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1. 发明授权

US07550534B2 Thermoplastic method, composition, and article 有权
标题翻译：热塑性方法，组成和制品
公开(公告)号：US07550534B2
公开(公告)日：2009-06-23
申请号：US11281306
申请日：2005-11-16
申请人： Xinyu Zhao , Vijay Mhetar , Thomas J. Hartle
发明人： Xinyu Zhao , Vijay Mhetar , Thomas J. Hartle
IPC分类号： C08L53/02
CPC分类号： C08L71/12 , C08L53/025 , C08L2205/02 , C08L2666/24 , C08L2666/02
摘要： A thermoplastic composition includes a poly(arylene ether), a hydrogenated block copolymer, a pre-blend of a thermoplastic vulcanizate and a hydrogenated block copolymer, an ethylene/alpha-olefin copolymer, and a hydrocarbon resin. Pre-blending the thermoplastic vulcanizate with a portion of the hydrogenated block copolymer was found to markedly improve the flame resistance and physical properties of the composition compared to those of compositions in which the thermoplastic vulcanizate and hydrogenated block copolymer are separately added to the final compounding process. Addition of hydrocarbon resin further improves the balance of flame retardancy and physical properties.
摘要翻译：热塑性组合物包括聚（亚芳基醚），氢化嵌段共聚物，热塑性硫化橡胶和氢化嵌段共聚物的预共混物，乙烯/α-烯烃共聚物和烃树脂。发现将热塑性硫化橡胶与一部分氢化嵌段共聚物预先混合，显着地提高了组合物的阻燃性和物理性能，与将热塑性硫化橡胶和氢化嵌段共聚物分别加入到最终配混方法中的组合物相比。加入烃树脂进一步提高了阻燃性和物理性能的平衡。

2. 发明授权

US07056980B2 Poly(arylene ether) compositions, articles thereof and methods of making them 失效
标题翻译：聚（亚芳基醚）组合物，其制品及其制备方法
公开(公告)号：US07056980B2
公开(公告)日：2006-06-06
申请号：US10604098
申请日：2003-06-26
申请人： Adeyinka Adedeji , Thomas J. Hartle , John C. Haylock , Vijay Mhetar , Ganesh Kannan
发明人： Adeyinka Adedeji , Thomas J. Hartle , John C. Haylock , Vijay Mhetar , Ganesh Kannan
IPC分类号： C08L53/00
CPC分类号： C08L71/123 , C08L23/02 , C08L25/06 , C08L53/02 , C08L71/12 , C08L2666/02 , C08L2666/24 , C08L2666/04
摘要： A composition comprising poly(arylene ether) resin and a hydrogenated block copolymer of an alkenyl aromatic compound and a conjugated diene, wherein the hydrogenated block copolymer has up to about 20 percent residual pendant aliphatic unsaturation and at least about 30 percent residual in-chain aliphatic unsaturation.
摘要翻译：包含聚（亚芳基醚）树脂和烯基芳族化合物和共轭二烯的氢化嵌段共聚物的组合物，其中氢化嵌段共聚物具有至多约20％的残余侧链脂肪族不饱和度和至少约30％的残留的链内脂族不饱和度

3. 发明授权

US07022765B2 Method for the preparation of a poly(arylene ether)-polyolefin composition, and composition prepared thereby 失效
标题翻译：聚（亚芳基醚） - 聚烯烃组合物的制备方法和由其制备的组合物
公开(公告)号：US07022765B2
公开(公告)日：2006-04-04
申请号：US10754126
申请日：2004-01-09
申请人： Adeyinka Adedeji , Thomas J. Hartle
发明人： Adeyinka Adedeji , Thomas J. Hartle
IPC分类号： C08L53/00
CPC分类号： C08L53/00 , C08F255/00 , C08J3/005 , C08J2371/12 , C08L23/10 , C08L23/12 , C08L25/06 , C08L51/06 , C08L53/02 , C08L53/025 , C08L71/12 , C08L2205/02 , C08L2205/03 , C08L2205/035 , C08L2205/08 , C08L2666/24 , C08L2666/22 , C08L2666/02 , C08L2666/04
摘要： A poly(arylene ether)-polyolefin composition is prepared by melt-blending a poly(arylene ether) and a compatibilizer to form a first blend, and melt-blending the first blend and a polyolefin to form a second blend. The composition lacks an unhydrogenated block copolymer, a poly(alkenyl aromatic) resin, or both. Multiple mixing elements, low throughput, and high extruder rotations per minute may be used to achieve high energy mixing of the first and second blends. Compositions prepared by the method exhibit an improved balance of impact strength, stiffness, and heat resistance, as well as reduced variability of physical properties.
摘要翻译：聚（亚芳基醚） - 聚烯烃组合物通过熔融共混聚（亚芳基醚）和增容剂以形成第一共混物并熔融共混第一共混物和聚烯烃以形成第二共混物来制备。该组合物缺少未氢化的嵌段共聚物，聚（烯基芳族）树脂或两者。可以使用多个混合元件，低通量和每分钟高的挤出机旋转以实现第一和第二共混物的高能量混合。通过该方法制备的组合物表现出改善的冲击强度，刚度和耐热性的平衡，以及物理性能的变化性降低。

