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1. 发明授权

US4684697A Compositions based on silane hydrolyzates and vinyl polymers containing hydrolyzable silyl groups 失效
标题翻译：基于硅烷水解物和含有可水解甲硅烷基的乙烯基聚合物的组合物
公开(公告)号：US4684697A
公开(公告)日：1987-08-04
申请号：US881434
申请日：1986-07-02
申请人： Wen-Hsuan Chang , William P. Blackburn , Paul J. Prucnal , Edward L. Dufford
发明人： Wen-Hsuan Chang , William P. Blackburn , Paul J. Prucnal , Edward L. Dufford
IPC分类号： C08G77/06 , C09D4/00 , C08F8/00
CPC分类号： C08G77/06 , C09D4/00
摘要： Disclosed are moisture-curable compositions based on (A) ungelled, partial hydrolyzates or organosilicon-containing materials in combination with (B) acrylic addition interpolymers containing hydrolyzable silyl groups.The organosilicon-containing material for preparation of the ungelled partial hydrolysis product has an average functionality based on easily hydrolyzable Y groups attached to silicon atoms of greater than or equal to 2.4 and contains greater than or equal to 10 mole percent of at least one organosilane compound corresponding to the formula R-Si-Y.sub.3. The partial hydrolysis product is prepared using a controlled amount of water.The acrylic addition interpolymer is not particularly limited provided that it contains at least one silicon atom directly bonded to a hydrolyzable group and is compatible with the ungelled partial hydrolysis product.
摘要翻译：公开了基于（A）未凝胶化，部分水解产物或含有机硅材料与（B）含有可水解甲硅烷基的丙烯酸加成互聚物的组合物的可湿固化组合物。用于制备未凝胶化部分水解产物的含有机硅材料具有基于与硅原子连接的容易水解的Y基团大于或等于2.4的平均官能度，并且含有大于或等于10摩尔％的至少一种有机硅烷化合物对应于式R-Si-Y3。使用受控量的水制备部分水解产物。丙烯酸类加成互聚物没有特别限制，只要其含有至少一个直接键合到可水解基团上的硅原子并与未凝胶化的部分水解产物相容即可。

2. 发明授权

US4678835A Coating composition containing an ungelled reaction product as a curative 失效
标题翻译：含有未凝胶化反应产物作为治疗剂的涂料组合物
公开(公告)号：US4678835A
公开(公告)日：1987-07-07
申请号：US824040
申请日：1986-01-30
申请人： Wen-Hsuan Chang , Edward L. Dufford , J. Alden Erikson , Paul J. Prucnal
发明人： Wen-Hsuan Chang , Edward L. Dufford , J. Alden Erikson , Paul J. Prucnal
IPC分类号： C09D7/12 , C07F7/00 , C08G77/54 , C09D183/04 , C09D183/05 , C09D183/14 , C09D201/02 , C08F8/00
CPC分类号： C08G77/54 , C09D183/14
摘要： A coating composition contains at least 15 percent by weight of an ungelled reaction product of:(i) at least 2 percent by weight of an amine having in a molecule thereof at least one amino hydrogen atom, and at least one silicon atom directly bonded to a hydrolyzable group;(ii) at least 4 percent by weight of a material containing at least one epoxide group, at least 30 percent of said material being essentially free of hydroxyl groups; and(iii) a material selected from vinyl alkoxysilanes; nonfunctional organosilanes; organosilicates; and partial hydrolysis products thereof; the percentages by weight being based on the total weight of the resin solids of the coating composition including (i), (ii) and (iii).
摘要翻译：涂料组合物含有至少15重量％的未凝胶化反应产物：（i）至少2重量％的分子中至少有一个氨基氢原子的胺和至少一个直接连接到可水解基团; （ii）至少4重量％的含有至少一个环氧基团的材料，至少30％的所述材料基本上不含羟基; 和（iii）选自乙烯基烷氧基硅烷的材料; 非功能性有机硅烷; 有机硅酸盐及其部分水解产物; 重量百分比基于包括（i），（ii）和（iii）的涂料组合物的树脂固体的总重量。

