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1. 发明授权

US06887927B2 Fluoropolymer compositions containing a nitrogen cure site monomer and a sulfone or sulfoxide compound 失效
标题翻译：含有氮固化位点单体和砜或亚砜化合物的含氟聚合物组合物
公开(公告)号：US06887927B2
公开(公告)日：2005-05-03
申请号：US10228507
申请日：2002-08-27
申请人： Werner M.A. Grootaert , Robert E. Kolb
发明人： Werner M.A. Grootaert , Robert E. Kolb
IPC分类号： C08J3/24 , C08F14/18 , C08K5/00 , C08K5/19 , C08K5/41 , C08K5/50 , C08L27/12
CPC分类号： C08F14/18 , C08K5/0025 , C08L27/12
摘要： Compositions comprising a fluoropolymer derived from a nitrogen-containing cure site monomer, a catalyst composition which comprises at least one anionic functional group and at least one cationic functional group having the formula QR′k(+), wherein Q is selected from phosphorous, sulfur, nitrogen, arsenic, or antimony, wherein each R′ is independently selected from hydrogen and a nonfluorinated, partially fluorinated, or perfluorinated, C1-C20 alkyl, aryl, aralkyl, or alkenyl group, and wherein k is the valence of Q plus one; wherein the catalyst composition is a compound or the precursors thereof added separately or as a mixture; and a composition of the formula: R″2SOx wherein each R″ is C1-C30 alkyl, aralkyl, the two R″ groups together form a heterocyclic C3-C30 cycloalkyl, aryl, or aralkyl, each R″ can be fluorinated, and x is 1 or 2. Also provided are methods of making a fluoropolymer and fluoropolymer articles containing fluoropolymer compositions.
摘要翻译：包含衍生自含氮固化位点单体的含氟聚合物的组合物，包含至少一个阴离子官能团的催化剂组合物和至少一种具有式QR'（+ ）其中Q选自磷，硫，氮，砷或锑，其中每个R'独立地选自氢和非氟化，部分氟化或全氟化的C 1 H 2， -C 20烷基，芳基，芳烷基或烯基，其中k是Q + 1的化合价; 其中所述催化剂组合物是分别或作为混合物加入的化合物或其前体; 和式“R”2 SO x x的组合物，其中每个R“为C 1 -C 30 - ， - 烷基，芳烷基，两个R“基团一起形成杂环C 3 -C 30 - 环烷基，芳基或芳烷基，每个R”可以被氟化，并且x是1或2.还提供了制备含氟聚合物组合物的含氟聚合物和含氟聚合物制品的方法。

2. 发明授权

US06890995B2 Fluoropolymer compositions 有权
标题翻译：含氟聚合物组合物
公开(公告)号：US06890995B2
公开(公告)日：2005-05-10
申请号：US10060690
申请日：2002-01-30
申请人： Robert E. Kolb , Werner M. A. Grootaert , Klaus Hintzer
发明人： Robert E. Kolb , Werner M. A. Grootaert , Klaus Hintzer
IPC分类号： C08L27/12 , C08K5/00 , C08K5/50 , C08L29/10 , C08F8/34
CPC分类号： C08K5/0025 , C08K5/50 , C08L27/12 , C08L27/18
摘要： Compositions comprising a fluoropolymer having interpolymerized units derived from a nitrogen-containing cure site monomer and a catalyst composition are provided. The catalyst composition includes a compound having the general formula: {RA}(−){QR′k}(+) or the precursors thereof, wherein R is a nonfluorinated, partially fluorinated, or perfluorinated alkyl, alkenyl, cycloalkyl, cycloalkenyl, aryl or aralkyl, A is an acid- or acid-derivative anion, Q is phosphorous, sulfur, nitrogen, arsenic, or antimony, and each R′ is hydrogen or an alkyl, aryl, aralkyl, or alkenyl group, k is the valence of Q; and optionally (c) an alcohol of the formula R2—OH, wherein R2 is an alkyl group which can be fluorinated. Also provided are a method of making a fluoropolymer, a method of increasing induction time, and fluoropolymer articles containing curable or cured fluoropolymer compositions.
摘要翻译：提供包含含有衍生自含氮固化位点单体的共聚单元的含氟聚合物和催化剂组合物的组合物。催化剂组合物包括具有以下通式的化合物：<？in-line-formula description =“In-line Formulas”end =“lead”？> {RA}（ - ）< （+）线内公式描述=“在线公式”end =“尾”→其前体，其中R是非氟化，部分氟化的或全氟化的烷基，烯基，环烷基，环烯基，芳基或芳烷基，A是酸或酸衍生的阴离子，Q是磷，硫，氮，砷或锑，并且每个R'是氢或烷基，芳基，芳烷基或烯基，k是Q的化合价; 和任选地（c）式R 2 -OH的醇，其中R 2是可被氟化的烷基。还提供了制备含氟聚合物的方法，增加诱导时间的方法和含有可固化或固化的含氟聚合物组合物的含氟聚合物制品。

