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1. 发明授权

US5235099A Process for the preparation of ureidoperoxycarboxylic acids 失效
标题翻译：制备尿嘧啶羧酸的方法
公开(公告)号：US5235099A
公开(公告)日：1993-08-10
申请号：US793815
申请日：1991-11-18
申请人： Wolf-Dieter Muller , Frank Jaekel , Peter Naumann , Gerd Reinhardt
发明人： Wolf-Dieter Muller , Frank Jaekel , Peter Naumann , Gerd Reinhardt
IPC分类号： B01J27/02 , A01N47/28 , A01N47/30 , A01N47/32 , B01J31/02 , B01J31/08 , C07B61/00 , C07C407/00 , C07C409/40 , C11D3/39
CPC分类号： A01N47/28 , A01N47/30 , A01N47/32 , C07C407/00 , C11D3/3945 , C07C2101/14
摘要： A process for the preparation of ureidoperoxycarboxylic acids of the formula ##STR1## in which x is the number 1 or 2,A,if x is 1,is hydrogen, C.sub.1 -C.sub.20 -alkyl, aryl, preferably phenyl, or haloaryl, preferably chlorophenyl, orif x is 2,is C.sub.1 -C.sub.20 -alkylene or arylene, preferably phenylene,B is a group of the formula ##STR2## in which n is a number from 1 to 20,m is the number 0, 1 or 2,R.sup.1 is C.sub.1 -C.sub.20 -alkyl andR.sup.2 is in each case hydrogen or C.sub.1 -C.sub.20 -alkyl, which comprises dissolving carbamoyllactams of the formula ##STR3## in which x, A and B have the abovementioned meanings, in a one- to six-fold, preferably a one- to three-fold, amount by weight of a strong catalyst acid, by then adding water in a one- to ten-fold molar excess, relative to the carbamoyllactam, to the solution of the carbamoyllactam in the catalyst acid and by heating the reaction mixture to form the ureidocarboxylic acid, by then adding to the reaction mixture an aqueous hydrogen peroxide solution in a one- to ten-fold, preferably a two- to four fold, molar excess per oxidizable carboxyl group of the ureidocarboxylic acid formed in the preceding reaction step, and by then precipitating the resulting ureidoperoxycarboxylic acid from the reaction mixture.These compounds are suitable as bleaches, oxidants and disinfectants.
摘要翻译：制备式A [NHCONHBCOOOH] x的脲基过氧羧酸的方法，其中x为数1或2，如果x为1，则为A，为C 1 -C 20烷基，芳基，优选苯基或卤代芳基，优选氯苯基，或如果x为2，则为C 1 -C 20亚烷基或亚芳基，优选亚苯基，B为下式的基团：其中n为1至20的数，m为数 0,1或2，R 1是C 1 -C 20烷基，R 2在各自的情况下是氢或C 1 -C 20 - 烷基，其包括将式（ⅩⅧ）的氨基甲酰基内酰胺溶解在其中x，A和B具有上述含义，以强的催化剂酸的重量比为1至6倍，优选1至3倍，然后将相对于氨基甲酰基内酰胺的1至10倍摩尔过量的水加入到催化剂中的氨基甲酰基内酰胺，并加热反应混合物形成脲基羧酸，然后向反应混合物中加入过氧化氢水溶液在上述反应步骤中形成的脲基羧酸的每个可氧化羧基的摩尔过量为十倍，优选为二至四倍，然后从反应混合物中沉淀所得的脲基过氧羧酸。这些化合物适合作为漂白剂，氧化剂和消毒剂。

