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1. 发明授权

US5615492A Drying of water-containing useful materials or mixtures thereof with superheated steam 失效
标题翻译：含水有用材料或其与过热蒸汽的混合物的干燥
公开(公告)号：US5615492A
公开(公告)日：1997-04-01
申请号：US569176
申请日：1996-02-23
申请人： Wilfried Raehse , Gunter Effey , Wilhelm Beck
发明人： Wilfried Raehse , Gunter Effey , Wilhelm Beck
IPC分类号： A23C1/04 , A23L3/46 , A61K9/14 , B01D1/18 , B01J2/04 , C11D11/02 , F26B3/12 , F26B17/10 , F26B21/06
CPC分类号： B01D1/18 , F26B3/12
摘要： A process for drying water-containing materials in a closed-circuit system using a vertical drying tower having inlets located at a lower portion of the tower, the inlets circulating superheated steam in countercurrent to the water-containing materials descending through the vertical drying tower thereby drying the water-containing materials, the improvement being:(a) providing an auxiliary fluid having a temperature below that of the superheated steam entering into the vertical drying tower;(b) providing a double jacket having a permeable inner wall wherein the double jacket surrounds the lower portion of the vertical drying tower below the inlets; and(c) introducing the auxiliary fluid through the permeable inner wall of the double jacket and into the vertical drying tower in a tangential or radial direction relative to the permeable inner wall.
摘要翻译： PCT No.PCT / EP94 / 01987 371日期1996年2月23日 102（e）日期1996年2月23日PCT提交1994年6月18日PCT公布。公开号WO95 / 00222 日期1995年1月5日一种使用垂直干燥塔在闭路系统中干燥含水材料的方法，所述立式干燥塔具有位于塔的下部的入口，所述入口循环过热蒸汽与所述含水材料逆流通过垂直干燥塔由此干燥含水材料，其改进在于：（a）提供温度低于进入垂直干燥塔的过热蒸汽温度的辅助流体; （b）提供具有可渗透内壁的双层护套，其中双层护套围绕入口下方的垂直干燥塔的下部包围; 和（c）将辅助流体通过双层护套的可渗透的内壁引入相对于可渗透的内壁的切向或径向的垂直干燥塔中。

2. 发明授权

US5785859A Optimized process for conditioning steam-based vapor streams 失效
标题翻译：基于蒸汽蒸汽流的优化方法
公开(公告)号：US5785859A
公开(公告)日：1998-07-28
申请号：US682796
申请日：1996-10-18
申请人： Wilfried Raehse , Reiner Vogler , Johann F. Fues , Wilhelm Beck , Kathleen Paatz , Truc Tran Anh , Levent Yueksel
发明人： Wilfried Raehse , Reiner Vogler , Johann F. Fues , Wilhelm Beck , Kathleen Paatz , Truc Tran Anh , Levent Yueksel
IPC分类号： B01D1/00 , B01D1/18 , B01D5/00 , B01D17/02 , B01D17/04 , B01D61/02 , B01D61/14 , B01D61/16 , C02F1/44 , C07B63/00 , C11B9/02 , C11D13/30 , F26B25/00 , B01D47/00 , B01D61/00
CPC分类号： B01D61/022 , B01D17/0214 , B01D5/003 , B01D5/0057 , B01D5/0093 , B01D61/02 , B01D61/147 , B01D61/16 , C02F1/444 , C07B63/00 , C11B9/022 , F26B25/006 , B01D17/047 , B01D17/048 , Y02P70/34 , Y02P70/40
摘要： The invention relates to an optimized process for conditioning a stream of superheated steam laden with steam-volatile organic components by condensation of the steam phase with recovery of the heat of condensation and at least partial separation of the steam-volatile organic components from the water-based condensate. The process operates with a first heat exchange stage in which the continuously introduced vapor stream is combined with a circulated and cooled liquid stream of condensed vapors. In a following second energy transfer stage, heat is indirectly removed from the liquid stream thus heated. A sidestream is removed from the liquid circuit of the condensed vapors and subjected to separation in a membrane process while the rest of the liquid stream is returned to the first stage. The invention also relates to the use of this working principle for industrial applications, more particularly for the separation of organic mixtures by superheated steam and/or the drying of water-based useful-material preparations with superheated steam as the drying gas.
摘要翻译： PCT No.PCT / EP95 / 00228 Sec。 371日期：1996年10月18日 102（e）日期1996年10月18日PCT提交1995年1月23日PCT公布。公开号WO95 / 21010 日期1995年8月10日本发明涉及一种优化的方法，用于通过蒸汽相的冷凝与回收冷凝热来调节负载有蒸汽挥发性有机成分的过热蒸汽流，并且至少部分分离蒸汽挥发性有机物来自水基冷凝物的组分。该过程在第一热交换阶段中进行，其中连续引入的蒸气流与循环和冷却的冷凝蒸气的液流混合。在接下来的第二能量转移阶段中，从被加热的液体流中间接地除去热量。侧流从冷凝蒸汽的液体回路中除去，并在膜过程中分离，而其余液体流返回到第一级。本发明还涉及这种工业原理在工业应用中的应用，特别是用于通过过热蒸汽分离有机混合物和/或用作为干燥气体的过热蒸汽的水基有用材料制剂的干燥。

