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1. 发明授权

US4808663A Method of preparing acrylic polymers containing hydrolyzable moieties from organosilane compounds 失效
标题翻译：制备含有有机硅烷化合物的可水解部分的丙烯酸聚合物的方法
公开(公告)号：US4808663A
公开(公告)日：1989-02-28
申请号：US88731
申请日：1987-08-24
申请人： Wen H. Chang , Paul J. Prucnal , John R. Peffer , Edward L. Dufford , Ronald R. Ambrose
发明人： Wen H. Chang , Paul J. Prucnal , John R. Peffer , Edward L. Dufford , Ronald R. Ambrose
IPC分类号： C08F8/42 , C08G77/442 , C09D143/04 , C08F8/00
CPC分类号： C09D143/04 , C08F8/42 , C08G77/442
摘要： Disclosed is an ungelled acrylic resin composition containing an acrylic polymer having in a molecule thereof at least one group containing a silicon atom selected from: ##STR1## each R independently is selected from the group of moieties consisting of Y, hydrogen, a C.sub.1 -C.sub.10 group joined to Si through an Si-C linkage, and OR.sup.7 in which R.sup.7 represents alkykl having at least 4 carbon atoms, aryl, alkylaryl, arylalkyl, aryloxyalkyl, or alkyloxyalkyl, wherein Y represents an easily hydrolyzable group.The acrylic resin composition, contains an amount of easily hydrolyzable Y moieties such that the ratio of the number of grams of the ungelled acrylic resin composition to equivalent of easily hydrolyzable Y moieties in the ungelled acrylic resin composition is in the range of from 40 to 667. Preferred acrylic resin compositions of the invention can be cured in the presence of atmospheric moisture and a suitable catalyst at a temperature of less than or equal to 121 degrees Celsius within 3 hours.Disclosed is a method for producing the ungelled acrylic resin composition.Also disclosed is a nonaqueous composition, particularly a nonaqueous coating composition, containing the ungelled acrylic resin composition. Preferred coating compositions containing an ungelled acrylic resin composition can be cured in the presence of atmospheric moisture and a suitable catalyst at a temperature of less than or equal to 121 degrees C. within 3 hours.
摘要翻译：公开了一种无胶凝的丙烯酸类树脂组合物，其含有丙烯酸类聚合物，其分子中至少含有选自以下的硅原子的基团：每个R独立地选自Y，氢，，通过Si-C键与Si连接的C1-C10基团，其中R7表示具有至少4个碳原子的烷基的OR7，芳基，烷基芳基，芳基烷基，芳氧基烷基或烷氧基烷基，其中Y表示易水解基团。丙烯酸树脂组合物含有一定量的易水解的Y部分，使得未凝胶化丙烯酸树脂组合物的克数与未凝胶化丙烯酸树脂组合物中容易水解的Y部分的当量比例在40至667的范围内本发明优选的丙烯酸树脂组合物可以在大气湿度和合适的催化剂存在下在3小时内在小于或等于121摄氏度的温度下固化。公开了一种制造无凝胶的丙烯酸树脂组合物的方法。还公开了含非凝胶型丙烯酸树脂组合物的非水性组合物，特别是非水性涂料组合物。含有未胶凝的丙烯酸树脂组合物的优选涂料组合物可在大气水分和合适的催化剂存在下在3小时内在小于或等于121℃的温度下固化。

