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1. 发明授权

US4804758A Preparation of 1,4-diazabicyclo[2.2.2]octanes 失效
标题翻译：制备1,4-二氮杂双环[2.2.2]辛烷
公开(公告)号：US4804758A
公开(公告)日：1989-02-14
申请号：US105537
申请日：1987-10-08
申请人： Wolfgang Hoelderich , Kurt Schneider , Walter Best
发明人： Wolfgang Hoelderich , Kurt Schneider , Walter Best
IPC分类号： C07D487/08
CPC分类号： C07D487/08 , Y02P20/582
摘要： 1,4-Diazabicyclo[2.2.2]octane and C-substituted 1,4-diazabicyclo[2.2.2]octanes of the formula (I) ##STR1## where R.sup.1 and R.sup.2 are each hydrogen or alkyl or alkenyl, each of 1 to 4 carbon atoms, are prepared from a heterocyclic amine of the formula (II) ##STR2## where R.sup.1 and R.sup.2 have the above meanings, R.sup.3 is hydrogen, hydroxyethyl or aminoethyl and X is hydroxyl or amino, in the presence of borosilicate and/or iron silicate zeolites as catalysts. Particularly suitable catalysts are the borosilicate and iron silicate zeolites of the pentasil type.
摘要翻译：式（I）的1,4-二氮杂双环[2.2.2]辛烷和C-取代的1,4-二氮杂双环[2.2.2]辛烷其中R 1和R 2各自为氢或烷基或链烯基，每个1-4个碳原子由式（II）的杂环胺制备，其中R 1和R 2具有上述含义，R 3是氢，羟乙基或氨基乙基，X是羟基或氨基，在硼硅酸盐和/或铁硅酸盐沸石作为催化剂的存在。特别合适的催化剂是pentasil型的硼硅酸盐和硅酸铁沸石。

2. 发明授权

US4874899A Preparation of unsaturated and saturated ketones 失效
标题翻译：不饱和和饱和酮的制备
公开(公告)号：US4874899A
公开(公告)日：1989-10-17
申请号：US206731
申请日：1988-06-15
申请人： Wolfgang Hoelderich , Leopold Hupfer , Kurt Schneider
发明人： Wolfgang Hoelderich , Leopold Hupfer , Kurt Schneider
IPC分类号： C07C45/59 , C07C49/11 , C07C49/203 , C07C49/21
CPC分类号： C07C45/59 , C07C49/11 , C07C49/203 , C07C49/21 , Y02P20/582
摘要： Unsaturated ketones of the formula ##STR1## and saturated ketones of the formula ##STR2## where R.sup.1, R.sup.2 and R.sup.3 are each hydrogen, alkyl of 1 to 12 carbon atoms or a cycloalkyl, aryl, aralkyl or alkylaryl radical which inturn may be substituted, or R.sup.1 and R.sup.3 or R.sup.2 and R.sup.3, together with the carbon atoms to which they are bonded, may form a cycloalkane, are prepared by a process in which a 5-methylene-1,3-dioxolanone which is substituted in the 4-position and is of the forumla ##STR3## where R.sup.1, R.sup.2 and R.sup.3 have the above meanings, (a) for the preparation of an unsaturated ketone, is converted in the presence of a zeolite, of a phosphate having a zeolite structure and/or of B, Ce, Fe, Zr or Sr phosphate as catalysts and (b) for the preparation of a saturated ketone, is converted in the presence of the same catalysts which additionally carry one or more hydrogenation components.
摘要翻译：其中R1，R2和R3各自为氢，1至12个碳原子的烷基或可以被取代的环烷基，芳基，芳烷基或烷基芳基，其中式（IMAGE）的不饱和酮和式“IMAGE”的饱和酮，或R 1和R 3或R 2和R 3与它们所键合的碳原子一起形成环烷烃的方法通过以下方法制备：其中在4-位被取代的5-亚甲基-1,3-二氧杂环戊酮并且是其中R1，R2和R3具有上述含义的论文（a），（a）制备不饱和酮的方法，在沸石存在下，具有沸石结构的磷酸盐和/或 B，Ce，Fe，Zr或Sr磷酸盐作为催化剂，（b）制备饱和酮的催化剂在相同催化剂的存在下转化，另外还含有一种或多种氢化组分。