4. 发明授权

US06660794B2 Glass-filled poly(arylene ether)-polyolefin composition and articles derived therefrom 有权
标题翻译：玻璃填充聚（亚芳基醚） - 聚烯烃组合物及其衍生物
公开(公告)号：US06660794B2
公开(公告)日：2003-12-09
申请号：US09682926
申请日：2001-11-01
申请人： Adeyinka Adedeji , Thomas J. Hartle , John C. Haylock
发明人： Adeyinka Adedeji , Thomas J. Hartle , John C. Haylock
IPC分类号： C08L5300
CPC分类号： C08L71/123 , C08L2666/04 , C08L2666/24
摘要： A reinforced thermoplastic composition includes specific amounts of a poly(arylene ether), a homopolymer of an alkenyl aromatic monomer, a polyolefin, a hydrogenated block copolymer with a high styrene content, an unhydrogenated block copolymer, and, glass fibers. The composition exhibits extremely high stiffness while maintaining high impact strength.
摘要翻译：增强的热塑性组合物包括特定量的聚（亚芳基醚），烯基芳族单体的均聚物，聚烯烃，具有高苯乙烯含量的氢化嵌段共聚物，未氢化的嵌段共聚物和玻璃纤维。该组合物在保持高冲击强度的同时显示出非常高的刚度。

5. 发明授权

US06339166B1 Phosphinimine modification of organic polymers and silicones 失效
标题翻译：有机聚合物和硅氧烷的磷腈改性
公开(公告)号：US06339166B1
公开(公告)日：2002-01-15
申请号：US09850259
申请日：2001-05-07
申请人： Harry R. Allcock , Thomas J. Hartle , Michael B. McIntosh , Nicolas J. Sunderland , Robbyn Prange , Jonathan P. Taylor
发明人： Harry R. Allcock , Thomas J. Hartle , Michael B. McIntosh , Nicolas J. Sunderland , Robbyn Prange , Jonathan P. Taylor
IPC分类号： C07F708
CPC分类号： C07F9/65815 , C08C19/22 , C08C19/24 , C08F8/30 , C08F8/40 , C08G77/395 , C08G77/42
摘要： Methods have been developed to produce phosphazene modified organic or siloxane polymers. The method includes (a) providing an organic or siloxane polymer comprising phosphine units, and (b) reacting the organic or siloxane polymer with a phosphazene azide compound under conditions wherein the phosphazene azide compound is bound to the phosphine unites in the polymer, thereby producing the phosphazene-modified organic or siloxane polymer. The organic polymer of step (a) is produced by reacting a first monomer comprising phosphine with a second monomer via free radical or anionic polymerization techniques to produce the organic polymer comprising phosphine units. The first and second monomers can be identical. A wide variety of organic polymer backbones can be modified using these techniques. The second monomer, for example, can be selected from monomers forming polyolefins, polydienes, polyacrylics, polyethylenes, polyvinyl chlorides, polyisoprenes, polystyrenes, polycaprolactam, poly(methyl)(meth)acrylates, and polypropylenes. Alternatively, the siloxane polymer of step (a) is produced by reacting a monomer comprising phosphine with a hydrosilicone polymer via hydrosilylation polymerization techniques to produce the siloxane polymer comprising phosphine units. These phosphazene modified organic and siloxane polymers are useful in a variety of applications, particularly as a fire retardant material.
摘要翻译：已经开发了制备磷腈改性的有机或硅氧烷聚合物的方法。该方法包括（a）提供包含磷化氢单元的有机或硅氧烷聚合物，和（b）在叠氮化磷化合物与聚合物中的膦化合物结合的条件下使有机或硅氧烷聚合物与叠氮化磷化合物反应，从而产生磷腈改性的有机或硅氧烷聚合物。通过自由基或阴离子聚合技术使包含膦的第一单体与第二单体反应制备步骤（a）的有机聚合物，以制备包含磷化氢单元的有机聚合物。第一和第二单体可以相同。使用这些技术可以改变各种各样的有机聚合物主链。例如，第二单体可以选自形成聚烯烃，聚二烯，聚丙烯酸，聚乙烯，聚氯乙烯，聚异戊二烯，聚苯乙烯，聚己内酰胺，聚（甲基）（甲基）丙烯酸酯和聚丙烯的单体。或者，步骤（a）的硅氧烷聚合物通过氢化硅烷化聚合技术使包含膦的单体与氢硅氧烷聚合物反应制备包含磷化氢单元的硅氧烷聚合物来制备。这些磷腈改性的有机和硅氧烷聚合物可用于各种应用，特别是作为阻燃材料。