3. 发明授权

US5814597A Multicomponent mixtures based on water-soluble alkali metal silicate compounds and their use, more particularly as builders in detergents 失效
标题翻译：基于水溶性碱金属硅酸盐化合物的多组分混合物及其用途，更特别地作为洗涤剂中的助洗剂
公开(公告)号：US5814597A
公开(公告)日：1998-09-29
申请号：US700485
申请日：1996-10-10
申请人： Wilfried Raehse , Johann F. Fues , Kathleen Paatz , Wilhelm Beck , Wolfgang Hlavacek
发明人： Wilfried Raehse , Johann F. Fues , Kathleen Paatz , Wilhelm Beck , Wolfgang Hlavacek
IPC分类号： C01B33/32 , C11D3/02 , C11D3/06 , C11D3/08 , C11D3/10 , C11D3/20 , C11D3/37 , C11D11/00 , C11D11/02
CPC分类号： C11D3/046 , C11D11/0082 , C11D11/02 , C11D3/06 , C11D3/08 , C11D3/10 , C11D3/2075 , C11D3/3761
摘要： The invention relates to a solid material (primary drying product) containing alkali metal silicate with a modulus (molar ratio of SiO.sub.2 to M.sub.2 O, M=alkali metal) of 0.8 to 4 in homogeneous admixture with other inorganic and/or organic useful materials and/or auxiliaries, which has been dried from a finely sprayed aqueous preparation of mixtures of the alkali metal silicates and the inorganic and/or organic useful materials and/or auxiliaries by means of a hot gas stream. The solid material according to the invention is characterized in that, as a primary drying product in homogeneous admixture with the alkali metal silicate, it contains at least 10% by weight of water-soluble inorganic and/or organic salts, has apparent densities of at least 150 g/l, possesses a microporous absorbent internal structure and has been dried with superheated steam as the hot gas stream. The invention also relates in particular to detergent builder systems based on multicomponent systems containing this overdried alkali metal silicate and to their use for subsequent impregnation with other free-flowing useful materials and mixtures thereof from the field of detergents and to the detergents obtained.
摘要翻译： PCT No.PCT / EP95 / 00604 Sec。 371日期：1996年10月10日 102（e）日期1996年10月10日PCT提交1995年2月20日PCT公布。第WO95 / 23841号公报日期1995年9月8日本发明涉及含有碱金属硅酸盐的固体材料（初级干燥产物），其模量（SiO 2与M 2 O的摩尔比，M =碱金属）为0.8〜4，与其它无机和/或有机有用材料和/或辅助剂，其已经通过热气流由碱金属硅酸盐和无机和/或有机有用材料和/或助剂的混合物的精细喷雾的水性制剂干燥。根据本发明的固体材料的特征在于，作为与碱金属硅酸盐均匀混合的初级干燥产物，其含有至少10重量％的水溶性无机和/或有机盐，其表观密度为至少150g / l，具有微孔吸收性内部结构，并用过热蒸汽作为热气流进行干燥。本发明还特别涉及基于含有这种过度浸渍的碱金属硅酸盐的多组分体系的洗涤剂助洗剂体系，以及其用于随后从洗涤剂领域和所得洗涤剂的其它自由流动的有用材料及其混合物浸渍的用途。