2. 发明授权

US5518650A Imidocarboxylic acid activators and sulfimidocarboxylic acid activators, processes for their preparation and their use 失效
标题翻译：二羧酸活化剂和亚磺酰基羧酸活化剂，其制备方法及其用途
公开(公告)号：US5518650A
公开(公告)日：1996-05-21
申请号：US455671
申请日：1995-05-31
申请人： Frank Jaekel , Gerd Reinhardt , Wolf-Dieter Muller
发明人： Frank Jaekel , Gerd Reinhardt , Wolf-Dieter Muller
IPC分类号： C07D207/452 , C07D207/40 , C07D209/48 , C07D211/88 , C07D223/10 , C07D275/02 , C07D275/06 , C07D279/02 , C07D281/02 , C07D401/06 , C07D401/10 , C07D403/06 , C07D403/10 , C07D417/06 , C07D417/10 , C11D3/39 , C11D3/395 , C11D3/48 , C11D7/54 , D06L3/02 , C09K3/00 , C01B15/00
CPC分类号： C07D207/40 , C07D209/48 , C11D3/392
摘要： This invention is directed to a process for bleaching textile objects and bleaching agent containing a persalt activators and salts thereof which are derived from imidocarboxylic acids and sulfimidocarboxylic acids of the formula I: ##STR1## in which A is a group of the formula ##STR2## n is the number 0, 1 or 2, R.sup.1 is hydrogen, chlorine, bromine, C.sub.1 -C.sub.20 -alkyl, C.sub.2 -C.sub.20 -alkenyl, aryl, or alkylaryl,R.sup.2 is hydrogen, chlorine, bromine, --SO.sub.3 M, --CO.sub.2 M or --OSO.sub.3 M,X is C.sub.1 -C.sub.9 -alkylene or arylene,B is a group of the formula C.dbd.O or SO.sub.2,L is a leaving group.
摘要翻译：本发明涉及一种漂白纺织品和漂白剂的方法，所述漂白剂含有衍生自式I的亚氨基羧酸和亚磺酰亚氨基羧酸的式（I）的持久性活化剂及其盐：其中A是式 n是数字0,1或2，R1是氢，氯，溴，C1-C20-烷基，C2-C20-烯基，芳基或烷基芳基，R2是氢，氯，溴，-SO 3 M，-CO 2 M或-OSO 3 M，X为C 1 -C 9 - 亚烷基或亚芳基，B为式C = O或SO 2的基团，L为离去基团。

3. 发明授权

US5610318A Imidocarboxylic acid activators and sulfimidocarboxylic acid activators processes for their preparation and their use 失效
标题翻译：二酰亚胺羧酸活化剂和亚磺酰基羧酸活化剂的制备及其用途
公开(公告)号：US5610318A
公开(公告)日：1997-03-11
申请号：US455351
申请日：1995-05-31
申请人： Frank Jaekel , Gerd Reinhardt , Wolf-Dieter M uller
发明人： Frank Jaekel , Gerd Reinhardt , Wolf-Dieter M uller
IPC分类号： C07D207/452 , C07D207/40 , C07D209/48 , C07D211/88 , C07D223/10 , C07D275/02 , C07D275/06 , C07D279/02 , C07D281/02 , C07D401/06 , C07D401/10 , C07D403/06 , C07D403/10 , C07D417/06 , C07D417/10 , C11D3/39 , C11D3/395 , C11D3/48 , C11D7/54 , D06L3/02 , C07D207/02
CPC分类号： C07D207/40 , C07D209/48 , C11D3/392
摘要： This invention is directed to a process for preparing a compound containing a persalt activators and salts thereof which are derived from imidocarboxylic acids and sulfimidocarboxylic acids of the formula I: ##STR1## in which A is a group of the formula ##STR2## n is the number 0, 1 or 2, R.sup.1 is hydrogen, chlorine, bromine, C.sub.1 -C.sub.20 -alkyl, C.sub.2 -C.sub.20 -alkenyl, aryl, or alkylaryl,R.sup.2 is hydrogen, chlorine, bromine, --SO.sub.3 M, --CO.sub.2 M or --OSO.sub.3 M, X is C.sub.1 -C.sub.19 -alkylene or arylene,B is a group of the formula C.dbd.O or SO.sub.2,L is a leaving group.
摘要翻译：本发明涉及一种制备含有衍生自式I的亚氨基羧酸和亚磺酰亚胺羧酸的含有活性剂及其盐的化合物的方法：其中A是下式的基团： n是数字0,1或2，R1是氢，氯，溴，C1-C20-烷基，C2-C20-烯基，芳基或烷基芳基，R2是氢，氯，溴， SO 3 M，-CO 2 M或-OSO 3 M，X为C 1 -C 19 - 亚烷基或亚芳基，B为式C = O或SO 2的基团，L为离去基团。

