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1. 发明授权

US4168963A Herbicidal agents 失效
标题翻译：除草剂
公开(公告)号：US4168963A
公开(公告)日：1979-09-25
申请号：US797171
申请日：1977-05-16
申请人： Walter Rupp , Manfred Finke , Hermann Bieringer , Peter Langeluddeke , Hans-Jerg Kleiner
发明人： Walter Rupp , Manfred Finke , Hermann Bieringer , Peter Langeluddeke , Hans-Jerg Kleiner
IPC分类号： A01N57/18 , A01N57/20 , A01P13/00 , C07F9/30 , C07F9/547 , C07F9/553 , C07F9/6512 , A01N9/36
CPC分类号： C07F9/301
摘要： Herbicidal agents, containing as active ingredient a compound of the formula ##STR1## or their salts with acids, are useful for combatting a great variety of mono- and dicotyledonous weeds. In the formula R.sub.1 is methyl or halomethyl, R.sub.2 is OH, SH, OM or SM (M=equivalent of a base), R.sub.3 is the same as R.sub.2 or an ester, amide or hydrazide group, R.sub.4 and R.sub.5 are preferably hydrogen and X is oxygen or sulfur.
摘要翻译：作为活性成分含有下式化合物的除草剂或其与酸的盐可用于对抗各种单子叶和双子叶杂草。式中R 1为甲基或卤代甲基，R 2为OH，SH，OM或SM（M =碱的当量），R 3与R 2或酯，酰胺或酰肼基相同，R 4和R 5优选为氢，X 是氧或硫。

2. 发明授权

US4314052A Polyester which is soluble or dispersible in water, a process for its preparation and its use as a levelling auxiliary, levelling auxiliaries and processes for uniform dyeing 失效
标题翻译：可溶于水或分散于水中的聚酯，其制备方法及其用作流平助剂，流平助剂和均匀染色方法
公开(公告)号：US4314052A
公开(公告)日：1982-02-02
申请号：US110343
申请日：1980-01-07
申请人： Friedrich Engelhardt , Karl Hintermeier , Joachim Ribka , Walter Dursch , Walter Rupp
发明人： Friedrich Engelhardt , Karl Hintermeier , Joachim Ribka , Walter Dursch , Walter Rupp
IPC分类号： C08G63/00 , C08G63/692 , C08G63/78 , C08G63/91 , D06P1/52 , C08G63/68 , C08G79/04 , D06P1/60
CPC分类号： C08G63/692 , D06P1/5271
摘要： Improved polyesters soluble or dispersible in water having an apparent average molecular weight of 800 to 5,000 and containing phosphonic ester moieties are useful as levelling auxiliaries for uniform dyeing and are produced by esterifying dibasic acids and dihydric alcohols, either or both of which contain phosphonic acid moieties, phosphonic acid ester moieties or both.
摘要翻译：可溶于或可分散于表观平均分子量为800至5,000的含有膦酸酯部分的水中的改性聚酯可用作均匀染色的流平助剂，并通过酯化二元酸和二元醇制备，其中一种或两者含有膦酸部分，膦酸酯部分或两者。

3. 发明授权

US4001352A Process for the preparation of ethane-1,2-diphosphinic acid diesters 失效
标题翻译：乙二胺二磷酸乳液的制备方法
公开(公告)号：US4001352A
公开(公告)日：1977-01-04
申请号：US571769
申请日：1975-04-25
申请人： Hans-Jerg Kleiner , Walter Rupp
发明人： Hans-Jerg Kleiner , Walter Rupp
IPC分类号： C07F9/32 , C07F9/40
CPC分类号： C07F9/3235
摘要： A process for the preparation of ethane-1,2,-diphosphinic acid diesters of the formula ##STR1## where R.sub.1 represents alkyl, phenyl and/or phenalkyl groups having from 1 to 18 carbon atoms and R.sub.2 alkyl groups having from 1 to 18 carbon atoms, which may be optionally substituted by halogen atoms, which comprises reacting phosphonous acid esters of the formula ##STR2## where R.sub.1 and R.sub.2 are as define above, with acetylene in the presence of catalytic amounts of radical-forming agents and/or with UV irradiation.