6. 发明授权

US06872777B2 Poly(arylene ether)-polyolefin composition, method for the preparation thereof, and articles derived therefrom 有权
标题翻译：聚（亚芳基醚） - 聚烯烃组合物，其制备方法和由其衍生的制品
公开(公告)号：US06872777B2
公开(公告)日：2005-03-29
申请号：US10063336
申请日：2002-04-12
申请人： Adeyinka Adedeji , Thomas J. Hartle , John C. Haylock
发明人： Adeyinka Adedeji , Thomas J. Hartle , John C. Haylock
IPC分类号： C08J3/20 , C08K3/34 , C08K7/02 , C08L23/02 , C08L23/10 , C08L25/04 , C08L25/06 , C08L53/02 , C08L71/12 , C08L53/00
CPC分类号： C08L71/123 , C08L23/02 , C08L25/06 , C08L53/02 , C08L71/12 , C08L2666/02 , C08L2666/24 , C08L2666/04
摘要： A thermoplastic composition includes a poly(arylene ether), a poly(alkenyl aromatic) resin, a polyolefin, and a selectively hydrogenated block copolymer of an alkenyl aromatic compound and a conjugated diene having up to about 20 percent residual pendant aliphatic unsaturation and at least about 30 percent residual in-chain aliphatic unsaturation. The composition exhibits an excellent balance of stiffness, impact strength, and heat resistance and is useful for a variety of applications including automotive fascia, automotive front-end modules, automotive grill opening reinforcements, food trays, and power tool casings.
摘要翻译：热塑性组合物包括聚（亚芳基醚），聚（链烯基芳族）树脂，聚烯烃和链烯基芳族化合物和共轭二烯的选择性氢化嵌段共聚物，其具有至多约20％的残余侧链脂族不饱和度，并且至少约30％残留的链内脂族不饱和度。该组合物显示出刚度，冲击强度和耐热性的优异平衡，并且可用于各种应用，包括汽车面板，汽车前端模块，汽车格栅开口加强件，食品托盘和电动工具外壳。

7. 发明授权

US06855767B2 Poly(arylene ether)-polyolefin composition and articles derived therefrom 有权
标题翻译：聚（亚芳基醚） - 聚烯烃组合物及其衍生物
公开(公告)号：US06855767B2
公开(公告)日：2005-02-15
申请号：US09682921
申请日：2001-11-01
申请人： Adeyinka Adedeji , David R. Lamb , Vincent L. Lanning , Thomas J. Hartle , John C. Haylock
发明人： Adeyinka Adedeji , David R. Lamb , Vincent L. Lanning , Thomas J. Hartle , John C. Haylock
IPC分类号： C08L23/10 , C08L23/12 , C08L25/06 , C08L51/02 , C08L71/12 , C08L53/00
CPC分类号： C08L23/10 , C08L23/12 , C08L25/06 , C08L51/02 , C08L71/12 , C08L71/123 , C08L2666/04 , C08L2666/24 , C08L2666/02
摘要： A thermoplastic composition includes a poly(arylene ether), a poly(alkenyl aromatic) resin, a polyolefin, a hydrogenated block copolymer of alkenyl aromatic compound and a conjugated diene having an alkenyl aromatic content of about 40 to about 90 weight percent, and an unhydrogenated block copolymer of an alkenyl aromatic compound and a conjugated diene. The composition exhibits excellent stiffness-impact strength balance, low property variability, and long melt hang time.
摘要翻译：热塑性组合物包括聚（亚芳基醚），聚（烯基芳族）树脂，聚烯烃，链烯基芳族化合物的氢化嵌段共聚物和链烯基芳族含量为约40至约90重量％的共轭二烯，以及链烯基芳族化合物和共轭二烯的非氢化嵌段共聚物。该组合物显示出优异的刚度 - 冲击强度平衡，低的性能变化性和长的熔融悬挂时间。