2. 发明授权

US4788107A Substrates coated with nonaqueous compositions comprising acrylic polymers containing hydrolyzable moieties from organosilane compounds 失效
标题翻译：包含非水性组合物的底物，其包含含有来自有机硅烷化合物的可水解部分的丙烯酸聚合物
公开(公告)号：US4788107A
公开(公告)日：1988-11-29
申请号：US88357
申请日：1987-08-24
申请人： Wen H. Chang , Paul J. Prucnal , John R. Peffer , Edward L. Dufford , Ronald R. Ambrose
发明人： Wen H. Chang , Paul J. Prucnal , John R. Peffer , Edward L. Dufford , Ronald R. Ambrose
IPC分类号： C08F8/42 , C08G77/442 , C09D143/04 , B32B9/04
CPC分类号： C09D143/04 , C08F8/42 , C08G77/442 , Y10T428/31663
摘要： Disclosed is an ungelled acrylic resin composition containing an acrylic polymer having in a molecule thereof at least one group containing a silicon atom selected from: ##STR1## wherein each R independently is selected from the group of moieties consisting of Y, hydrogen, a C.sub.1 -C.sub.10 group joined to Si through an Si--C linkage, and OR.sup.7 in which R.sup.7 represents alkyl having at least 4 carbon atoms, aryl, alkylaryl, arylaklyl, aryloxyalkyl, or alkyloxyalkyl, wherein Y represents an easily hydrolyzable group.The acrylic resin composition, contains an amount of easily hydrolyzable Y moieties such that the ratio of the number of grams of the ungelled acrylic resin composition to equivalent of easily hydrolyzable Y moieties in the ungelled acrylic resin composition is in a range of from 40 to 667. Prefered acrylic resin compositions of the invention can be cured in the presence of atmospheric moisture and a suitable catalyst at a temperature of less than or equal to 121 degrees Celsius within 3 hours.Disclosed is a method for producing the ungelled acrylic resin composition.Also disclosed is a nonaqueous composition, particularly a nonaqueous coating composition, containing the ungelled acrylic resin composition. Preferred coating compositions containing an ungelled acrylic resin composition can be cured in the presence of atmospheric moisture and a suitable catalyst at a temperature of less than or equal to 121 degrees C within 3 hours.
摘要翻译：公开了一种含有丙烯酸类聚合物的非凝胶型丙烯酸树脂组合物，其分子内含有至少一个含有选自以下的硅原子的基团：其中每个R独立地选自Y，氢，通过Si-C键与Si连接的C1-C10基团和其中R7表示具有至少4个碳原子的烷基的OR7，芳基，烷基芳基，芳基烷基，芳氧基烷基或烷氧基烷基，其中Y表示易水解基团。丙烯酸树脂组合物含有一定量的易水解的Y部分，使未凝胶化丙烯酸树脂组合物的克数与在非胶凝的丙烯酸树脂组合物中容易水解的Y部分的当量的比例在40至667的范围内本发明优选的丙烯酸树脂组合物可以在大气水分和合适的催化剂存在下在3小时内在小于或等于121摄氏度的温度下固化。公开了一种制造无凝胶的丙烯酸树脂组合物的方法。还公开了含非凝胶型丙烯酸树脂组合物的非水性组合物，特别是非水性涂料组合物。含有无凝胶的丙烯酸树脂组合物的优选涂料组合物可在大气水分和合适的催化剂存在下在3小时内在小于或等于121℃的温度下固化。

3. 发明授权

US4714738A Acrylic polymers containing hydrolyzable moieties from organosilane compounds 失效
标题翻译：含有有机硅烷化合物的可水解部分的丙烯酸聚合物
公开(公告)号：US4714738A
公开(公告)日：1987-12-22
申请号：US728973
申请日：1985-04-30
申请人： Wen H. Chang , Paul J. Prucnal , John R. Peffer , Edward L. Dufford , Ronald R. Ambrose
发明人： Wen H. Chang , Paul J. Prucnal , John R. Peffer , Edward L. Dufford , Ronald R. Ambrose
IPC分类号： C09D133/04 , B32B27/30 , C08F8/42 , C08F30/00 , C08F30/08 , C08G77/442 , C08K5/00 , C08L1/08 , C08L5/08 , C08L29/04 , C08L33/00 , C08L33/04 , C09D143/04 , C08F8/00
CPC分类号： C09D143/04 , C08F8/42 , C08G77/442
摘要： Disclosed is an ungelled acrylic resin composition containing an acrylic polymer having in a molecule thereof at least one group containing a silicon atom selected from: ##STR1## wherein each R independently is selected from the group of moieties consisting of Y, hydrogen, a C.sub.1 -C.sub.10 group joined to Si through an Si-C linkage, and OR.sup.7 in which R.sup.7 represents alkyl having at least 4 carbon atoms, aryl, alkylaryl, arylalkyl, aryloxyalkyl, or alkyloxyalkyl, wherein Y represents an easily hydrolyzable group.The acrylic resin composition, contains an amount of easily hydrolyzable Y moieties such that the ratio of the number of grams of the ungelled acrylic resin composition to equivalent of easily hydrolyzable Y moieties in the ungelled acrylic resin composition is in a range of from 40 to 667. Preferred acrylic resin compositions of the invention can be cured in the presence of atmospheric moisture and a suitable catalyst at a temperature of less than or equal to 121 degrees Celsius within 3 hours.Disclosed is a method for producing the ungelled acrylic resin composition.Also disclosed is a nonaqueous composition, particularly a nonaqueous coating composition, containing the ungelled acrylic resin composition. Preferred coating compositions containing an ungelled acrylic resin composition can be cured in the presence of atmospheric moisture and a suitable catalyst at a temperature of less than or equal to 121 degrees C. within 3 hours.
摘要翻译：公开了一种含有丙烯酸类聚合物的非凝胶型丙烯酸树脂组合物，其分子内含有至少一个含有选自以下的硅原子的基团：其中每个R独立地选自Y，氢，通过Si-C键与Si连接的C1-C10基团，和其中R7表示具有至少4个碳原子的烷基的OR7，芳基，烷芳基，芳烷基，芳氧基烷基或烷氧基烷基，其中Y表示易水解基团。丙烯酸树脂组合物含有一定量的易水解的Y部分，使未凝胶化的丙烯酸树脂组合物的克数与在非胶凝的丙烯酸树脂组合物中容易水解的Y部分的当量的比例在40至667的范围内本发明优选的丙烯酸树脂组合物可以在大气湿度和合适的催化剂存在下在3小时内在小于或等于121摄氏度的温度下固化。公开了一种制造无凝胶的丙烯酸树脂组合物的方法。还公开了含非凝胶型丙烯酸树脂组合物的非水性组合物，特别是非水性涂料组合物。含有未胶凝的丙烯酸树脂组合物的优选涂料组合物可在大气水分和合适的催化剂存在下在3小时内在小于或等于121℃的温度下固化。

