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1. 发明授权

US07790217B2 Method of attaching an antimicrobial cationic polyelectrolyte to the surface of a substrate 有权
标题翻译：将抗微生物阳离子聚电解质连接到基底表面的方法
公开(公告)号：US07790217B2
公开(公告)日：2010-09-07
申请号：US11569942
申请日：2006-08-22
申请人： William Toreki , Bernd Liesenfeld , David Moore , Susan Leander , Christopher Batich
发明人： William Toreki , Bernd Liesenfeld , David Moore , Susan Leander , Christopher Batich
IPC分类号： B05D3/02
CPC分类号： A01N33/12 , A01N37/12 , A61L2/18 , A61L2/232 , A61L15/46 , A61L2300/208 , A61L2300/216 , A61L2300/404 , A61L2300/80 , A01N25/10 , A01N25/24 , A01N25/34 , A01N2300/00
摘要： A method of bonding an antimicrobial cationic polyelectrolyte to the surface of a substrate is described, wherein the antimicrobial thus attached to the substrate provides the substrate with antimicrobial properties, and at least a portion of the bonded antimicrobial is substantially non-leachable during normal conditions of use and storage. A method of manufacturing an antimicrobial material is described which comprises exposure of the substrate to a solution of antimicrobial cationic polyelectrolyte, followed by drying the exposed substrate thoroughly to impart a non-leaching property to at least a portion of the antimicrobial cationic polyelectrolytes.
摘要翻译：描述了将抗微生物阳离子聚电解质结合到基底表面的方法，其中由此附着到基底上的抗微生物赋予底物抗微生物性质，并且至少一部分结合的抗微生物剂在正常条件下基本上不可浸出使用和存储。描述了制造抗微生物材料的方法，其包括将基底暴露于抗微生物阳离子聚电解质溶液，然后彻底干燥曝光的底物，以赋予至少一部分抗微生物阳离子聚电解质非浸出性。

2. 发明授权

US08092854B2 Method of attaching an antimicrobial cationic polyelectrolyte to the surface of a substrate 有权
标题翻译：将抗微生物阳离子聚电解质连接到基底表面的方法
公开(公告)号：US08092854B2
公开(公告)日：2012-01-10
申请号：US12875741
申请日：2010-09-03
申请人： William Toreki , Bernd Liesenfeld , David Moore , Susan Leander , Christopher Batich
发明人： William Toreki , Bernd Liesenfeld , David Moore , Susan Leander , Christopher Batich
IPC分类号： B05D3/02
CPC分类号： A01N33/12 , A01N37/12 , A61L2/18 , A61L2/232 , A61L15/46 , A61L2300/208 , A61L2300/216 , A61L2300/404 , A61L2300/80 , A01N25/10 , A01N25/24 , A01N25/34 , A01N2300/00
摘要： A method of bonding an antimicrobial cationic polyelectrolyte to the surface of a substrate is described, wherein the antimicrobial thus attached to the substrate provides the substrate with antimicrobial properties, and at least a portion of the bonded antimicrobial is substantially non-leachable during normal conditions of use and storage. A method of manufacturing an antimicrobial material is described which comprises exposure of the substrate to a solution of antimicrobial cationic polyelectrolyte, followed by drying the exposed substrate thoroughly to impart a non-leaching property to at least a portion of the antimicrobial cationic polyelectrolytes.
摘要翻译：描述了将抗微生物阳离子聚电解质结合到基底表面的方法，其中由此附着到基底上的抗微生物赋予底物抗微生物性质，并且至少一部分结合的抗微生物剂在正常条件下基本上不可浸出使用和存储。描述了制造抗微生物材料的方法，其包括将基底暴露于抗微生物阳离子聚电解质溶液，然后彻底干燥曝光的底物，以赋予至少一部分抗微生物阳离子聚电解质非浸出性。