4. 发明授权

US6066365A Process for the preparation of low-dust granules 失效
标题翻译：制备低尘颗粒的方法
公开(公告)号：US6066365A
公开(公告)日：2000-05-23
申请号：US63985
申请日：1993-05-19
申请人： Frank Jaekel , Gerd Reinhardt , Gerhard Noltner
发明人： Frank Jaekel , Gerd Reinhardt , Gerhard Noltner
IPC分类号： B01J2/16 , B01J2/30 , C11D3/39 , C11D7/54 , C11D11/00 , C11D17/00 , C11D17/06 , D06L3/02 , B05D7/00
CPC分类号： C11D3/3907 , C11D11/0082 , C11D11/0088 , C11D17/0039 , C11D17/06 , C11D3/3935 , C11D3/3945
摘要： The present invention relates to a process for the preparation of low-dust granules, which comprises applying an aqueous solution or suspension of a hydrate-forming compound to a particulate starting material, the particulate starting material being at a temperature below the transition temperature of the hydrate-forming compound during the application of the aqueous solution or suspension and the aqueous solution being at a temperature above the transition temperature, effecting granulation subsequently or simultaneously and, if desired, drying the granules obtained.
摘要翻译：本发明涉及一种制备低灰尘颗粒的方法，其包括将水合物形成化合物的水溶液或悬浮液施加到颗粒起始材料上，所述颗粒起始材料的温度低于在施用水溶液或悬浮液期间水合物形成化合物和水溶液处于高于转变温度的温度下，随后或同时进行造粒，如果需要，干燥所获得的颗粒。

5. 发明授权

US5419846A Stable granules for detergents, cleaning agents and disinfectants 失效
标题翻译：用于洗涤剂，清洁剂和消毒剂的稳定颗粒
公开(公告)号：US5419846A
公开(公告)日：1995-05-30
申请号：US108478
申请日：1993-08-18
申请人： Frank Jaekel , Gerd Reinhardt , Gerhard Noltner , Eric Jacquinot , Rudiger Funk , Manfred Muller
发明人： Frank Jaekel , Gerd Reinhardt , Gerhard Noltner , Eric Jacquinot , Rudiger Funk , Manfred Muller
IPC分类号： A01N25/12 , A01N25/26 , B01J2/28 , C11D3/12 , C11D3/37 , C11D3/39 , C11D3/48 , C11D17/00 , C11D17/06 , D06L1/00 , D06L3/00
CPC分类号： C11D3/378 , B01J2/28 , C11D17/0039 , C11D3/124 , C11D3/3761 , C11D3/3945 , C11D3/48
摘要： The present invention relates to stable granules comprising active substance, granulating auxiliary, enveloping substance and if appropriate additional components, wherein the enveloping substance in each case comprisesa) silicon dioxide particles orb) homopolymers of unsaturated sulfonic acids orc) copolymers of unsaturated sulfonic acids and unsaturated carboxylic acids ord) homopolymers of (meth)acrylic acid esters ore) copolymers of (meth)acrylic acid esters and unsaturated carboxylic acids orf) mixtures of one or more of these constituents.
摘要翻译：本发明涉及包含活性物质，造粒助剂，包封物质以及合适的其它成分的稳定颗粒，其中每种情况下的包封物质包括a）二氧化硅颗粒或b）不饱和磺酸的均聚物或c）不饱和磺酸的共聚物酸和不饱和羧酸或d）（甲基）丙烯酸酯的均聚物或e）（甲基）丙烯酸酯和不饱和羧酸的共聚物或f）这些组分中的一种或多种的混合物。