4. 发明授权

US5544427A Process for the production of granules suitable as wetting agents, detergents and/or cleaning products 失效
标题翻译：用于生产适合作为润湿剂，洗涤剂和/或清洁产品的颗粒的方法
公开(公告)号：US5544427A
公开(公告)日：1996-08-13
申请号：US284694
申请日：1994-08-12
申请人： Wilfried Raehse , Wilhelm Beck , Dieter Jung , Dieter Sonnemann
发明人： Wilfried Raehse , Wilhelm Beck , Dieter Jung , Dieter Sonnemann
IPC分类号： F26B21/02 , B01D1/14 , B01D1/18 , B01F17/00 , B01J2/02 , B01J2/04 , B01J2/16 , C11D11/00 , C11D11/02 , C11D11/04 , C11D17/06 , F26B3/12 , F26B21/04 , F26B3/08
CPC分类号： C11D11/0082 , B01D1/18 , C11D11/02 , C11D11/04 , F26B21/04 , F26B3/12
摘要： A process for the production of pourable and free flowing granules of materials or mixtures thereof which are suitable for use as wetting agents, detergents or cleaning products wherein an aqueous solution or suspension of the wetting agents, detergents or cleaning products is dried using a hot gas stream of superheated steam. Drying is terminated before the granules are damaged by heat, and the hot gas stream is freed from entrained particles of the materials by means of filters.
摘要翻译： PCT No.PCT / EP93 / 00265 Sec。 371日期1994年8月12日 102（e）日期1994年8月12日PCT提交1993年2月4日PCT公布。第WO93 / 15812号公报日期1993年8月19日一种用于生产可倾倒和自由流动的材料或其混合物的颗粒的方法，其适用于润湿剂，洗涤剂或清洁产品，其中润湿剂，洗涤剂或清洁产品的水溶液或悬浮液为使用过热蒸汽的热气流干燥。在颗粒被热损坏之前，干燥终止，并且通过过滤器将热气流从材料夹带的颗粒中除去。

5. 发明授权

US5519948A Process for the production of granules suitable as wetting agents, detergents and/or cleaning products 失效
标题翻译：用于生产适合作为润湿剂，洗涤剂和/或清洁产品的颗粒的方法
公开(公告)号：US5519948A
公开(公告)日：1996-05-28
申请号：US284613
申请日：1994-10-26
申请人： Wilfried Raehse , Johann Fues , Wilhelm Beck , Otto Koch
发明人： Wilfried Raehse , Johann Fues , Wilhelm Beck , Otto Koch
IPC分类号： F26B21/02 , B01D1/14 , B01D1/18 , B01J2/16 , C11D11/00 , C11D11/02 , C11D11/04 , F26B3/12 , F26B21/04 , F26B3/00
CPC分类号： B01D1/18 , C11D11/0082 , C11D11/02 , C11D11/04 , F26B21/04 , F26B3/12
摘要： A process for the production of pourable, free-flowing granules which are suitable for use as wetting agents, detergents or cleaning products from aqueous solutions or suspensions of such materials in a fluidized-bed spray granulation apparatus employing a hot fluidizing gas. The aqueous selections or suspensions are dried with superheated steam as the fluidizing and drying gas wherein the drying step is carried out in a closed-loop system comprising a steam circuit from which the water evaporated from the aqueous solutions or suspensions of starting materials is removed as a partial stream and the thermal energy released is returned to the steam circuit. The granules are discharged from the granulation apparatus before they can be damaged by heat.
摘要翻译： PCT No.PCT / EP93 / 00266 Sec。 371日期：1994年10月26日 102（e）日期1994年10月26日PCT提交1993年2月4日PCT公布。出版物WO93 / 15813 日期1988年8月19日。一种用于生产可倾倒，自由流动的颗粒的方法，其适用于在水溶液或这些材料的悬浮液中用作润湿剂，洗涤剂或清洁产品，在流化床喷雾造粒设备中使用热流化气。水性选择或悬浮液用作为流化和干燥气体的过热蒸汽干燥，其中干燥步骤在闭环系统中进行，所述闭环系统包括蒸汽回路，从蒸汽回路中蒸发出水溶液或原料悬浮液，部分流和释放的热能返回到蒸汽回路。颗粒在造成热量损坏之前从造粒装置中排出。