3. 发明授权

US06720360B1 Ultra-clean fluoropolymers 失效
标题翻译：超清洁含氟聚合物
公开(公告)号：US06720360B1
公开(公告)日：2004-04-13
申请号：US09495600
申请日：2000-02-01
申请人： Werner M. A. Grootaert , Georg Burkard , William D. Coggio , Klaus Hintzer , Bernhard Hirsch , Robert E. Kolb , Albert Killich , Gernot Loehr
发明人： Werner M. A. Grootaert , Georg Burkard , William D. Coggio , Klaus Hintzer , Bernhard Hirsch , Robert E. Kolb , Albert Killich , Gernot Loehr
IPC分类号： C08J520
CPC分类号： C09D127/18 , C08F6/16 , C08F6/22 , C08F14/18 , C08K5/14 , C08L27/12 , C08L27/18 , C08L2205/02 , C09D127/12 , C08F2/16 , C08L2666/04 , C08F2/22
摘要： High purity fluoropolymers are obtained by the emulsion polymerization process, removing essentially all ions and coagulating the polymer essentially without adding ions. These polymers are useful in the field of electronic devices.
摘要翻译：通过乳液聚合方法获得高纯度含氟聚合物，基本上除去所有离子并基本上凝结聚合物而不添加离子。这些聚合物在电子设备领域是有用的。

4. 发明授权

US06566455B2 Fluoropolymer composition with organo-onium and blocked oxalate and carbonate compounds 有权
公开(公告)号：US06566455B2
公开(公告)日：2003-05-20
申请号：US10033483
申请日：2001-12-28
申请人： Naiyong Jing , Brant U. Kolb , Robert E. Kolb
发明人： Naiyong Jing , Brant U. Kolb , Robert E. Kolb
IPC分类号： C08L2722
CPC分类号： C07C69/63 , C07C69/36 , C08K5/09 , C08L75/00
摘要： In one aspect, the invention provides curable fluoropolymer compositions comprising fluoropolymer, onium, and alkyl or aryl oxalate-blocked compound and carbonate-blocked compound as crosslinking agents. In other aspects, the invention provides methods of making curable fluoropolymer compositions and provides alkyl or aryl oxalate-blocked and carbonate-blocked compounds.

5. 发明授权

US06482522B1 Elastomer compositions for bonding to fluoropolymers 失效
标题翻译：用于结合含氟聚合物的弹性体组合物
公开(公告)号：US06482522B1
公开(公告)日：2002-11-19
申请号：US08994378
申请日：1997-12-19
申请人： Edward E. Parsonage , Robert E. Kolb
发明人： Edward E. Parsonage , Robert E. Kolb
IPC分类号： B32B2700
CPC分类号： B32B27/08 , B32B25/04 , C08J5/12 , C08L19/003 , Y10T156/1089 , Y10T428/1352 , Y10T428/3154 , Y10T428/31544
摘要： A method for increasing the adhesion of a first layer comprising a fluoropolymer substantially free of interpolymerized units derived from vinylidene fluoride to a second layer comprising a curable elastomer is described. The method comprises adding a dehydrofluorinating composition to the curable elastomer, contacting the layers and curing the layered article so formed. The resulting multilayer compositions and articles are also disclosed.
摘要翻译：描述了一种用于增加包含基本上不含衍生自偏二氟乙烯的共聚单元的含氟聚合物的第一层与包含可固化弹性体的第二层的粘合力的方法。该方法包括向可固化弹性体中加入脱氟化氢组合物，使层接触并固化如此形成的层状制品。还公开了所得的多层组合物和制品。