6. 发明授权

US5153189A Sulfimidoperoxycarboxylic acids 失效
标题翻译：磺酰氧基羧基酸
公开(公告)号：US5153189A
公开(公告)日：1992-10-06
申请号：US793803
申请日：1991-11-18
申请人： Walter Rupp , Hanspeter Gethoffer , Gerd Reinhardt , Frank Jaekel
发明人： Walter Rupp , Hanspeter Gethoffer , Gerd Reinhardt , Frank Jaekel
IPC分类号： A01N43/80 , C07D275/02 , C07D275/03 , C07D275/06 , C07D279/02 , C07D281/02 , C11D3/39 , C11D7/54
CPC分类号： C07D275/02 , C07D275/03 , C07D275/06 , C11D3/3945
摘要： Sulfimidoperoxycarboxylic acids of the formula ##STR1## in which A is a group of the formula ##STR2## n is the number 0, 1 or 2, R.sup.1 is hydrogen, fluorine, chlorine, bromine, C.sub.1 -C.sub.20 - alkyl, C.sub.2 -C.sub.20 -alkenyl, aryl or C.sub.1 -C.sub.10 -alkylaryl,R.sup.2 is hydrogen, fluorine, chlorine, bromine or a group of the formula SO.sub.3 M, CO.sub.2 M or OSO.sub.3 M,M is hydrogen, an alkali metal or ammonium ion or the stoichiometric amount of an alkaline earth metal ion andX is C.sub.1 -C.sub.19 -alkylene or ortho-, meta- or para-arylene.These sulfimidoperoxycarboxylic acids are suitable as bleaches, oxidants or disinfectants.
摘要翻译：式中，A为式（1）的基团的亚磺酰基过氧羧酸为数字0,1或2，R 1为氢，氟，氯，溴，C 1 -C 20烷基，C 2 C 20 - 烯基，芳基或C 1 -C 10烷基芳基，R 2是氢，氟，氯，溴或式SO 3 M，CO 2 M或OSO 3 M的基团，M是氢，碱金属或铵离子或化学计量的碱土金属离子和X是C 1 -C 19 - 亚烷基或邻 - 间 - 或对 - 亚芳基。这些亚磺酰过氧羧酸适合作为漂白剂，氧化剂或消毒剂。

7. 发明授权

US5438147A Imidocarboxylic acid activators and sulfimidocarboxylic acid activators, processes for their preparation and their use 失效
标题翻译：二羧酸活化剂和亚磺酰基羧酸活化剂，其制备方法及其用途
公开(公告)号：US5438147A
公开(公告)日：1995-08-01
申请号：US876517
申请日：1992-04-30
申请人： Frank Jaekel , Gerd Reinhardt , Wolf-Dieter Meller
发明人： Frank Jaekel , Gerd Reinhardt , Wolf-Dieter Meller
IPC分类号： C07D207/452 , C07D207/40 , C07D209/48 , C07D211/88 , C07D223/10 , C07D275/02 , C07D275/06 , C07D279/02 , C07D281/02 , C07D401/06 , C07D401/10 , C07D403/06 , C07D403/10 , C07D417/06 , C07D417/10 , C11D3/39 , C11D3/395 , C11D3/48 , C11D7/54 , D06L3/02
CPC分类号： C07D207/40 , C07D209/48 , C11D3/392
摘要： A persalt activator or salt thereof which is derived from an imidocarboyxlic acid or sulimidocarboxylic acid of the formula I: ##STR1## in which A is a group of the formula ##STR2## n is the number 0, 1 or 2, R.sup.1 is hydrogen, chlorine, bromine, C.sub.1 -C.sub.20 -alkyl, C.sub.2 -C.sub.20 -alkenyl, aryl, or alkylaryl,R.sup.2 is hydrogen, chlorine, bromine or a group of the formula --SO.sub.3 M, --CO.sub.2 M or --OSO.sub.3 M,X is C.sub.1 -C.sub.19 -alkylene or arylene,B is a group of the formula C.dbd.O or SO.sub.2, andL is a leaving group.
摘要翻译：衍生自式I的亚氨基羧酸或磺酰胺羧酸的透明质激活剂或其盐：其中A是下式的基团：氯，溴，C 1 -C 20烷基，C 2 -C 20 - 烯基，芳基或烷基芳基，R 2是氢，氯，溴或式-SO 3 M，-CO 2 M或-OSO 3 M的基团，X是C 1 -C 19亚烷基或亚芳基，B是式C = O或SO 2，L为离去基团。

