylic acid containing aldehydes as the impurities while the formation of acrylic acid polymer is inhibited. The method for purification of acrylic acid includes the step of distilling a crude acrylic acid which is charged with an aldehyde treatment chemical, wherein the concentration ratio of furfural to acrolein by weight in the crude acrylic acid is adjusted so as to satisfy the following equation: (furfural concentration by weight)/(acrolein concentration by weight)≦100.
摘要翻译：本发明提供了一种工业上容易和经济的丙烯酸纯化方法，其能够在抑制丙烯酸聚合物形成的同时，有效地除去含粗醛的丙烯酸作为杂质的杂质。纯化丙烯酸的方法包括蒸馏装入醛处理化学品的粗丙烯酸的步骤，其中调整粗丙烯酸中的糠醛与丙烯醛的重量比，以满足下列等式：（糠醛浓度按重量计）/（丙烯醛浓度重量）<= 100。<？in-line-formula description =“In-line formula”end =“lead” “公式”end =“tail”？>

6. 发明授权

US06657079B1 Method for mixing gases and apparatus therefor 失效
标题翻译：气体混合方法及其设备
公开(公告)号：US06657079B1
公开(公告)日：2003-12-02
申请号：US09640630
申请日：2000-08-17
申请人： Tetsuji Mitsumoto , Tatsuaki Yoshimura , Takeshi Nishimura , Sei Nakahara
发明人： Tetsuji Mitsumoto , Tatsuaki Yoshimura , Takeshi Nishimura , Sei Nakahara
IPC分类号： C07C4534
CPC分类号： C07C45/35 , C07C45/33 , C07C47/22
摘要： A method for mixing a plurality of gases including forming a helical flow within a mixing vessel thereby allowing simplification of construction, avoiding pressure drop to the fullest possible extent, and expediting the mixture lest the volume of a gas within the explosion limits should increase, and an apparatus to be used for the method.
摘要翻译：一种用于混合多种气体的方法，包括在混合容器内形成螺旋流，从而允许简化构造，避免压力下降到最大可能程度，并加速混合物，以免爆炸极限内的气体体积增加，用于该方法的装置。

7. 发明授权

US07282118B2 Method for production of easily polymerizable substance and purification apparatus 有权
标题翻译：易聚合物质的制造方法和净化装置
公开(公告)号：US07282118B2
公开(公告)日：2007-10-16
申请号：US09828093
申请日：2001-04-06
申请人： Tetsuji Mitsumoto , Takeshi Nishimura , Sei Nakahara , Hidefumi Haramaki
发明人： Tetsuji Mitsumoto , Takeshi Nishimura , Sei Nakahara , Hidefumi Haramaki
IPC分类号： B01D3/32 , C07C51/42
CPC分类号： B01D3/225 , B01D3/326 , Y10S203/11
摘要： This invention resides in providing a method for the prevention of possible polymerization of the easily polymerizable substance during the purification thereof by a column provided with (a) at least one tray directly fixed to a support ring with a bolt and a nut and/or (b) at least one tray fixed to a support ring with a vertical clamp or a distillation column provided in the lower part thereof with a splash collision plate.
摘要翻译：本发明在于提供一种防止易于聚合的物质在其净化过程中可能的聚合的方法，所述塔具有（a）至少一个直接用螺栓和螺母固定在支撑环上的托盘和/或（ b）至少一个托架，其具有垂直夹具或蒸馏塔固定在支撑环上，该塔板在其下部设有飞溅碰撞板。