4. 发明授权

US5153189A Sulfimidoperoxycarboxylic acids 失效
标题翻译：磺酰氧基羧基酸
公开(公告)号：US5153189A
公开(公告)日：1992-10-06
申请号：US793803
申请日：1991-11-18
申请人： Walter Rupp , Hanspeter Gethoffer , Gerd Reinhardt , Frank Jaekel
发明人： Walter Rupp , Hanspeter Gethoffer , Gerd Reinhardt , Frank Jaekel
IPC分类号： A01N43/80 , C07D275/02 , C07D275/03 , C07D275/06 , C07D279/02 , C07D281/02 , C11D3/39 , C11D7/54
CPC分类号： C07D275/02 , C07D275/03 , C07D275/06 , C11D3/3945
摘要： Sulfimidoperoxycarboxylic acids of the formula ##STR1## in which A is a group of the formula ##STR2## n is the number 0, 1 or 2, R.sup.1 is hydrogen, fluorine, chlorine, bromine, C.sub.1 -C.sub.20 - alkyl, C.sub.2 -C.sub.20 -alkenyl, aryl or C.sub.1 -C.sub.10 -alkylaryl,R.sup.2 is hydrogen, fluorine, chlorine, bromine or a group of the formula SO.sub.3 M, CO.sub.2 M or OSO.sub.3 M,M is hydrogen, an alkali metal or ammonium ion or the stoichiometric amount of an alkaline earth metal ion andX is C.sub.1 -C.sub.19 -alkylene or ortho-, meta- or para-arylene.These sulfimidoperoxycarboxylic acids are suitable as bleaches, oxidants or disinfectants.
摘要翻译：式中，A为式（1）的基团的亚磺酰基过氧羧酸为数字0,1或2，R 1为氢，氟，氯，溴，C 1 -C 20烷基，C 2 C 20 - 烯基，芳基或C 1 -C 10烷基芳基，R 2是氢，氟，氯，溴或式SO 3 M，CO 2 M或OSO 3 M的基团，M是氢，碱金属或铵离子或化学计量的碱土金属离子和X是C 1 -C 19 - 亚烷基或邻 - 间 - 或对 - 亚芳基。这些亚磺酰过氧羧酸适合作为漂白剂，氧化剂或消毒剂。

5. 发明授权

US4842776A Styrylaryloxy ether sulfonates, a process for their preparation and their use in the recovery of crude oil 失效
标题翻译：苯乙烯基氧基醚磺酸盐，其制备方法及其在回收原油中的应用
公开(公告)号：US4842776A
公开(公告)日：1989-06-27
申请号：US112560
申请日：1987-10-22
申请人： Manfred Schmidt , Walter Rupp , Gerhart Schneider , Eva M. Kohn
发明人： Manfred Schmidt , Walter Rupp , Gerhart Schneider , Eva M. Kohn
IPC分类号： C07C309/04 , C07C309/09 , C09K8/584 , E21B43/22
CPC分类号： C07C309/00 , C09K8/584
摘要： Styrylaryloxy ether sulfonates of the formula ##STR1## in which either R.sub.1 denotes styryl and simultaneously R.sub.2 and R.sub.3 are identical or different and denote hydrogen or styryl, or R.sub.1 and R.sub.2 are nonidentical and each denote methyl or styryl and simultaneously R.sub.3 denotes hydrogen or styryl, x denotes a number from 2 to 20, and M denotes an ammonium or alkali metal cation. These compounds are suitable as surfactant auxiliaries in oil recovery.
摘要翻译：式“IMAGE”的苯乙烯基氧基醚磺酸盐，其中R1表示苯乙烯基，同时R2和R3相同或不同，表示氢或苯乙烯基，或R1和R2不相同，各自表示甲基或苯乙烯基，同时R3表示氢或苯乙烯基， x表示2〜20的数，M表示铵或碱金属阳离子。这些化合物适合作为油回收中的表面活性剂助剂。