3. 发明授权

US4885395A Preparation of alpha, beta-unsaturated ketones 失效
标题翻译：制备α，β-不饱和酮
公开(公告)号：US4885395A
公开(公告)日：1989-12-05
申请号：US100846
申请日：1987-09-25
申请人： Wolfgang Hoelderich , Kurt Schneider , Leopold Hupfer
发明人： Wolfgang Hoelderich , Kurt Schneider , Leopold Hupfer
IPC分类号： B01J29/04 , B01J29/40 , B01J29/85 , C07C45/66 , C07C45/67
CPC分类号： B01J29/85 , B01J29/04 , B01J29/40 , C07C45/66 , C07C45/673 , C07C45/676 , Y02P20/582
摘要： Alpha,beta-unsaturated ketones of the formula (I) ##STR1## where R.sup.1, R.sup.2 and R.sup.3 are each hydrogen, alkyl, alkenyl of 1 to 12 carbon atoms, cycloalkyl, aryl, aralkyl or alkylaryl, are prepared by converting the corresponding .alpha.-hydroxy, alkoxy or carboxy compound in the presence of an acidic catalyst.Preferred starting materials are 3-methyl-3-hydroxy-butan-2-one, 3-methyl-3-hydroxypentan-2-one and 3-pentamethylene-3-hydroxypropan-2-one, and preferred catalysts are zeolites of the pentasil type.
摘要翻译：式（I）的α，β-不饱和酮其中R 1，R 2和R 3各自为氢，具有1至12个碳原子的烷基，烯基，环烷基，芳基，芳烷基或烷芳基，其通过转化在酸性催化剂存在下，相应的α-羟基，烷氧基或羧基化合物。优选的原料是3-甲基-3-羟基 - 丁-2-酮，3-甲基-3-羟基戊-2-酮和3-五亚甲基-3-羟基丙-2-酮，优选的催化剂是pentasil的沸石类型。

4. 发明授权

US4866210A Preparation of ketones 失效
标题翻译：酮的制备
公开(公告)号：US4866210A
公开(公告)日：1989-09-12
申请号：US144372
申请日：1988-01-15
申请人： Wolfgang Hoelderich , Leopold Hupfer , Kurt Schneider
发明人： Wolfgang Hoelderich , Leopold Hupfer , Kurt Schneider
IPC分类号： C07C45/65 , C07C45/67
CPC分类号： C07C45/65 , C07C45/673 , C07C45/676 , Y02P20/582
摘要： Ketones of the formula ##STR1## where R.sup.1 to R.sup.3 are each hydrogen and R.sup.1 to R.sup.4 are each alkyl of 1 to 12 carbon atoms, cycloalkyl of 4 to 8 carbon atoms, aryl, aralkyl or alkylaryl, which each in turn may be substituted, or R.sup.1 and R.sup.2 and R.sup.3 together with the carbon atoms to which they are bonded form a cycloalkane, are prepared by reacting ketones of the formula ##STR2## where one of R.sup.1, R.sup.2, R.sup.3 and R.sup.5 is hydroxyl, alkoxy or carboxyl while the remaining R.sup.1 to R.sup.4 have the abovementioned meanings, with hydrogen in the presence of acid catalysts supporting one or more hydrogenation components, zeolites of the pentasil type being particularly suitable.
摘要翻译：其中R 1至R 3各自为氢且R 1至R 4各自为具有1至12个碳原子的烷基，4至8个碳原子的环烷基，芳基，芳烷基或烷基芳基的式“IMAGE”的酮，其各自依次可被取代，或者R 1和R 2和R 3与它们所键合的碳原子一起形成环烷烃，是通过使下式的酮反应制备的：其中R1，R2，R3和R5之一是羟基，烷氧基或羧基，而其余的 R1至R4具有上述含义，在负载一种或多种氢化组分的酸催化剂存在下用氢气，pentasil型沸石是特别合适的。

5. 发明授权

US07101831B2 Compositions of material, especially lubricants and pressure transmitting means, the production and use thereof 有权
标题翻译：材料的组成，特别是润滑剂和压力传递装置，其生产和使用
公开(公告)号：US07101831B2
公开(公告)日：2006-09-05
申请号：US10181710
申请日：2001-01-19
申请人： Wolfgang Hoelderich , Ulrich Keller , Jutta Fischer , Patrick Weckes , Theo Mang , Rolf Luther , Helena Wagner
发明人： Wolfgang Hoelderich , Ulrich Keller , Jutta Fischer , Patrick Weckes , Theo Mang , Rolf Luther , Helena Wagner
IPC分类号： C10M101/00 , C07C59/00
CPC分类号： C07C69/67 , C07C59/305 , C07C59/66 , C10M101/04 , C10M105/34 , C10M105/38 , C10M129/68 , C10M129/70 , C10M129/74 , C10M2207/2815 , C10M2207/2835 , C10M2207/401 , C10N2220/026 , C10N2220/10 , C10N2230/06 , C10N2230/10 , C10N2230/64 , C10N2240/04 , C10N2240/08 , C10N2260/00
摘要： The invention relates to novel compositions of matter which may advantageously be used as lubricants or pressure transfer media or else for functional liquids and lubricant additives. The lubricants according to the invention are the reaction products of an electro-philic addition of linear or branched, aliphatic or aromatic carboxylic acids, carboxylic anhydrides, carbonyl halides or novel neoacids to the double bonds of fatty acids, esters thereof and/or of other fatty acid derivatives and also of synthetic esters. Owing to their increased oxidation resistance compared to the starting materials and also their low toxicity, the novel class of synthetic esters based on oleochemicals may find use in novel environmentally compatible lubricants, pressure transfer systems, functional liquids and lubricant additives.
摘要翻译：本发明涉及可有利地用作润滑剂或压力转移介质或功能性液体和润滑剂添加剂的新型物质组合物。根据本发明的润滑剂是直链或支链的脂族或芳族羧酸，羧酸酐，羰基卤化物或新型新酸的亲电加成到脂肪酸，其酯和/或其它物质的双键的反应产物脂肪酸衍生物以及合成酯。由于它们与起始原料相比具有增加的抗氧化性，而且它们的低毒性，基于油脂化学品的新一类合成酯可用于新型环境相容的润滑剂，压力传递系统，功能性液体和润滑剂添加剂。