4. 发明授权

US4543405A High solids polyurethane polyols and coating compositions thereof 失效
标题翻译：高固含量聚氨酯多元醇及其涂料组合物
公开(公告)号：US4543405A
公开(公告)日：1985-09-24
申请号：US656559
申请日：1984-10-01
申请人： Ronald R. Ambrose , Wen-Hsuan Chang , David T. McKeough , John R. Peffer
发明人： Ronald R. Ambrose , Wen-Hsuan Chang , David T. McKeough , John R. Peffer
IPC分类号： C08G18/10 , C08G18/32 , C08G18/38 , C08G18/42 , C08G18/46 , C09D175/04
CPC分类号： C08G18/10 , C08G18/3206 , C08G18/3212 , C08G18/3831 , C08G18/423 , C08G18/4615 , C09D175/04
摘要： There are disclosed herein polyurethane polyols and coating compositions formulated therewith. The polyurethane polyols are prepared by typically reacting low molecular weight polyols in amounts sufficient to produce reaction products containing a significant amount of unreacted starting polyols which can be subsequently removed by means such as vacuum distillation.
摘要翻译：本文公开了用其配制的聚氨酯多元醇和涂料组合物。聚氨酯多元醇通过使低分子量多元醇的量通常反应来制备，其量足以产生含有大量未反应的起始多元醇的反应产物，其随后可通过诸如真空蒸馏的方法除去。

5. 发明授权

US4605724A High solids lactone-polyester polyols and coating compositions thereof 失效
标题翻译：高固含量的内酯 - 聚酯多元醇及其涂料组合物
公开(公告)号：US4605724A
公开(公告)日：1986-08-12
申请号：US656555
申请日：1984-10-01
申请人： Ronald R. Ambrose , Wen-Hsuan Chang , David T. McKeough , John R. Peffer
发明人： Ronald R. Ambrose , Wen-Hsuan Chang , David T. McKeough , John R. Peffer
IPC分类号： C08G18/42 , C08G63/60 , C08G18/32
CPC分类号： C08G18/4269 , C08G63/60
摘要： There are disclosed herein lactone-polyester polyols which are derived from lactones, resinous polyols thereof, and coating compositions formulated therewith. The polyester polyols are typically prepared by reacting a large excess of low molecular weight polyols with lactones or functional equivalents thereof. The polyols are employed in amounts sufficient to produce reaction products containing a significant amount of unreacted polyols which can be subsequently removed by means such as vacuum distillation.
摘要翻译：本文公开了衍生自内酯的内酯 - 聚酯多元醇，其树脂多元醇和与其配制的涂料组合物。聚酯多元醇通常通过使大量过量的低分子量多元醇与内酯或其功能等同物反应来制备。多元醇的用量足以产生含有大量未反应的多元醇的反应产物，其随后可通过诸如真空蒸馏的方法除去。