3. 发明授权

US4808663A Method of preparing acrylic polymers containing hydrolyzable moieties from organosilane compounds 失效
标题翻译：制备含有有机硅烷化合物的可水解部分的丙烯酸聚合物的方法
公开(公告)号：US4808663A
公开(公告)日：1989-02-28
申请号：US88731
申请日：1987-08-24
申请人： Wen H. Chang , Paul J. Prucnal , John R. Peffer , Edward L. Dufford , Ronald R. Ambrose
发明人： Wen H. Chang , Paul J. Prucnal , John R. Peffer , Edward L. Dufford , Ronald R. Ambrose
IPC分类号： C08F8/42 , C08G77/442 , C09D143/04 , C08F8/00
CPC分类号： C09D143/04 , C08F8/42 , C08G77/442
摘要： Disclosed is an ungelled acrylic resin composition containing an acrylic polymer having in a molecule thereof at least one group containing a silicon atom selected from: ##STR1## each R independently is selected from the group of moieties consisting of Y, hydrogen, a C.sub.1 -C.sub.10 group joined to Si through an Si-C linkage, and OR.sup.7 in which R.sup.7 represents alkykl having at least 4 carbon atoms, aryl, alkylaryl, arylalkyl, aryloxyalkyl, or alkyloxyalkyl, wherein Y represents an easily hydrolyzable group.The acrylic resin composition, contains an amount of easily hydrolyzable Y moieties such that the ratio of the number of grams of the ungelled acrylic resin composition to equivalent of easily hydrolyzable Y moieties in the ungelled acrylic resin composition is in the range of from 40 to 667. Preferred acrylic resin compositions of the invention can be cured in the presence of atmospheric moisture and a suitable catalyst at a temperature of less than or equal to 121 degrees Celsius within 3 hours.Disclosed is a method for producing the ungelled acrylic resin composition.Also disclosed is a nonaqueous composition, particularly a nonaqueous coating composition, containing the ungelled acrylic resin composition. Preferred coating compositions containing an ungelled acrylic resin composition can be cured in the presence of atmospheric moisture and a suitable catalyst at a temperature of less than or equal to 121 degrees C. within 3 hours.
摘要翻译：公开了一种无胶凝的丙烯酸类树脂组合物，其含有丙烯酸类聚合物，其分子中至少含有选自以下的硅原子的基团：每个R独立地选自Y，氢，，通过Si-C键与Si连接的C1-C10基团，其中R7表示具有至少4个碳原子的烷基的OR7，芳基，烷基芳基，芳基烷基，芳氧基烷基或烷氧基烷基，其中Y表示易水解基团。丙烯酸树脂组合物含有一定量的易水解的Y部分，使得未凝胶化丙烯酸树脂组合物的克数与未凝胶化丙烯酸树脂组合物中容易水解的Y部分的当量比例在40至667的范围内本发明优选的丙烯酸树脂组合物可以在大气湿度和合适的催化剂存在下在3小时内在小于或等于121摄氏度的温度下固化。公开了一种制造无凝胶的丙烯酸树脂组合物的方法。还公开了含非凝胶型丙烯酸树脂组合物的非水性组合物，特别是非水性涂料组合物。含有未胶凝的丙烯酸树脂组合物的优选涂料组合物可在大气水分和合适的催化剂存在下在3小时内在小于或等于121℃的温度下固化。