6. 发明授权

US5756588A Scorch safety of curable fluoroelastomer compositions 失效
标题翻译：可固化含氟弹性体组合物的焦烧安全性
公开(公告)号：US5756588A
公开(公告)日：1998-05-26
申请号：US932504
申请日：1997-09-18
申请人： Robert E. Kolb , Naiyong Jing
发明人： Robert E. Kolb , Naiyong Jing
IPC分类号： C08K5/00 , C08K5/13 , C08K5/19 , C08K5/36 , C08K5/50 , C08L27/12 , C08F8/00
CPC分类号： C08K5/0025 , C08K5/13
摘要： This invention provides a curable fluoroelastomer composition comprising: (A) a fluorine-containing polymer or a blend of fluorine-containing polymers each comprising interpolymerized units derived from one or more fluorine-containing ethylenically unsaturated monomers; (B) an aromatic polyhydroxy crosslinking agent; (C) at least one organo-onium compound; and (D) a monohydroxyfunctional phenol. The compositions provide for a method of improving scorch safety of curable fluoroelastomer compositions.
摘要翻译：本发明提供了一种可固化的含氟弹性体组合物，其包含：（A）含氟聚合物或含氟聚合物的共混物，其各自包含衍生自一种或多种含氟烯属不饱和单体的共聚单元; （B）芳族多羟基交联剂; （C）至少一种有机鎓化合物; 和（D）单羟基官能苯酚。该组合物提供了改善可固化的含氟弹性体组合物的焦烧安全性的方法。

7. 发明授权

US4894410A Fluorine-containing polymers with pendent thioorgano groups 失效
标题翻译：含硫基有机基团的含氟聚合物
公开(公告)号：US4894410A
公开(公告)日：1990-01-16
申请号：US165936
申请日：1988-03-09
申请人： Robert E. Kolb , Paul F. Tuckner , Richard A. Guenthner
发明人： Robert E. Kolb , Paul F. Tuckner , Richard A. Guenthner
IPC分类号： C08J3/24 , C08F8/34 , C08F14/18 , C09D127/12
CPC分类号： C08F8/34 , C08F2810/20
摘要： This invention provides fluorine-containing polymers having at least one thioorgano group. These polymers are prepared by reacting a fluoropolymer precursor with one or more, organic, thiolate compounds thereby modifying the fluoropolymer precursor by grafting onto its backbone the thioorgano groups. Said thioorgano groups may contain functional moieties that modify the cure properties, bulk, properties or compatibility of the thioorgano fluoropolymer precursor. This invention also provides shaped or formed cured articles, coatings and solutions comprising the thioorgano fluoropolymers, and blends thereof with other compatible polymers.

8. 发明授权

US4287320A Composition of fluoroelastomer and diorganosulfuroxide 失效
标题翻译：含氟弹性体和二有机硫氧化物的组成
公开(公告)号：US4287320A
公开(公告)日：1981-09-01
申请号：US122513
申请日：1980-02-19
申请人： Robert E. Kolb
发明人： Robert E. Kolb
IPC分类号： C08K5/41 , C08K13/02 , C08F8/34 , C08F8/00
CPC分类号： C08K5/41 , C08K13/02
摘要： A diorgano sulfur oxide is included in a curable vinylidene fluoride elastomer formulation to provide desirable curing characteristics.
摘要翻译：二有机硫氧化物包括在可固化偏二氟乙烯弹性体配方中以提供所需的固化特性。