6. 发明授权

US4540771A High solids polyester polyols and resinous polyols thereof 失效
标题翻译：高固体聚酯多元醇及其树脂多元醇
公开(公告)号：US4540771A
公开(公告)日：1985-09-10
申请号：US656562
申请日：1984-10-01
申请人： Ronald R. Ambrose , Wen-Hsuan Chang , David T. McKeough , John R. Peffer
发明人： Ronald R. Ambrose , Wen-Hsuan Chang , David T. McKeough , John R. Peffer
IPC分类号： C08G18/42 , C08G63/18 , C08G63/02
CPC分类号： C08G63/18 , C08G18/42 , C08G18/4211 , C08G18/423 , C08G18/4291
摘要： There are disclosed herein polyester polyols, resinous polyols thereof, and coating compositions formulated therewith. The polyester polyols are prepared by typically reacting a large excess of low molecular weight polyols with polycarboxylic acid or functional equivalents thereof. The polyols are employed in amounts sufficient to produce reaction products containing a significant amount of unreacted polyols which can be subsequently removed by means such as vacuum distillation.
摘要翻译：在此公开了聚酯多元醇，其树脂多元醇和与其配制的涂料组合物。聚酯多元醇通过使大量过量的低分子量多元醇与多元羧酸或其功能等同物反应而典型地反应来制备。多元醇的用量足以产生含有大量未反应的多元醇的反应产物，其随后可通过诸如真空蒸馏的方法除去。

7. 发明授权

US4622369A Urethane resins containing hydrolyzable moieties from organosilane compounds 失效
标题翻译：含有有机硅烷化合物的可水解部分的聚氨酯树脂
公开(公告)号：US4622369A
公开(公告)日：1986-11-11
申请号：US728967
申请日：1985-04-30
申请人： Wen H. Chang , David T. McKeough , Ronald R. Ambrose
发明人： Wen H. Chang , David T. McKeough , Ronald R. Ambrose
IPC分类号： C08G18/00 , C08G18/83 , C08K5/54 , C08L75/00 , C08L75/04 , C09D175/00 , C09D175/04 , C08F20/00
CPC分类号： C08G18/837
摘要： Disclosed is an ungelled urethane resin composition containing a urethane compound having in a molecule thereof at least one group containing a silicon atom selected from: ##STR1## wherein Q represents the residue from a urethane polyol; eachR which may be the same or different, represents hydrogen or a C.sub.1 -C.sub.10 group joined to Si through an Si-C linkage; andY represents an easily hydrolyzable group.The urethane resin composition contains an amount of easily hydrolyzable Y moieties such that the ratio of the number of grams of the ungelled urethane resin composition to equivalents of easily hydrolyzable Y moieties in the ungelled urethane resin composition is in a range of from 40 to 667. Preferred urethane resin compositions can be cured in the presence of atmospheric moisture and a suitable catalyst at a temperature of less than or equal to 121 degrees Celsius within 3 hours.Disclosed is a method for producing the ungelled urethane resin composition.Also disclosed is a nonaqueous composition, particularly a nonaqueous coating composition, containing an ungelled urethane resin composition. Preferred coating compositions containing an ungelled urethane resin composition can be cured in the presence of atmospheric moisture and a suitable catalyst at a temperature of less than or equal to 121 degrees Celsius.
摘要翻译：本发明公开了一种非凝胶型聚氨酯树脂组合物，其含有在分子中具有至少一个含有选自以下的硅原子的氨基甲酸酯化合物：其中Q表示氨基甲酸酯多元醇的残基; 每个R可以相同或不同，表示氢或通过Si-C键与Si连接的C1-C10基团; Y代表易水解基团。聚氨酯树脂组合物含有一定量的易水解的Y部分，使非凝胶聚氨酯树脂组合物的克数与易凝胶化聚氨酯树脂组合物中容易水解的Y部分的当量之比在40至667的范围内。优选的聚氨酯树脂组合物可在大气水分和合适的催化剂存在下在3小时内在小于或等于121℃的温度下固化。公开了非凝胶化聚氨酯树脂组合物的制造方法。还公开了含有非凝胶化聚氨酯树脂组合物的非水性组合物，特别是非水性涂料组合物。含有未胶凝的聚氨酯树脂组合物的优选涂料组合物可在大气湿度和合适的催化剂存在下在小于或等于121摄氏度的温度下固化。