3. 发明申请

US20100330261A1 METHOD OF ATTACHING AN ANTIMICROBIAL CATIONIC POLYELECTROLYTE TO THE SURFACE OF A SUBSTRATE 有权
标题翻译：将抗微生物阳离子聚电解质连接到基材表面的方法
公开(公告)号：US20100330261A1
公开(公告)日：2010-12-30
申请号：US12875741
申请日：2010-09-03
申请人： William Toreki , Bernd Liesenfeld , David Moore , Susan Leander , Christopher Batich
发明人： William Toreki , Bernd Liesenfeld , David Moore , Susan Leander , Christopher Batich
IPC分类号： B05D7/00 , B05D3/02 , B05D3/06
CPC分类号： A01N33/12 , A01N37/12 , A61L2/18 , A61L2/232 , A61L15/46 , A61L2300/208 , A61L2300/216 , A61L2300/404 , A61L2300/80 , A01N25/10 , A01N25/24 , A01N25/34 , A01N2300/00
摘要： A method of bonding an antimicrobial cationic polyelectrolyte to the surface of a substrate is described, wherein the antimicrobial thus attached to the substrate provides the substrate with antimicrobial properties, and at least a portion of the bonded antimicrobial is substantially non-leachable during normal conditions of use and storage. A method of manufacturing an antimicrobial material is described which comprises exposure of the substrate to a solution of antimicrobial cationic polyelectrolyte, followed by drying the exposed substrate thoroughly to impart a non-leaching property to at least a portion of the antimicrobial cationic polyelectrolytes.
摘要翻译：描述了将抗微生物阳离子聚电解质结合到基底表面的方法，其中由此附着到基底上的抗微生物赋予底物抗微生物性质，并且至少一部分结合的抗微生物剂在正常条件下基本上不可浸出使用和存储。描述了制造抗微生物材料的方法，其包括将基底暴露于抗微生物阳离子聚电解质溶液，然后彻底干燥曝光的底物，以赋予至少一部分抗微生物阳离子聚电解质非浸出性。

4. 发明申请

US20090181157A1 METHOD OF ATTACHING AN ANTIMICROBIAL CATIONIC POLYELECTROLYTE TO THE SURFACE OF A SUBSTRATE 有权
标题翻译：将抗微生物阳离子聚电解质连接到基材表面的方法
公开(公告)号：US20090181157A1
公开(公告)日：2009-07-16
申请号：US11569942
申请日：2006-08-22
申请人： William Toreki , Bernd Liesenfeld , David Moore , Susan Leander , Christopher Batich
发明人： William Toreki , Bernd Liesenfeld , David Moore , Susan Leander , Christopher Batich
IPC分类号： B05D3/02
CPC分类号： A01N33/12 , A01N37/12 , A61L2/18 , A61L2/232 , A61L15/46 , A61L2300/208 , A61L2300/216 , A61L2300/404 , A61L2300/80 , A01N25/10 , A01N25/24 , A01N25/34 , A01N2300/00
摘要： A method of bonding an antimicrobial cationic polyelectrolyte to the surface of a substrate is described, wherein the antimicrobial thus attached to the substrate provides the substrate with antimicrobial properties, and at least a portion of the bonded antimicrobial is substantially non-leachable during normal conditions of use and storage. A method of manufacturing an antimicrobial material is described which comprises exposure of the substrate to a solution of antimicrobial cationic polyelectrolyte, followed by drying the exposed substrate thoroughly to impart a non-leaching property to at least a portion of the antimicrobial cationic polyelectrolytes.
摘要翻译：描述了将抗微生物阳离子聚电解质结合到基底表面的方法，其中由此附着到基底上的抗微生物赋予底物抗微生物性质，并且至少一部分结合的抗微生物剂在正常条件下基本上不可浸出使用和存储。描述了制造抗微生物材料的方法，其包括将基底暴露于抗微生物阳离子聚电解质溶液，然后彻底干燥曝光的底物，以赋予至少一部分抗微生物阳离子聚电解质非浸出性。