4. 发明授权

US4788107A Substrates coated with nonaqueous compositions comprising acrylic polymers containing hydrolyzable moieties from organosilane compounds 失效
标题翻译：包含非水性组合物的底物，其包含含有来自有机硅烷化合物的可水解部分的丙烯酸聚合物
公开(公告)号：US4788107A
公开(公告)日：1988-11-29
申请号：US88357
申请日：1987-08-24
申请人： Wen H. Chang , Paul J. Prucnal , John R. Peffer , Edward L. Dufford , Ronald R. Ambrose
发明人： Wen H. Chang , Paul J. Prucnal , John R. Peffer , Edward L. Dufford , Ronald R. Ambrose
IPC分类号： C08F8/42 , C08G77/442 , C09D143/04 , B32B9/04
CPC分类号： C09D143/04 , C08F8/42 , C08G77/442 , Y10T428/31663
摘要： Disclosed is an ungelled acrylic resin composition containing an acrylic polymer having in a molecule thereof at least one group containing a silicon atom selected from: ##STR1## wherein each R independently is selected from the group of moieties consisting of Y, hydrogen, a C.sub.1 -C.sub.10 group joined to Si through an Si--C linkage, and OR.sup.7 in which R.sup.7 represents alkyl having at least 4 carbon atoms, aryl, alkylaryl, arylaklyl, aryloxyalkyl, or alkyloxyalkyl, wherein Y represents an easily hydrolyzable group.The acrylic resin composition, contains an amount of easily hydrolyzable Y moieties such that the ratio of the number of grams of the ungelled acrylic resin composition to equivalent of easily hydrolyzable Y moieties in the ungelled acrylic resin composition is in a range of from 40 to 667. Prefered acrylic resin compositions of the invention can be cured in the presence of atmospheric moisture and a suitable catalyst at a temperature of less than or equal to 121 degrees Celsius within 3 hours.Disclosed is a method for producing the ungelled acrylic resin composition.Also disclosed is a nonaqueous composition, particularly a nonaqueous coating composition, containing the ungelled acrylic resin composition. Preferred coating compositions containing an ungelled acrylic resin composition can be cured in the presence of atmospheric moisture and a suitable catalyst at a temperature of less than or equal to 121 degrees C within 3 hours.
摘要翻译：公开了一种含有丙烯酸类聚合物的非凝胶型丙烯酸树脂组合物，其分子内含有至少一个含有选自以下的硅原子的基团：其中每个R独立地选自Y，氢，通过Si-C键与Si连接的C1-C10基团和其中R7表示具有至少4个碳原子的烷基的OR7，芳基，烷基芳基，芳基烷基，芳氧基烷基或烷氧基烷基，其中Y表示易水解基团。丙烯酸树脂组合物含有一定量的易水解的Y部分，使未凝胶化丙烯酸树脂组合物的克数与在非胶凝的丙烯酸树脂组合物中容易水解的Y部分的当量的比例在40至667的范围内本发明优选的丙烯酸树脂组合物可以在大气水分和合适的催化剂存在下在3小时内在小于或等于121摄氏度的温度下固化。公开了一种制造无凝胶的丙烯酸树脂组合物的方法。还公开了含非凝胶型丙烯酸树脂组合物的非水性组合物，特别是非水性涂料组合物。含有无凝胶的丙烯酸树脂组合物的优选涂料组合物可在大气水分和合适的催化剂存在下在3小时内在小于或等于121℃的温度下固化。

5. 发明授权

US4714738A Acrylic polymers containing hydrolyzable moieties from organosilane compounds 失效
标题翻译：含有有机硅烷化合物的可水解部分的丙烯酸聚合物
公开(公告)号：US4714738A
公开(公告)日：1987-12-22
申请号：US728973
申请日：1985-04-30
申请人： Wen H. Chang , Paul J. Prucnal , John R. Peffer , Edward L. Dufford , Ronald R. Ambrose
发明人： Wen H. Chang , Paul J. Prucnal , John R. Peffer , Edward L. Dufford , Ronald R. Ambrose
IPC分类号： C09D133/04 , B32B27/30 , C08F8/42 , C08F30/00 , C08F30/08 , C08G77/442 , C08K5/00 , C08L1/08 , C08L5/08 , C08L29/04 , C08L33/00 , C08L33/04 , C09D143/04 , C08F8/00
CPC分类号： C09D143/04 , C08F8/42 , C08G77/442
摘要： Disclosed is an ungelled acrylic resin composition containing an acrylic polymer having in a molecule thereof at least one group containing a silicon atom selected from: ##STR1## wherein each R independently is selected from the group of moieties consisting of Y, hydrogen, a C.sub.1 -C.sub.10 group joined to Si through an Si-C linkage, and OR.sup.7 in which R.sup.7 represents alkyl having at least 4 carbon atoms, aryl, alkylaryl, arylalkyl, aryloxyalkyl, or alkyloxyalkyl, wherein Y represents an easily hydrolyzable group.The acrylic resin composition, contains an amount of easily hydrolyzable Y moieties such that the ratio of the number of grams of the ungelled acrylic resin composition to equivalent of easily hydrolyzable Y moieties in the ungelled acrylic resin composition is in a range of from 40 to 667. Preferred acrylic resin compositions of the invention can be cured in the presence of atmospheric moisture and a suitable catalyst at a temperature of less than or equal to 121 degrees Celsius within 3 hours.Disclosed is a method for producing the ungelled acrylic resin composition.Also disclosed is a nonaqueous composition, particularly a nonaqueous coating composition, containing the ungelled acrylic resin composition. Preferred coating compositions containing an ungelled acrylic resin composition can be cured in the presence of atmospheric moisture and a suitable catalyst at a temperature of less than or equal to 121 degrees C. within 3 hours.
摘要翻译：公开了一种含有丙烯酸类聚合物的非凝胶型丙烯酸树脂组合物，其分子内含有至少一个含有选自以下的硅原子的基团：其中每个R独立地选自Y，氢，通过Si-C键与Si连接的C1-C10基团，和其中R7表示具有至少4个碳原子的烷基的OR7，芳基，烷芳基，芳烷基，芳氧基烷基或烷氧基烷基，其中Y表示易水解基团。丙烯酸树脂组合物含有一定量的易水解的Y部分，使未凝胶化的丙烯酸树脂组合物的克数与在非胶凝的丙烯酸树脂组合物中容易水解的Y部分的当量的比例在40至667的范围内本发明优选的丙烯酸树脂组合物可以在大气湿度和合适的催化剂存在下在3小时内在小于或等于121摄氏度的温度下固化。公开了一种制造无凝胶的丙烯酸树脂组合物的方法。还公开了含非凝胶型丙烯酸树脂组合物的非水性组合物，特别是非水性涂料组合物。含有未胶凝的丙烯酸树脂组合物的优选涂料组合物可在大气水分和合适的催化剂存在下在3小时内在小于或等于121℃的温度下固化。