6. 发明授权

US5463100A Process for the preparation of aminoaryl .beta.-sulfatoethyl sulfone compounds 失效
标题翻译：制备氨基芳基β-磺基乙基砜化合物的方法
公开(公告)号：US5463100A
公开(公告)日：1995-10-31
申请号：US301311
申请日：1994-09-06
申请人： Walter Rupp
发明人： Walter Rupp
IPC分类号： C07C315/04 , C07C317/18 , C07C305/18
CPC分类号： C07C315/04
摘要： Aminoaryl .beta.-sulfatoethyl sulfone compounds, such as, for example 4-(.beta.-sulfatoethylsulfonyl)-aniline, can be prepared in a quick and easy manner from their corresponding .beta.-hydroxyethyl sulfone compounds by sulfation by spraying a solution or suspension or paste of this aminoaryl .beta.-hydroxyethyl sulfone compound or the acylamino compound thereof in sulfuric acid or aqueous sulfuric acid into a hot inert gas stream of a convection dryer. In this procedure, the drying, esterification reaction and the hydrolysis of any acylamino group present takes place synchronously. The sulfato compound is preferably obtained in the form of granules.
摘要翻译：氨基芳基β-磺酰基乙基砜化合物，例如4-（β-磺基乙酰基磺酰基） - 苯胺，可以通过硫酸化以快速和容易的方式从相应的β-羟基乙基砜化合物制备，通过喷洒溶液或悬浮液或糊剂该氨基芳基β-羟乙基砜化合物或其在硫酸或硫酸水溶液中的酰氨基化合物转化成对流干燥器的热惰性气流。在该方法中，存在的任何酰氨基的干燥，酯化反应和水解同步进行。硫酸酯化合物优选以颗粒形式获得。

7. 发明授权

US4526728A 2-Acrylamido- and 2-methacrylamido-2-methyl propanephosphonic acids and their salts, process for the preparation thereof, and use thereof for the manufacture of copolymers 失效
标题翻译： 2-丙烯酰氨基 - 和2-甲基丙烯酰胺基-2-甲基丙膦酸及其盐，其制备方法及其在制备共聚物中的用途
公开(公告)号：US4526728A
公开(公告)日：1985-07-02
申请号：US596895
申请日：1984-04-05
申请人： Manfred Finke , Walter Rupp , Erwin Weiss
发明人： Manfred Finke , Walter Rupp , Erwin Weiss
IPC分类号： C07F9/38 , C08F30/02 , C08G63/00 , C08G63/44
CPC分类号： C08F30/02 , C07F9/3808
摘要： 2-(Meth)acrylamido-2-methylpropanephosphonic acid is prepared by reaction of 2-methylprop-1-ene-1-phosphonic acid or 2-methylpro-2-ene-1-phosphonic acid with (meth)acrylonitrile in the presence of an equimolar amount of a strong acid. The compounds are suitable as such or in the form of their salts as comonomer for the manufacture of copolymers, which are used inter alia as dyeing auxiliaries and as scale inhibitors.
摘要翻译： 2-（甲基）丙烯酰氨基-2-甲基丙烷膦酸通过2-甲基丙-1-烯-1-膦酸或2-甲基丙-2-烯-1-膦酸与（甲基）丙烯腈在存在下反应制备等摩尔量的强酸。化合物本身或其盐的形式是共聚单体的形式，用于制备共聚物，其尤其用作染色助剂和作为阻垢剂。

8. 发明授权

US4778629A Process for the preparation of acyloxybenzenesulfonic acids and salts thereof 失效
标题翻译：酰氧基苯磺酸及其盐的制备方法
公开(公告)号：US4778629A
公开(公告)日：1988-10-18
申请号：US922277
申请日：1986-10-23
申请人： Fritz-Feo Grabley , Gerd Reinhardt , Georg Bader , Walter Rupp
发明人： Fritz-Feo Grabley , Gerd Reinhardt , Georg Bader , Walter Rupp
IPC分类号： C07C309/42 , C07C20060101 , C07C67/00 , C07C301/00 , C07C303/06 , C07C303/32 , C07C309/28 , C11C3/00
CPC分类号： C07C309/00
摘要： A process for the preparation of acyloxybenzenesulfonic acids and salts thereof, of the formula ##STR1## in which R is C.sub.1 -C.sub.17 -alkyl or C.sub.2 -C.sub.17 -alkenyl and M is an alkali or alkaline earth metal, ammonium or hydrogen, including the stages of (a) sulfonation of phenol, if appropriate (b) thermal treatment of the sulfonated phenol, (c) esterification of the sulfonated phenol and if appropriate (d) neutralization of the ester, wherein the sulfonation of the phenol is carried out with sulfuric acid or oleum and the water of reaction is removed during or after stage (b) by distillation and/or by reaction with a dehydrating agent.
摘要翻译：制备其中R为C 1 -C 17 - 烷基或C 2 -C 17 - 链烯基且M为碱金属或碱土金属，铵或氢的式“IMAGE”的酰氧基苯磺酸及其盐的方法，包括步骤（a）苯酚磺化，如果合适（b）磺化苯酚的热处理，（c）磺化苯酚的酯化，如果合适（d）中和该酯，其中苯酚的磺化用硫酸进行酸或发烟硫酸，并且通过蒸馏和/或通过与脱水剂反应在阶段（b）期间或之后除去反应水。