5. 发明申请

US20130011491A1 Antimicrobial Textiles Comprising Peroxide 有权
标题翻译：包含过氧化物的抗菌纺织品
公开(公告)号：US20130011491A1
公开(公告)日：2013-01-10
申请号：US13616209
申请日：2012-09-14
申请人： William Toreki , Albina Mikhaylova , Susan Leander , Bernd Liesenfeld , Gerald M. Olderman
发明人： William Toreki , Albina Mikhaylova , Susan Leander , Bernd Liesenfeld , Gerald M. Olderman
IPC分类号： A01N59/00 , B05D3/00 , A01P1/00 , D06M11/50 , C09K3/00
CPC分类号： D06M11/50 , A61L15/46 , A61L2300/11 , A61L2300/404 , C09D5/14 , C11D3/046 , C11D3/3947 , C11D17/048 , D06M11/155 , D06M11/57 , D06M11/65 , D06M16/00
摘要： This invention pertains to method for imparting a durable antimicrobial activity to substrates, particularly textiles. An acetate-free metal and peroxide antimicrobial treatment formulation is prepared by adjusting the pH of a mixture of a metal salt in aqueous hydrogen peroxide to about 7.5. The substrate is treated with the composition and dried to afford the treated substrate with antimicrobial activity. Zinc salts, ions, or complexes are preferred.
摘要翻译：本发明涉及赋予基材，特别是纺织品持久的抗微生物活性的方法。通过将金属盐在过氧化氢水溶液中的混合物的pH调节至约7.5来制备不含乙酸盐的金属和过氧化物抗微生物处理制剂。用组合物处理底物并干燥以提供具有抗微生物活性的经处理的底物。锌盐，离子或络合物是优选的。

6. 发明申请

US20110171280A1 Antimicrobial Textiles Comprising Peroxide 有权
标题翻译：包含过氧化物的抗菌纺织品
公开(公告)号：US20110171280A1
公开(公告)日：2011-07-14
申请号：US12971659
申请日：2010-12-17
申请人： William Toreki , Albina Mikhaylova , Susan Leander , Bernd Liesenfeld , Gerald M. Olderman
发明人： William Toreki , Albina Mikhaylova , Susan Leander , Bernd Liesenfeld , Gerald M. Olderman
IPC分类号： A01N25/34 , A01N59/00 , A61L15/44 , A61L15/18 , A01P1/00 , C09K3/00 , B05D3/00
CPC分类号： D06M11/50 , A61L15/46 , A61L2300/11 , A61L2300/404 , C09D5/14 , C11D3/046 , C11D3/3947 , C11D17/048 , D06M11/155 , D06M11/57 , D06M11/65 , D06M16/00
摘要： This invention pertains to method for imparting a durable antimicrobial activity to substrates, particularly textiles. An acetate-free metal and peroxide antimicrobial treatment formulation is prepared by adjusting the pH of a mixture of a metal salt in aqueous hydrogen peroxide to about 7.5. The substrate is treated with the composition and dried to afford the treated substrate with antimicrobial activity. Zinc salts, ions, or complexes are preferred.
摘要翻译：本发明涉及赋予基材，特别是纺织品持久的抗微生物活性的方法。通过将金属盐在过氧化氢水溶液中的混合物的pH调节至约7.5来制备不含乙酸盐的金属和过氧化物抗微生物处理制剂。用组合物处理底物并干燥以提供具有抗微生物活性的经处理的底物。锌盐，离子或络合物是优选的。

7. 发明授权

US08926999B2 Antimicrobial textiles comprising peroxide 有权
标题翻译：含有过氧化物的抗菌纺织品
公开(公告)号：US08926999B2
公开(公告)日：2015-01-06
申请号：US13616209
申请日：2012-09-14
申请人： William Toreki , Albina Mikhaylova , Susan Leander , Bernd Liesenfeld , Gerald M. Olderman
发明人： William Toreki , Albina Mikhaylova , Susan Leander , Bernd Liesenfeld , Gerald M. Olderman
IPC分类号： A01N59/00 , B05D3/00 , A01P1/00 , D06M11/50 , C09K3/00 , D06M11/155 , D06M11/65 , D06M16/00
CPC分类号： D06M11/50 , A61L15/46 , A61L2300/11 , A61L2300/404 , C09D5/14 , C11D3/046 , C11D3/3947 , C11D17/048 , D06M11/155 , D06M11/57 , D06M11/65 , D06M16/00
摘要： This invention pertains to method for imparting a durable antimicrobial activity to substrates, particularly textiles. An acetate-free metal and peroxide antimicrobial treatment formulation is prepared from a metal derivative, hydrogen peroxide and a source of hydroxide ion. The substrate is treated with the composition and dried to afford the treated substrate with antimicrobial activity. Zinc salts, ions, or complexes are preferred.
摘要翻译：本发明涉及赋予基材，特别是纺织品持久的抗微生物活性的方法。从金属衍生物，过氧化氢和氢氧根离子源制备无乙酸盐的金属和过氧化物抗微生物处理制剂。用组合物处理底物并干燥以提供具有抗微生物活性的经处理的底物。锌盐，离子或络合物是优选的。