6. 发明授权

US3962369A Sealer-primer for elastomeric coatings 失效
标题翻译：用于弹性体涂层的密封底漆
公开(公告)号：US3962369A
公开(公告)日：1976-06-08
申请号：US534405
申请日：1974-12-19
申请人： Wen-Hsuan Chang , Roger L. Scriven , Paul J. Prucnal
发明人： Wen-Hsuan Chang , Roger L. Scriven , Paul J. Prucnal
IPC分类号： C08G18/83 , C09D175/04 , C08L61/20 , C08L61/26
CPC分类号： C08G18/831 , C09D175/04 , Y10T428/2419
摘要： Compositions useful as sealing primers for elastomeric coatings comprise (A) the reaction product of a polyurethane polyol and a polycarboxylic acid or acid anhydride, and (B) an aminoplast resin. When used as primers, the compositions of the instant invention increase the durability, gloss retention and adhesion of elastomeric coatings. Such primers are particularly useful on resilient and rubbery substrates such as EPDM rubber, foam rubber, polyurethane foam and vinyl foam.
摘要翻译：可用作弹性体涂料的密封底漆的组合物包含（A）聚氨酯多元醇与多元羧酸或酸酐的反应产物和（B）氨基塑料树脂。当用作底漆时，本发明的组合物增加了弹性体涂料的耐久性，光泽保持性和粘合性。这种底漆在弹性和橡胶基质如EPDM橡胶，泡沫橡胶，聚氨酯泡沫和乙烯基泡沫塑料上特别有用。

7. 发明授权

US4018849A Polyurethane polyol compositions modified with an alkylenimine 失效
标题翻译：用亚烷基亚胺改性的聚氨酯多元醇组合物
公开(公告)号：US4018849A
公开(公告)日：1977-04-19
申请号：US602856
申请日：1975-08-07
申请人： Wen-Hsuan Chang , Roger L. Scriven , Paul J. Prucnal
发明人： Wen-Hsuan Chang , Roger L. Scriven , Paul J. Prucnal
IPC分类号： C08G18/83 , C09D175/04 , C08L61/24 , C08L61/28
CPC分类号： C08G18/833 , C09D175/04
摘要： Compositions useful as coating compositions comprise the reaction product of a polyurethane polyol which contains acidic carboxyl groups with an alkylenimine. Particularly desirable coatings are produced by further combining the imine-modified polyurethane polyols with aminoplast resins. The compositions are characterized by improved pigment wetting properties and provide coatings having improved low temperature, flexibility and increased adhesion.
摘要翻译：可用作涂料组合物的组合物包含含有酸性羧基的亚氨基亚胺的聚氨酯多元醇的反应产物。通过将亚胺改性的聚氨酯多元醇与氨基塑料树脂进一步组合来生产特别理想的涂层。组合物的特征在于改善颜料润湿性能并提供具有改进的低温，柔韧性和增加的粘附性的涂层。