9. 发明授权

US4336206A Process for the manufacture of cyanohydrin acylates of aldehydes 失效
标题翻译：制备醛类羟腈酰化物的方法
公开(公告)号：US4336206A
公开(公告)日：1982-06-22
申请号：US149969
申请日：1980-05-15
申请人： Rainer Mundnich , Manfred Finke , Walter Rupp , Klaus Dehmer
发明人： Rainer Mundnich , Manfred Finke , Walter Rupp , Klaus Dehmer
IPC分类号： C07C255/16 , C07C67/00 , C07C253/00 , C07C255/14 , C07C255/31 , C07C255/38 , C07C120/00 , C07C121/38 , C07C121/46 , C07C121/66
CPC分类号： C07C255/00
摘要： Cyanohydrin acylates of aldehydes are manufactured by reacting aldehydes with aqueous solutions of cyanides and organic acid chlorides or anhydrides in the molar ratio of aldehyde:cyanide:acid chloride or anhydride of 1:1:1 with deviations of at most only about 10%, optionally in the presence of an inert organic solvent immiscible with water in a one-stage process. The process products are intermediates mainly in the fields of pharmaceuticals and plant protection.
摘要翻译：醛的氰基醇酰化物通过使醛与氰化物和有机酰氯或酸酐的水溶液以醛：氰化物：酰氯或酸酐的1:1:1的摩尔比反应制备，偏差最多仅为约10％，任选地在一步法中与水不混溶的惰性有机溶剂的存在下进行。过程产品主要是药物和植物保护领域的中间体。

10. 发明授权

US4096182A Process for the simultaneous preparation of 2,5-dioxo-1,2-oxa-phospholanes and .beta.-halogenpropionic acid halide 失效
标题翻译：同时制备2,5-二氧代-1,2-氧杂磷杂环己烷和{62-卤代丙酸卤化物的方法
公开(公告)号：US4096182A
公开(公告)日：1978-06-20
申请号：US778052
申请日：1977-03-16
申请人： Walter Rupp , Manfred Finke
发明人： Walter Rupp , Manfred Finke
IPC分类号： C07C53/50 , C07C51/00 , C07C67/00 , C07F9/30 , C07F9/32 , C07F9/6571 , C07F9/6574 , C07C51/58 , C07F9/02
CPC分类号： C07F9/657172 , C07F9/3211
摘要： 2,5-Dioxo-1,2-oxa-phospholanes of the formula (I) ##STR1## wherein R.sup.1 is an organic radical and R.sup.2 and R.sup.3 each also represents an organic radical or hydrogen, are prepared by reacting 2-haloformylethyl-phosphinic acid halides of the formula (II) ##STR2## wherein R.sup.1, R.sup.2 and R.sup.3 are defined as in formula (I) and X means Cl or Br, preferably Cl, with an approximatey equimolar quantity of acrylic acid. The compounds (II) may also be produced in the reaction batch and in situ by reacting about equimolar quantities of a dihalophosphine of the formula (III) ##STR3## with an .alpha.,.beta.-unsaturated acid (IV)R.sup.4 -- OH (IV)In the formulae (III) and (IV) R.sup.1, R.sup.2, R.sup.3 and X are defined as indicated above.In the reaction there is formed, in addition to the compounds (I), practically exclusively .beta.-halopropionic acid and no free hydrogen halide.The phospholanes (I) are valuable flame retarding agents for plastics, intermediates, for example, for the synthesis of biocidals etc.
摘要翻译：式（I）的2,5-二氧代-1,2-氧杂 - 磷酸酯其中R1是有机基团，R2和R3各自也表示有机基团或氢，通过2- 式（II）的卤代甲基乙基 - 次膦酸卤化物其中R 1，R 2和R 3如式（I）中所定义，X表示Cl或Br，优选Cl，具有近似等摩尔量的丙烯酸。化合物（II）也可以在反应批中生产，并通过使约等摩尔量的式（III）的二卤代膦与（α）β-不饱和酸（IV）R 4 -OH反应（IV）式（III）和（IV）中，R 1，R 2，R 3和X如上所述定义。

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