8. 发明授权

US08277827B2 Antimicrobial textiles comprising peroxide 有权
标题翻译：含有过氧化物的抗菌纺织品
公开(公告)号：US08277827B2
公开(公告)日：2012-10-02
申请号：US12971659
申请日：2010-12-17
申请人： William Toreki , Albina Mikhaylova , Susan Leander , Bernd Liesenfeld , Gerald M. Olderman
发明人： William Toreki , Albina Mikhaylova , Susan Leander , Bernd Liesenfeld , Gerald M. Olderman
IPC分类号： A01N25/34 , A01N59/00 , A61L15/44 , A61L15/18 , A01P1/00 , C09K3/00 , B05D3/00
CPC分类号： D06M11/50 , A61L15/46 , A61L2300/11 , A61L2300/404 , C09D5/14 , C11D3/046 , C11D3/3947 , C11D17/048 , D06M11/155 , D06M11/57 , D06M11/65 , D06M16/00
摘要： This invention pertains to method for imparting a durable antimicrobial activity to substrates, particularly textiles. An acetate-free metal and peroxide antimicrobial treatment formulation is prepared by adjusting the pH of a mixture of a metal salt in aqueous hydrogen peroxide to about 7.5. The substrate is treated with the composition and dried to afford the treated substrate with antimicrobial activity. Zinc salts, ions, or complexes are preferred.
摘要翻译：本发明涉及赋予基材，特别是纺织品持久的抗微生物活性的方法。通过将金属盐在过氧化氢水溶液中的混合物的pH调节至约7.5来制备不含乙酸盐的金属和过氧化物抗微生物处理制剂。用组合物处理底物并干燥以提供具有抗微生物活性的经处理的底物。锌盐，离子或络合物是优选的。

9. 发明申请

US20080206293A1 Absorbent substrate with a non-leaching antimicrobial activity and a controlled-release bioactive agent. 审中-公开
标题翻译：具有非浸出抗菌活性的吸收性底物和受控释放的生物活性剂。
公开(公告)号：US20080206293A1
公开(公告)日：2008-08-28
申请号：US12036107
申请日：2008-02-22
申请人： William Toreki , Bernd Liesenfeld , David Moore , Gregory Schultz , Gerald Olderman , Gregory Staab
发明人： William Toreki , Bernd Liesenfeld , David Moore , Gregory Schultz , Gerald Olderman , Gregory Staab
IPC分类号： A61K9/00 , A61F13/00 , A61K31/65 , A61K38/18 , A01N25/08 , A01P1/00 , A61P31/04 , A61K38/02 , A01N25/00 , A61K31/165 , A61K31/14
CPC分类号： A61L15/44 , A61L15/46
摘要： This invention relates to antimicrobial wound dressings having a non-leaching antimicrobial activity, releasable antimicrobial and antiprotease agents, and a controlled-release bioactive agent such as doxycycline. The Wound dressing material is absorbent and acts as a substrate for antimicrobial and antiprotease agents as well as bioactive agents. More generally, this invention relates to methods and compositions for materials having a non-leaching coating that has antimicrobial properties. The coating is applied to substrates such as gauze-type wound dressings, powders and other substrates. Covalent, non-leaching, non-hydrolyzable bonds are formed between the substrate and the polymer molecules that form the coating. A high concentration of anti-microbial groups on multi-length polymeric molecules and relatively long average chain lengths, contribute to an absorbent or superabsorbent surface with a high level antimicrobial efficacy. Utilization of non-leaching coatings having a plurality of anionic or cationic sites is used according to this invention to bind a plurality of oppositely charged biologically or chemically active compounds, and to release the bound oppositely charged biologically or chemically active compounds from said substrate over a period of time to achieve desired objectives as diverse as improved wound healing to reduction in body odor.
摘要翻译：本发明涉及具有非浸出抗微生物活性的抗微生物伤口敷料，可释放的抗微生物剂和抗蛋白酶试剂，以及控释释放生物活性剂如多西环素。伤口敷料材料是吸收剂并用作抗微生物剂和抗蛋白酶剂以及生物活性剂的底物。更一般来说，本发明涉及具有抗菌性能的非浸出涂层的材料的方法和组合物。将涂层施加到诸如纱布式伤口敷料，粉末和其它底物的基底上。在底物和形成涂层的聚合物分子之间形成共价，非浸出，不可水解的键。在多长度聚合物分子上具有高浓度的抗微生物群和相当长的平均链长，有助于具有高水平抗微生物效能的吸收剂或超吸收剂表面。根据本发明使用具有多个阴离子或阳离子位点的非浸出涂层的使用以结合多个带相反电荷的生物或化学活性化合物，并通过一个或多个阴离子或化学活性化合物从所述底物上释放结合的带相反电荷的生物或化学活性化合物一段时间以达到预期的目标，如改善伤口愈合以减少体臭。