6. 发明授权

US07417019B2 Hollow body with a compartment, containing a portion of a washing, cleaning or rinsing agent 有权
标题翻译：空心体带有隔间，其中包含一部分洗涤剂，清洁剂或漂洗剂
公开(公告)号：US07417019B2
公开(公告)日：2008-08-26
申请号：US10333067
申请日：2001-07-04
申请人： Henriette Weber , Sandra Hoffmann , Wilfried Raehse , Dieter Jung , Frank Meier , Christian Block , Rolf Bayersdoerfer , Markus Semrau , Karl-Martin Faeser , Paul Birnbrich , Dieter Nickel
发明人： Henriette Weber , Sandra Hoffmann , Wilfried Raehse , Dieter Jung , Frank Meier , Christian Block , Rolf Bayersdoerfer , Markus Semrau , Karl-Martin Faeser , Paul Birnbrich , Dieter Nickel
IPC分类号： C11D17/00 , C11D3/395
CPC分类号： C11D17/042 , C11D17/043 , C11D17/045
摘要： Detergent portions containing at least one detersive formulation wholly or partly contained in a dimensionally stable hollow body having an enclosure that wholly or partly surrounds the detersive formulation, the enclosure being formed of an uncompressed material that can disintegrate under laundering, cleaning, or washing conditions and that gives the hollow body dimensional stability, and optionally, the dimensionally stable hollow body having one or more means forming one or more compartments therein.
摘要翻译：洗涤剂部分含有至少一种完全或部分地包含在尺寸稳定的中空体中的洗涤剂制剂，该中空体具有完全或部分包围洗涤制剂的外壳，该外壳由在洗衣，清洗或洗涤条件下可分解的未压缩材料形成，其赋予中空体的尺寸稳定性，并且可选地，尺寸稳定的中空体具有一个或多个在其中形成一个或多个隔室的装置。

7. 发明申请

US20050245425A1 Dry neutralisation method II 审中-公开
标题翻译：干中和法二
公开(公告)号：US20050245425A1
公开(公告)日：2005-11-03
申请号：US11148825
申请日：2005-06-09
申请人： Bernhard Orlich , Gerhard Blasey , Hans-Friedrich Kruse , Wilfried Raehse
发明人： Bernhard Orlich , Gerhard Blasey , Hans-Friedrich Kruse , Wilfried Raehse
IPC分类号： C11D11/00 , C11D17/06 , C11D17/00
CPC分类号： C11D17/065 , C11D11/0088 , C11D17/06
摘要： A process for making detergent granules having a bulk density of 300 to 700 g/l. A solid carrier containing neutralizing agent is mixed in a rotating mixer with a liquid binding agent containing surfactant acid to forma partially granulated premixture. The premixture is fluidized, sprayed with additional binder, and granulated in a fluidized bed reactor to form the detergent granules.
摘要翻译：一种制备体积密度为300-700g / l的洗涤剂颗粒的方法。将含有中和剂的固体载体在旋转混合器中与含有表面活性剂酸的液体粘合剂混合以形成部分颗粒状预混合物。将预混合物流化，用另外的粘合剂喷雾，并在流化床反应器中造粒形成洗涤剂颗粒。

8. 发明授权

US06458755B2 Amorphous alkali metal silicate compound 有权
公开(公告)号：US06458755B2
公开(公告)日：2002-10-01
申请号：US09734052
申请日：2000-12-11
申请人： Kathrin Schnepp-Hentrich , Rene-Andres Artiga Gonzalez , Katrin Burmeister , Hubert Freese , Manfred Greger , Bernd Larson , Volker Bauer , Peter Sandkuehler , Wilfried Raehse
发明人： Kathrin Schnepp-Hentrich , Rene-Andres Artiga Gonzalez , Katrin Burmeister , Hubert Freese , Manfred Greger , Bernd Larson , Volker Bauer , Peter Sandkuehler , Wilfried Raehse
IPC分类号： C11D308
CPC分类号： C11D3/08 , C11D11/00 , C11D11/02
摘要： A spray-dried amorphous alkali metal silicate compound which provides multiple-cycle washing performance. The silicate compound has a molar ratio of M2O to SiO2 of 1:1.5 to 1:3.3 wherein M represents an alkali metal. The compound contains 0.5 to less than 30% by weight of anionic surfactant and has an absorption capacity for liquid components which is at least 20% higher than that of the same quantity of the alkali metal silicate compound which is free from anionic surfactant.