9. 发明授权

US06803425B2 Fluoropolymers having pendant imidate structures 失效
标题翻译：含有亚氨酸酯侧链结构的含氟聚合物
公开(公告)号：US06803425B2
公开(公告)日：2004-10-12
申请号：US10122487
申请日：2002-04-11
申请人： Klaus Hintzer , Werner M. A. Grootaert , Robert E. Kolb , Franz Maerz , Werner Schwertfeger
发明人： Klaus Hintzer , Werner M. A. Grootaert , Robert E. Kolb , Franz Maerz , Werner Schwertfeger
IPC分类号： C08F814
CPC分类号： C08F16/24 , C08F214/18 , C08F214/262 , C08J5/18
摘要： A composition comprising (a) a fluoropolymer having pendant imidate groups, which imidate groups have the formula: —C═NH(OR) wherein R is a C1-C10 aliphatic group which aliphatic group may have F or Cl substituents; and optionally, (b) a perfluorovinyl ether of the general formula: CF2═CFO(R′fO)a(R″fO)bRf wherein R′f and R″f are the same or are different C1-C6 linear or branched perfluoroalkylene groups; a and b are, independently, 0 or an integer from 1 to 10; and Rf is a C1-C8 perfluoroalkyl group or a C1-C15 perfluoroalkoxy group. Also provided are a method of making a fluoropolymer composition and curable and cured articles comprising a fluoropolymer composition.
摘要翻译：一种组合物，其包含（a）具有亚酰氨基侧基的含氟聚合物，所述亚胺基具有下式：-C = NH（OR），其中R是C1-C10脂族基团，该脂族基团可以具有F或Cl取代基; 和（b）通式CF 2 = CFO（R'fO）a（R“f O）b R f的全氟乙烯基醚，其中R'f和R''f相同或不同，C1-C6直链或支链全氟亚烷基; a和b独立地为0或1〜10的整数; Rf为C1-C8全氟烷基或C1-C15全氟烷氧基。还提供了制备包含含氟聚合物组合物的含氟聚合物组合物和可固化和固化的制品的方法。

10. 发明授权

US06773755B2 Process for preparing a multi-layer article having a fluoroplastic layer and an elastomer layer 失效
标题翻译：制备具有氟塑料层和弹性体层的多层制品的方法
公开(公告)号：US06773755B2
公开(公告)日：2004-08-10
申请号：US09980749
申请日：2001-11-15
申请人： Tatsuo Fukushi , Robert E. Kolb , Craig R. Hoff , Steven J. Wellner , Attila Molnar
发明人： Tatsuo Fukushi , Robert E. Kolb , Craig R. Hoff , Steven J. Wellner , Attila Molnar
IPC分类号： B05D138
CPC分类号： C08J7/047 , B05D1/265 , B05D3/0254 , B05D5/083 , B05D7/02 , B05D7/542 , B29C47/0004 , B29C47/0021 , B29C47/0023 , B29C47/0026 , B29C47/0066 , B29C47/021 , B29C47/025 , B29C47/04 , B29C47/065 , B29C47/28 , B29K2023/16 , B29K2027/16 , B29K2027/18 , B29K2995/0015 , B29L2023/22 , B29L2031/712 , B32B25/08 , C08J2321/00 , C08J2427/00
摘要： A method for enhancing the bond strength between a VDF-containing fluoroplastic layer and an elastomer layer of a multi-layer article. A VDF-containing fluoroplastic composition is applied to the surface of a precursor article that includes a curable elastomer layer to form a fluoroplastic layer. Prior to application of the fluoroplastic composition, the curable elastomer layer is thermally insulated to prevent it from undergoing substantial heating. Following application, the fluoroplastic layer is heated and the curable elastomer layer is cured (e.g., thermally cured). Preferably, the elastomer cure occurs separately from and subsequent to heating the fluoroplastic layer. The combination of thermally insulating the curable elastomer layer prior to application of the fluoroplastic composition and heating the fluoroplastic layer following application of the fluoroplastic composition results in formation of a strong bond between the fluoroplastic and elastomer layers upon cure.
摘要翻译：一种用于增强含VDF的氟塑料层与多层制品的弹性体层之间的结合强度的方法。将含VDF的氟塑料组合物施加到包含可固化弹性体层的前体制品的表面以形成氟塑料层。在施加氟塑料组合物之前，将可固化的弹性体层进行绝热以防止其发生实质的加热。在施加之后，加热氟塑料层并固化可固化的弹性体层（例如热固化）。优选地，弹性体固化与氟塑料层的加热分开并随后发生。在施加氟塑料组合物之前将可固化弹性体层热绝缘并在施加氟塑料组合物之后加热氟塑料层的组合导致在固化后在氟塑料和弹性体层之间形成强结合。

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