10. 发明授权

US08545862B2 Polyelectrolyte complex for imparting antimicrobial properties to a substrate 有权
标题翻译：用于赋予基质抗微生物性能的聚电解质络合物
公开(公告)号：US08545862B2
公开(公告)日：2013-10-01
申请号：US12830062
申请日：2010-07-02
申请人： William Toreki , David N. Moore , Bernd Liesenfeld , Albina Mikhaylova , Gerald M. Olderman
发明人： William Toreki , David N. Moore , Bernd Liesenfeld , Albina Mikhaylova , Gerald M. Olderman
IPC分类号： A01N25/00
CPC分类号： A61F13/00995 , A61F13/00063 , A61F2013/0091 , A61F2013/00931 , A61L2/18 , A61L2/232 , A61L15/44 , A61L15/46 , A61L2202/24 , A61L2202/26 , Y10T428/3154 , Y10T428/31565 , Y10T428/31663 , Y10T428/31736 , Y10T428/3179 , Y10T428/31797
摘要： Anionic polyelectrolytes are used as binding agents to reduce the solubility of cationic antimicrobial polyelectrolytes. Ionic attraction between the anionic stabilizing polyelectrolytes and the antimicrobial cationic polyelectrolytes results in formation of a polyelectrolyte complex (PEC). A treatment liquid comprising a stable colloid, suspension, dispersion, solution, coacervate, or emulsion of the PEC in an aqueous carrier is used to treat an article, thus coating, infiltrating, or infusing the PEC onto or into the article. Subsequent drying results in an antimicrobial article wherein the PEC is bound to the article and is significantly less prone, relative to either of the component polyelectrolytes, to being washed, leached, leaked, extracted, or migrated from the antimicrobial article during use, or when exposed to aqueous fluids or solvents. The antimicrobial article can be further treated with ethylene oxide which enhances its antimicrobial efficacy, its biocompatibility, and its utility in wound dressings, medical devices, clothing, etc.
摘要翻译：阴离子聚电解质用作粘合剂以降低阳离子抗菌聚电解质的溶解度。阴离子稳定聚电解质与抗微生物阳离子聚电解质之间的离子吸引导致聚电解质络合物（PEC）的形成。使用包含PEC在水性载体中的稳定的胶体，悬浮液，分散体，溶液，凝聚层或乳液的处理液来处理制品，从而将PEC涂覆，渗透或注入到物品上或进入该物品。随后的干燥导致抗微生物制品，其中PEC与制品结合，并且相对于组分聚电解质中的任何一种，在使用期间被洗涤，浸出，泄漏，提取或从抗微生物制品迁移，或者当暴露于含水流体或溶剂。抗菌制品可以进一步用环氧乙烷处理，提高其抗菌效能，其生物相容性及其在伤口敷料，医疗器械，衣服等中的应用。

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