8. 发明授权

US08461253B2 One-component, ambient curable waterborne coating compositions, related methods and coated substrates 有权
标题翻译：单组分环境可固化水性涂料组合物，相关方法和涂覆的基材
公开(公告)号：US08461253B2
公开(公告)日：2013-06-11
申请号：US12688393
申请日：2010-01-15
申请人： Ronald R. Ambrose , Mark S. Gaston , Brian K. Rearick , Irina G. Schwendeman , Venkateshwarlu Kalsani , Hongying Zhou , Michael J. Ziegler
发明人： Ronald R. Ambrose , Mark S. Gaston , Brian K. Rearick , Irina G. Schwendeman , Venkateshwarlu Kalsani , Hongying Zhou , Michael J. Ziegler
IPC分类号： C08F220/18 , C08F220/28 , C09D133/06 , C09D133/14
CPC分类号： C08F220/18 , C08F220/36 , C08F220/58 , C08K5/25 , C09D125/14 , Y10T428/31681 , Y10T428/31692 , Y10T428/31794 , Y10T428/31855
摘要： Disclosed are coating compositions that can be one-component, ambient curable, and waterborne. The coating compositions comprise acrylic copolymer resin particles comprising carbonyl functional groups and a crosslinking agent comprising functional groups, such as hydrazide groups, that are reactive with carbonyl groups.
摘要翻译：公开了可以是单组分，环境可固化和水性的涂料组合物。涂料组合物包含含有羰基官能团的丙烯酸共聚物树脂颗粒和包含与羰基反应的官能团如酰肼基团的交联剂。

9. 发明申请

US20110177352A1 ONE-COMPONENT, AMBIENT CURABLE WATERBORNE COATING COMPOSITIONS, RELATED METHODS AND COATED SUBSTRATES 有权
标题翻译：单组分，环氧固化水性涂料组合物，相关方法和涂层基材
公开(公告)号：US20110177352A1
公开(公告)日：2011-07-21
申请号：US12688393
申请日：2010-01-15
申请人： Ronald R. Ambrose , Mark S. Gaston , Brian K. Rearick , Irina G. Schwendeman , Venkateshwarlu Kalsani , Hongying Zhou , Michael J. Ziegler
发明人： Ronald R. Ambrose , Mark S. Gaston , Brian K. Rearick , Irina G. Schwendeman , Venkateshwarlu Kalsani , Hongying Zhou , Michael J. Ziegler
IPC分类号： A61K8/72 , B32B15/09 , B05D3/10 , B32B27/08
CPC分类号： C08F220/18 , C08F220/36 , C08F220/58 , C08K5/25 , C09D125/14 , Y10T428/31681 , Y10T428/31692 , Y10T428/31794 , Y10T428/31855
摘要： Disclosed are coating compositions that can be one-component, ambient curable, and waterborne. The coating compositions comprise acrylic copolymer resin particles comprising carbonyl functional groups and a crosslinking agent comprising functional groups, such as hydrazide groups, that are reactive with carbonyl groups.
摘要翻译：公开了可以是单组分，环境可固化和水性的涂料组合物。涂料组合物包含含有羰基官能团的丙烯酸共聚物树脂颗粒和包含与羰基反应的官能团如酰肼基团的交联剂。

10. 发明授权

US07981515B2 Bis epoxy polyesters and food cans coated with a composition comprising same 有权
标题翻译：双环氧聚酯和涂有包含其的组合物的食品罐
公开(公告)号：US07981515B2
公开(公告)日：2011-07-19
申请号：US11442866
申请日：2006-05-30
申请人： Ronald R. Ambrose , Ken W. Niederst , John M. Dudik , Mary Ann M. Fuhry
发明人： Ronald R. Ambrose , Ken W. Niederst , John M. Dudik , Mary Ann M. Fuhry
IPC分类号： B32B15/08 , C08G59/16 , C08G63/06 , C08L63/00 , C08L63/10 , C08L67/04
CPC分类号： C08G59/182 , C08G63/42 , C08G63/668 , C09D167/00 , Y10T428/13 , Y10T428/31529 , Y10T428/31681 , Y10T428/31786
摘要： Polyesters comprising the reaction product of a polyol and a bis-epoxy reacted with a mono- and/or di-phenolic carboxylic acid and/or ester are disclosed. Food cans coated at least in part on the interior with a composition comprising these polyesters are also disclosed. The composition used on the food cans is substantially free of BPA and BPF and substantially free of BADGE and BFDGE. Food cans coated at least in part on the interior with a composition comprising a polyester having a loss of molecular weight of less than 50% in an acidic medium are also disclosed.
摘要翻译：公开了包含与单 - 和/或二 - 酚羧酸和/或酯反应的多元醇和双环氧化物的反应产物的聚酯。还公开了至少部分地涂覆在内部的包含这些聚酯的组合物的食品罐。用于食品罐的组合物基本上不含BPA和BPF，并且基本上不含BADGE和BFDGE。还公开了至少部分地在内部涂覆有在酸性介质中包含分子量小于50％的聚酯的组合物的食品罐。

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