9. 发明授权

US5783545A Enzyme preparation containing a silver corrosion inhibitor 失效
标题翻译：含有银腐蚀抑制剂的酶制剂
公开(公告)号：US5783545A
公开(公告)日：1998-07-21
申请号：US663301
申请日：1996-07-24
申请人： Kathleen Paatz , Wilfried Raehse , Juergen Haerer , Werner Pichler , Birgit Burg
发明人： Kathleen Paatz , Wilfried Raehse , Juergen Haerer , Werner Pichler , Birgit Burg
IPC分类号： C09K15/02 , C11D3/02 , C11D3/12 , C11D3/386 , C11D17/00 , C12N9/98 , C23F11/00 , C11D3/00 , C11D7/18 , C11D7/54
CPC分类号： C11D3/048 , C09K15/02 , C11D17/0039 , C11D3/046 , C11D3/1213 , C11D3/122 , C11D3/38672 , C12N9/98 , C23F11/00
摘要： The invention provides an enzyme containing granule with a coating containing a silver corrosion inhibitor. The particle is formed from a core containing a first enzyme and an organic or inorganic carrier which can be coated with a second particulate enzyme. The core is coated with a coating containing at least one salt of manganese, titanium, zirconium, hafnium, vanadium, cobalt and cerium. A method for preparing the granule is also disclosed.
摘要翻译： PCT No.PCT / EP94 / 04152 Sec。 371日期：1996年7月24日 102（e）日期1996年7月24日PCT 1994年12月14日PCT PCT。 WO95 / 17493 PCT出版物日期：1995年6月29日本发明提供了含有含有银腐蚀抑制剂的涂层的含酶颗粒。颗粒由含有第一酶和可以用第二颗粒酶包被的有机或无机载体的核心形成。核心涂覆有包含至少一种锰，钛，锆，铪，钒，钴和铈的盐的涂层。还公开了制备颗粒的方法。

10. 发明授权

US5536430A Process of producing low-dust anionic surfactant concentrates in powder or granule form with improved solubility in aqueous media 失效
标题翻译：生产低灰尘阴离子表面活性剂的方法是粉末或颗粒形式，在水性介质中具有改善的溶解性
公开(公告)号：US5536430A
公开(公告)日：1996-07-16
申请号：US290860
申请日：1994-10-12
申请人： Johann Fues , Wilfried Raehse , Kathleen Paatz , Wolfgang Poly , Bert Gruber , Andreas Syldath , Sven Welper , Herbert Pattberg
发明人： Johann Fues , Wilfried Raehse , Kathleen Paatz , Wolfgang Poly , Bert Gruber , Andreas Syldath , Sven Welper , Herbert Pattberg
IPC分类号： B01D1/14 , B01D1/18 , C11D1/02 , C11D11/00 , C11D11/02 , C11D11/04 , C11D17/06 , F26B3/12 , F26B21/04
CPC分类号： C11D11/02 , B01D1/18 , C11D11/0082 , C11D11/04 , C11D17/06 , F26B21/04 , F26B3/12
摘要： Anionic surfactant concentrates in the form of solid free-flowing powders and/or granules which may also be present as compounds in admixture with other auxiliaries and/or useful materials suitable for use in detergents and/or cleaning products and which have apparent densities of at least about 150 g/l are produced by hot drying of the water-containing preparations with superheated steam as the drying gas. Preferred apparent densities are above about 200 g/l and are preferably at least about 350 g/l. In addition, the pourable and free-flowing material is preferably in the form of a substantially dust-free material through the presence of dust-binding auxiliaries and/or useful materials and/or by regulation of the residual water content. In one preferred embodiment, the anionic surfactant concentrate is in the form of porous carrier beads with an absorbent porous inner structure.
摘要翻译： PCT No.PCT / EP93 / 00302 Sec。 371日期：1994年10月12日 102（e）日期1994年10月12日PCT 1993年2月9日PCT公布。公开号WO93 / 16165 日期：1993年8月19日。阴离子表面活性剂以固体自由流动的粉末和/或颗粒的形式浓缩，其也可以作为化合物以与适用于洗涤剂和/或清洁产品的其它助剂和/或有用材料混合的形式存在并且具有至少约150g / l的表观密度通过用作为干燥气体的过热蒸汽的含水制剂进行热干燥而产生。优选的表观密度高于约200g / l，优选至少约350g / l。此外，可倾倒和自由流动的材料优选通过存在粉尘结合助剂和/或有用材料和/或通过调节残余水含量而基本上无粉尘的材料的形式。在一个优选的实施方案中，阴离子表面活性剂浓缩物是具有吸收性多孔内部结构的多孔载体珠粒的形式。

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