6. 发明授权

US5681973A Microporous heteropolyoxometallates and method of their production and use as catalysts 失效
标题翻译：微孔杂多金属氧酸盐及其生产和使用方法作为催化剂
公开(公告)号：US5681973A
公开(公告)日：1997-10-28
申请号：US502261
申请日：1995-07-13
申请人： Wolfgang Hoelderich , Markus Hoelscher , Goetz-Peter Schindler , Ulli Englert , Bodo Zibrowius , Dietrich Arntz
发明人： Wolfgang Hoelderich , Markus Hoelscher , Goetz-Peter Schindler , Ulli Englert , Bodo Zibrowius , Dietrich Arntz
IPC分类号： B01J27/188 , B01J27/19 , B01J27/198 , B01J31/02 , B01J31/16 , B01J31/34 , B01J31/36 , C07F11/00 , C07F19/00 , C07F9/02 , C07F6/00
CPC分类号： B01J31/1691 , B01J23/002 , B01J27/188 , B01J27/198 , B01J31/0237 , C07F11/005 , B01J2231/70 , B01J2231/72 , B01J2523/00 , B01J2531/56 , B01J2531/64 , B01J2531/66
摘要： Heteropolyoxometallates of tungsten, molybdenum and vanadium with a structurally defined micropore volume, a method of production by means of the hydrothermal reaction of the appropriate metal with an associated oxide, a diamine, phosphoric acid and water, and the use of the novel compounds as catalysts.
摘要翻译：具有结构限定的微孔体积的钨，钼和钒的多金属氧酸盐，通过适当金属与相关氧化物，二胺，磷酸和水的水热反应的生产方法，以及新型化合物作为催化剂的用途。

7. 发明授权

US5332830A Preparation of N-hydroxyazoles 失效
标题翻译： N-羟基唑的制备
公开(公告)号：US5332830A
公开(公告)日：1994-07-26
申请号：US37910
申请日：1993-03-26
申请人： Klaus H. von Locquenghien , Wolfgang Hoelderich , Ulf Baus , Wolfgang Reuther , Erwin Hahn
发明人： Klaus H. von Locquenghien , Wolfgang Hoelderich , Ulf Baus , Wolfgang Reuther , Erwin Hahn
IPC分类号： C07D231/12 , C07D233/54 , C07D249/08 , C07D521/00 , C07D233/56
CPC分类号： C07D231/12 , C07D233/56 , C07D249/08
摘要： N-Hydroxyazoles of the general formula I ##STR1## where A is ##STR2## and R.sup.1, R.sup.2 and R.sup.3 are each hydrogen, C.sub.1 -C.sub.4 -alkyl or halogen, are prepared by a process in which an azole of the general formula II ##STR3## where A, R.sup.1, R.sup.2 and R.sup.3 have the abovementioned meanings, is reacted with hydrogen peroxide or an alkyl peroxide in the presence of a zeolite catalyst at from -20.degree. to 150.degree. C. and from 0.1 to 150 bar.
摘要翻译：通式Ⅰ的N-羟基唑（I）其中A是，并且R 1，R 2和R 3各自是氢，C 1 -C 4 - 烷基或卤素，其通过以下方法制备：其中唑其中A，R 1，R 2和R 3具有上述含义的通式II的化合物在沸石催化剂存在下，在-20℃至150℃下与过氧化氢或烷基过氧化物反应。和0.1至150巴。