8. 发明申请

US20110021812A1 Process For Preparing Solid Alkaline Earth Metal Salts Of Secondary Paraffinsulphonic Acids 失效
标题翻译：制备碱性次磺酰基酸的固体碱土金属盐的方法
公开(公告)号：US20110021812A1
公开(公告)日：2011-01-27
申请号：US12921468
申请日：2009-03-04
申请人： Gerd Reinhardt , Peter Naumann , Georg Borchers , Mathias Groeschen
发明人： Gerd Reinhardt , Peter Naumann , Georg Borchers , Mathias Groeschen
IPC分类号： C07C309/04
CPC分类号： C11D1/143 , C11D11/02
摘要： A process for preparing solid alkaline earth metal salts of secondary paraffinsulphonic acids is claimed. This process comprises converting an aqueous solution of a secondary paraffinsulphonic acid and an alkaline earth metal hydroxide into solid form by spray drying.
摘要翻译：要求保护二级链烷烃磺酸的固体碱土金属盐的方法。该方法包括通过喷雾干燥将次级链烷烃磺酸和碱土金属氢氧化物的水溶液转化为固体形式。

9. 发明授权

US06822113B2 Process for preparing acyloxybenzenesulfonates 失效
公开(公告)号：US06822113B2
公开(公告)日：2004-11-23
申请号：US10431951
申请日：2003-05-08
申请人： Gerd Reinhardt , Peter Naumann , Alexander Lerch , Wolf-Dieter Mueller , Narayan D. Sadanani
发明人： Gerd Reinhardt , Peter Naumann , Alexander Lerch , Wolf-Dieter Mueller , Narayan D. Sadanani
IPC分类号： C07C6900
CPC分类号： C07C303/32 , C07C303/22 , C07C309/42
摘要： A process for preparing acyloxybenzenesulfonates by reacting anhydrous phenolsulfonates with carboxylic acid derivatives comprises conducting the reaction with a salt of a phenolsulfonic acid which has a water content of less than 0.5% by weight and has been contacted with a substance having basic properties.

10. 发明授权

US5149864A Ureidoperoxycarboxylic acids and preparation and use thereof 失效
标题翻译：尿嘧啶羧酸和其制备和用途
公开(公告)号：US5149864A
公开(公告)日：1992-09-22
申请号：US703461
申请日：1991-05-21
申请人： Hanspeter Gethoffer , Gerd Reinhardt , Peter Naumann
发明人： Hanspeter Gethoffer , Gerd Reinhardt , Peter Naumann
IPC分类号： A01N47/28 , C07C407/00 , C07C409/40 , C11D3/39 , C11D7/54
CPC分类号： C07C409/40 , C11D3/3945
摘要： Compounds of the formula ##STR1## where y is 1 or 2,A is hydrogen, C.sub.1 -C.sub.2 -alkyl, aryl or a group of the formula ##STR2## if y is 1, or C.sub.2 -C.sub.20 -alkylene or arylene if y is 2, R.sup.1 and R.sup.2 can be identical or different and each is hydrogen, C.sub.1 -C.sub.20 -alkyl, aryl, haloaryl, alkoxyaryl or alkylaryl, or else R.sup.1 and R.sup.2 together are a C.sub.2 -C.sub.4 -alkylene radical,x is 0 or 1,B is a group of the formula ##STR3## n is from 1 to 20, m is 0, 1 or 2,R.sup.3 is C.sub.1 -C.sub.20 -alkyl andR.sup.4 is in each case hydrogen or C.sub.1 -C.sub.20 -alkyl.These compounds are suitable for use as bleaching, oxidizing or disinfecting agents.
摘要翻译：其中y为1或2的化合物，如果y为1，则A为氢，C1-C2-烷基，芳基或式为IMA的基团，如果y为1，则为C2-C20-亚烷基或亚芳基 2，R 1和R 2可以相同或不同，各自为氢，C 1 -C 20 - 烷基，芳基，卤代芳基，烷氧基芳基或烷基芳基，或者R 1和R 2一起为C 2 -C 4亚烷基，x为0或1， B是下式的基团：n为1至20，m为0,1或2，R 3为C 1 -C 20烷基，R 4为氢或C 1 -C 20 - 烷基。这些化合物适用于漂白，氧化或消毒剂。

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