8. 发明授权

US06479588B1 Graft copolymer of polyamide and a glycidyl group-containing acrylate copolymer, process for preparation and coating composition containing the graft copolymer 失效
标题翻译：聚酰胺与含缩水甘油基丙烯酸酯共聚物的接枝共聚物，含有接枝共聚物的制备方法和涂料组合物
公开(公告)号：US06479588B1
公开(公告)日：2002-11-12
申请号：US09641760
申请日：2000-08-21
申请人： Szu-Ping Lu , Paul J. Prucnal , Hiram A. Norton
发明人： Szu-Ping Lu , Paul J. Prucnal , Hiram A. Norton
IPC分类号： C08F800
CPC分类号： C08F283/04 , C08F220/32
摘要： A graft copolymer comprising a polyamide to which is grafted a glycidyl group-containing acrylate copolymer. The graft copolymer can be prepared by dispersing in an organic solvent a polyamide and a material which will react with the polyamide to form the graft copolymer of the polyamide and the acrylate copolymer and reacting the polyamide and the material so as to form said graft copolymer. The graft copolymer can exhibit improved toughness and reduced friability and can be used to form molded articles and in coating compositions, especially powder coating compositions. The coatings can exhibit transparency, reduced brittleness and increased chip resistance. The powder coatings can further exhibit high gloss and smoothness due to superior flow characteristics thereby enabling thinner coatings to be used that provide acceptable appearance.
摘要翻译：包含接枝有含缩水甘油基的丙烯酸酯共聚物的聚酰胺的接枝共聚物。接枝共聚物可以通过在有机溶剂中分散聚酰胺和与聚酰胺反应形成聚酰胺和丙烯酸酯共聚物的接枝共聚物并与聚酰胺和材料反应以形成所述接枝共聚物的材料来制备。接枝共聚物可以显示出改进的韧性和脆性降低，并且可以用于形成模制品和涂料组合物，特别是粉末涂料组合物。涂层可以显示透明度，降低的脆性和增加的芯片电阻。由于优异的流动特性，粉末涂料可以进一步表现出高的光泽度和光滑度，从而可以使用提供可接受的外观的更薄的涂层。

9. 发明授权

US4065624A Radiation curable coating composition 失效
标题翻译：可辐射固化涂料组合物
公开(公告)号：US4065624A
公开(公告)日：1977-12-27
申请号：US652687
申请日：1976-01-27
申请人： Paul J. Prucnal , Robert DeMajistre
发明人： Paul J. Prucnal , Robert DeMajistre
IPC分类号： C08F2/50 , C08F299/02 , C09D4/00 , C08F4/00 , C08F20/22 , C08F20/28
CPC分类号： C08F299/026 , C09D4/00 , Y10T428/31935
摘要： 3-Halo-2-hydroxypropyl acrylates and methacrylates and 2-halo-1-(hydroxymethyl)ethyl acrylates and methacrylates are used as reactive solvent for an acrylic or methacrylic terminated polyether resin in radiation curable coating compositions.
摘要翻译： 3-卤代-2-羟丙基丙烯酸酯和甲基丙烯酸酯和2-卤代-1-（羟甲基）乙基丙烯酸酯和甲基丙烯酸酯用作可辐射固化涂料组合物中丙烯酸或甲基丙烯酸封端的聚醚树脂的反应性溶剂。

10. 发明授权

US5744522A Low gloss coating compositions 失效
标题翻译：低光泽涂料组合物
公开(公告)号：US5744522A
公开(公告)日：1998-04-28
申请号：US713517
申请日：1996-09-13
申请人： Paul J. Prucnal , Szu-Ping Lu
发明人： Paul J. Prucnal , Szu-Ping Lu
IPC分类号： C08G59/58 , C08F220/26 , C08G59/42 , C08L67/02 , C08L75/00 , C09D5/00 , C09D133/06 , C09D133/14 , C09D163/00 , C09D167/00 , C09D167/02 , C08L63/00 , C08F20/00
CPC分类号： C09D133/068 , C08G59/4238 , C09D167/02 , C08L67/02 , C08L75/00
摘要： A low gloss coating composition having a 60.degree. gloss of less than about 60 which contains: a) a glycidyl group-containing acrylic copolymer; b) an aromatic polyester; and c) an isocyanurate curing agent having the formula: ##STR1## wherein R.sub.1 -R.sub.3 are independently selected from the group consisting of divalent alkylene groups of 1 to 18 carbon atoms and divalent groups of 3 to 21 carbon atoms and containing an ester linkage, and R.sub.4 -R.sub.6 are independently selected from the group consisting of H, organic salt groups, alkyl groups of 1 to 20 carbon atoms and C(O)R.sub.7 wherein R.sub.7 is an alkyl group of 1 to 22 carbon atoms.
摘要翻译：具有小于约60°的60°光泽度的低光泽涂料组合物，其含有：a）含缩水甘油基的丙烯酸共聚物; b）芳族聚酯; 和c）具有下式的异氰脲酸酯固化剂：其中R 1 -R 3独立地选自1至18个碳原子的二价亚烷基和3至21个碳原子的二价基团并含有酯键，和R 4 -R 6独立地选自H，有机盐基团，1-20个碳原子的烷基和C（O）R 7，其中R 7是1至22个碳原子的烷基。

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