8. 发明授权

US06891061B1 Packed column and polymerizable compound treating method using the same 有权
标题翻译：填充柱和使用其的可聚合化合物处理方法
公开(公告)号：US06891061B1
公开(公告)日：2005-05-10
申请号：US09688169
申请日：2000-10-16
申请人： Takeshi Nishimura , Yukihiro Matsumoto , Sei Nakahara , Osamu Dodo
发明人： Takeshi Nishimura , Yukihiro Matsumoto , Sei Nakahara , Osamu Dodo
IPC分类号： B01D3/16 , B01D3/14 , B01D3/32 , B01J10/00 , B01J19/30 , B01J19/32 , C07C51/44 , C07C57/07 , C07C67/54 , C07C69/54 , C07C67/48 , C07C51/42
CPC分类号： B01J19/305 , B01D3/324 , B01D3/326 , B01J19/325 , B01J2219/185 , B01J2219/3221 , B01J2219/32213 , B01J2219/32272 , B01J2219/32275 , B01J2219/3325
摘要： Provided are a packed column arranged so as to be capable of effectively preventing polymerization of a polymerizable compound such as a (meth)acrylic acid in treating the compound, and a method for treating a polymerizable compound using the packed column. The packed column, which is provided with a packing support plate and is filled with a packing on the packing support plate, is arranged so as to include a packing layer (B) having a greater percentage of voids than that of a packing layer (A), between the packing support plate and the packing layer (A).
摘要翻译：提供了一种填充柱，其布置成能够有效地防止在处理该化合物时诸如（甲基）丙烯酸之类的可聚合化合物的聚合，以及使用填充柱处理可聚合化合物的方法。填充柱设置有填充支撑板并且填充在填料支撑板上的填料，以包括具有比填充层（A（A））更大百分比的空隙的填充层（B）），在包装支撑板和包装层（A）之间。

9. 发明授权

US06642414B2 Method for production of (meth) acrylic acid 失效
标题翻译：（甲基）丙烯酸的制造方法
公开(公告)号：US06642414B2
公开(公告)日：2003-11-04
申请号：US09772458
申请日：2001-01-30
申请人： Tetsuji Mitsumoto , Yukihiro Matsumoto , Sei Nakahara , Tatsuaki Yoshimura
发明人： Tetsuji Mitsumoto , Yukihiro Matsumoto , Sei Nakahara , Tatsuaki Yoshimura
IPC分类号： C07C5142
CPC分类号： C07C51/44 , C07C51/252 , C07C51/48 , C07C57/04
摘要： A method for producing (meth)acrylic acid of high purity by repressing formation of a polymer possibly generated during the course of production is disclosed. The production is accomplished by returning the waste liquid generated at the step of the addition of aldehyde treating agents (d) to the step of the absorption (b) and/or the step of separation (c).
摘要翻译：公开了通过抑制可能在生产过程中产生的聚合物的形成来生产高纯度（甲基）丙烯酸的方法。通过将在醛加工剂（d）的添加步骤中产生的废液返回到吸收步骤（b）和/或分离步骤（c）中来完成生产。

10. 发明申请

US20070003460A1 Reactor filled with solid particle and gas-phase catalytic oxidation with the reactor 有权
标题翻译：反应器用反应器填充固体颗粒和气相催化氧化
公开(公告)号：US20070003460A1
公开(公告)日：2007-01-04
申请号：US11498426
申请日：2006-08-03
申请人： Yukihiro Matsumoto , Takeshi Nishimura , Sei Nakahara , Naoto Kasaya
发明人： Yukihiro Matsumoto , Takeshi Nishimura , Sei Nakahara , Naoto Kasaya
IPC分类号： B01J8/04 , B01J8/08 , B01J10/00
CPC分类号： B01J8/067 , B01J8/001 , B01J2208/00044 , B01J2208/00061 , B01J2208/00212 , B01J2208/00513 , B01J2208/00539 , B01J2208/021 , B01J2208/025 , B01J2219/00777
摘要： A shell-and tube reactor including at least one reaction tube with a measuring means, substantially same solid particles being filled in the reaction tubes with or without the measuring means, a length of the filled solid particle layer, and a pressure drop thereof while passing a gas through the reaction tube, per each reaction tube, being substantially the same, respectively. By measuring the temperature of the catalyst particle layer, such a temperature as a representative can be gasped.
摘要翻译：包括具有测量装置的至少一个反应管的管壳式反应器，在具有或不具有测量装置的反应管中填充基本相同的固体颗粒，填充的固体颗粒层的长度及其通过时的压降通过反应管的每个反应管的气体分别基本相同。通过测量催化剂颗粒层的温度，可以将诸如代表性的温度气化。

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