8. 发明授权

US5225602A Phenylacetaldehydes and the preparation of phenylacetaldehydes 失效
标题翻译：苯乙酮和苯乙酮的制备
公开(公告)号：US5225602A
公开(公告)日：1993-07-06
申请号：US425372
申请日：1989-10-17
申请人： Wolfgang Hoelderich , Norbert Goetz , Leopold Hupfer , Rudolf Kropp , Hans Theobald , Bernd Wolf
发明人： Wolfgang Hoelderich , Norbert Goetz , Leopold Hupfer , Rudolf Kropp , Hans Theobald , Bernd Wolf
IPC分类号： C07C47/228 , C07C45/00 , C07C45/41 , C07C45/51 , C07C45/52 , C07C45/54 , C07C45/58 , C07C47/24 , C07C47/277 , C07C67/00 , C07C313/00 , C07C323/22
CPC分类号： C07C47/277 , C07C323/00 , C07C45/41 , C07C45/512 , C07C45/513 , C07C45/52 , C07C45/54 , C07C45/58 , C07C47/24 , Y02P20/582
摘要： Phenylacetaldehydes of the structure (I) ##STR1## where the substituents X are 2,4-dichloro, difluoro, trifluoro, tetrafluoro, p-trifluoromethyl, 2-methyl-4-fluoro, haloalkoxy or haloalkylthio radicals or are adjacent Cl, F, CF.sub.3, alkyl, alkoxy, haloalkoxy and/or haloalkylthio radicals.
摘要翻译：其中取代基X为2,4-二氯，二氟，三氟，四氟，对三氟甲基，2-甲基-4-氟，卤代烷氧基或卤代烷硫基，或与Cl相邻的苯基乙醛，F，CF 3，烷基，烷氧基，卤代烷氧基和/或卤代烷基硫基。

9. 发明授权

US5126493A Alkoxylation of active hydrogen compounds 失效
标题翻译：活性氢化合物的烷氧基化
公开(公告)号：US5126493A
公开(公告)日：1992-06-30
申请号：US681698
申请日：1991-04-05
申请人： Wolfgang Hoelderich , Jochen Houben , Gerhard Wolf , Michael G. Kinnaird
发明人： Wolfgang Hoelderich , Jochen Houben , Gerhard Wolf , Michael G. Kinnaird
IPC分类号： C07B41/04 , C07C41/03 , C08G65/26
CPC分类号： C08G65/2687 , C07B41/04 , C07C41/03 , C07C41/26
摘要： Alkoxylates of active hydrogen compounds having a peaked molecular weight distribution are prepared by reacting the active hydrogen compound with an alkylene oxide of from 2 to 4 carbon atoms using iron oxides as alkoxylation catalysts.
摘要翻译：具有峰分子量分布的活性氢化合物的烷氧基化物通过使用氧化铁作为烷氧基化催化剂使活性氢化合物与2至4个碳原子的氧化烯反应来制备。

10. 发明授权

US5110834A Production of chlorofluorocarbon-free urethane-containing soft-elastic moldings having a cellular core and a compacted peripheral zone 失效
标题翻译：生产含有细胞核和压缩的外围区域的无氟尿素软硫弹性模具
公开(公告)号：US5110834A
公开(公告)日：1992-05-05
申请号：US770382
申请日：1991-10-03
申请人： Peter Horn , Wolfgang Hoelderich , Rudolf Taddey , Dieter Tintelnot
发明人： Peter Horn , Wolfgang Hoelderich , Rudolf Taddey , Dieter Tintelnot
IPC分类号： B29C45/00 , B29C44/00 , B29K75/00 , B29L31/56 , C08G18/00 , C08G18/08 , C08G101/00 , C08J9/00 , C08J9/02 , C08J9/34 , C08K7/26 , C08L75/00
CPC分类号： C08J9/34 , C08G18/0885 , C08J9/0066 , C08J2375/04 , Y10S264/15
摘要： Chlorofluorocarbon-free urethane-containing, soft-elastic moldings having a cellular core, a compacted peripheral zone and an essentially pore-free smooth surface are produced by reactinga) an organic and/or modified organic polyisocyanate withb) at least one relatively high-molecular-weight compound containing at least two reactive hydrogen atoms and, if desired,c) a low-molecular-weight chain extender and/or crosslinking agent,in the presence ofd) a blowing agent,e) a catalyst,f) a crystalline, microporous molecular sieve having a cavity diameter of less than 1.3 nm and comprising metal oxides or metal phosphates, and, if desired, further additives andg) assistants,in a closed mold with compaction, expediently by RIM.
摘要翻译：通过使a）有机和/或改性的有机多异氰酸酯与b）至少一种相对较高的反应产生具有多孔芯，压实的周边区和基本上无孔的光滑表面的不含氟氯化碳的含氨基甲酸酯的软弹性模制品 - 含有至少两个反应性氢原子的分子量化合物，如果需要，c）低分子量增链剂和/或交联剂，在d）发泡剂，e）催化剂的存在下，f）具有小于1.3nm的空腔直径小于1.3nm的结晶微孔分子筛，并且包含金属氧化物或金属磷酸盐，并且如果需要，还可以使用另外的添加剂和g）助剂，通过RIM有利地在密闭的模具中进行压实。

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