8. 发明授权

US5914388A Synthesis polyphosphazenes with controlled molecular weight and polydisperity 失效
标题翻译：合成聚磷腈，具有受控的分子量和多不连续性
公开(公告)号：US5914388A
公开(公告)日：1999-06-22
申请号：US917069
申请日：1997-08-22
申请人： Harry R. Allcock , Christopher T. Morrissey , Ian Manners , Charles H. Honeyman , James M. Nelson , Chester A. Crane , Scott D. Reeves , A. Paul Primrose , Thomas J. Hartle , R. Prange
发明人： Harry R. Allcock , Christopher T. Morrissey , Ian Manners , Charles H. Honeyman , James M. Nelson , Chester A. Crane , Scott D. Reeves , A. Paul Primrose , Thomas J. Hartle , R. Prange
IPC分类号： C08G79/02
CPC分类号： C08G79/025
摘要： A process for the preparation of polyphosphazenes is provided that includes the cationic solution polymerization reaction of a phosphoranimine, using a main group or transition metal halide, or other appropriate halide salt, including a linear phosphazene salt of any chain length, or a preformed non-phosphazene polymer containing a main or transition metal chloride, as an initiator. In a preferred embodiment, triarmed-star polyphosphazenes having the formula N{RN(H)R'.sub.2 P--(N.dbd.PR'.sub.2).sub.n }.sub.3 are prepared via this method. Also, a methods for synthesis of the monomer Cl.sub.3 P.dbd.NSiMe.sub.3 and cyclic trimer N.sub.3 P.sub.3 X.sub.6 from the reactants N(SiR.sub.3).sub.3 and PX.sub.5 are also described.
摘要翻译：提供了一种制备聚磷腈的方法，其包括使用主要基团或过渡金属卤化物或其它合适的卤化物盐（包括任何链长的线性磷腈盐）或预成型非离子表面活性剂的正亚胺的阳离子溶液聚合反应，含有主要或过渡金属氯化物的磷腈聚合物作为引发剂。在优选的实施方案中，通过该方法制备具有式N {RN（H）R'2P-（N = PR'2）n} 3的三臂星型聚磷腈。此外，还描述了从反应物N（SiR 3）3和PX 5合成单体Cl 3 P = NSiMe 3和环状三聚体N 3 P 3 X 6的方法。

9. 发明授权

US06919399B2 Articles and sheets containing glass-filled poly(arylene ether)-polyolefin composition 有权
标题翻译：含有玻璃填充聚（亚芳基醚） - 聚烯烃组合物的制品和片材
公开(公告)号：US06919399B2
公开(公告)日：2005-07-19
申请号：US10248902
申请日：2003-02-28
申请人： Adeyinka Adedeji , Thomas J. Hartle , John C. Haylock
发明人： Adeyinka Adedeji , Thomas J. Hartle , John C. Haylock
IPC分类号： C08L71/12 , C08J5/10 , C08K3/40
CPC分类号： C08L71/123 , Y10T428/31645 , Y10T428/31833 , C08L2666/24 , C08L2666/04
摘要： An article includes a reinforced thermoplastic composition containing specific amounts of a poly(arylene ether), a homopolymer of an alkenyl aromatic monomer, a polyolefin, a hydrogenated block copolymer with a high styrene content, an unhydrogenated block copolymer, and glass fibers. The composition contributes very high stiffness and high impact strength to the article.
摘要翻译：一种制品包括含有特定量的聚（亚芳基醚），链烯基芳族单体的均聚物，聚烯烃，苯乙烯含量高的氢化嵌段共聚物，未氢化嵌段共聚物和玻璃纤维的增强热塑性组合物。该组合物对制品贡献非常高的刚度和高冲击强度。

10. 发明授权

US06861472B2 Poly(arylene ether)-polyolefin compositions and articles derived therefrom 有权
标题翻译：聚（亚芳基醚） - 聚烯烃组合物及其衍生物
公开(公告)号：US06861472B2
公开(公告)日：2005-03-01
申请号：US09682923
申请日：2001-11-01
申请人： Adeyinka Adedeji , Thomas J. Hartle , John C. Haylock
发明人： Adeyinka Adedeji , Thomas J. Hartle , John C. Haylock
IPC分类号： C08L23/10 , C08L23/12 , C08L25/06 , C08L51/02 , C08L71/12 , C08L53/00
CPC分类号： C08L23/10 , C08L23/12 , C08L25/06 , C08L51/02 , C08L71/12 , C08L71/123 , C08L2666/04 , C08L2666/24 , C08L2666/02
摘要： A thermoplastic composition includes specified amounts of a poly(arylene ether), a homopolymer of an alkenyl aromatic monomer, a polyolefin, a hydrogenated block copolymer, and an unhydrogenated block copolymer, but the composition is substantially free of any rubber-modified poly(alkenyl aromatic) resin. The composition provides high stiffness and high impact strength and is suitable for molding a variety of articles, including automotive underhood components.
摘要翻译：热塑性组合物包括指定量的聚（亚芳基醚），烯基芳族单体的均聚物，聚烯烃，氢化嵌段共聚物和未氢化的嵌段共聚物，但该组合物基本上不含任何橡胶改性的聚芳香族）树脂。该组合物提供高刚度和高冲击强度，并且适用于成型各种制品，包括汽车底座部件。

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