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1. 发明授权

US4267317A Process for producing phenoxyalkene derivative 失效
标题翻译：苯氧基衍生物的制备方法
公开(公告)号：US4267317A
公开(公告)日：1981-05-12
申请号：US84161
申请日：1979-10-12
申请人： Wataro Koike , Tadashi Sasuga , Chihiro Yazawa
发明人： Wataro Koike , Tadashi Sasuga , Chihiro Yazawa
IPC分类号： A01N39/02 , A01N43/40 , C07C43/23 , C07C43/29 , C07C43/295 , C07C59/58 , C07C59/68 , C07C69/712 , C07C69/736 , C07C233/02 , C07C235/02 , C07C255/53 , C07C327/22 , C07D213/63 , C07D213/64 , C07D213/643 , C07C69/76 , C07C59/48 , C07C69/767
CPC分类号： C07D213/643 , C07C327/00 , C07C43/23 , C07C59/68
摘要： A phenoxyalkene derivative having the formula ##STR1## wherein R represents a hydrogen atom, ##STR2## and Y and Z are the same or different and respectively represent a hydrogen atom, trifluoromethyl group, a halogen atom, a lower alkyl group, nitro group or cyano group; R.sub.1 represents a hydrogen atom or a lower alkyl group and R.sub.2 represents carboxyl, hydroxymethyl, allyloxycarbonyl, a lower alkoxycarbonyl, a lower haloalkoxycarbonyl, a S-lower alkylthiocarbonyl, carbamoyl, a N-lower alkylcarbamoyl or a N-phenylcarbamoyl group is produced by reacting a phenol compound having the formula ##STR3## with a dihalogen compound having the formula ##STR4## wherein R, R.sub.1 and R.sub.2 are defined above and X.sub.1 represents a halogen atom and X.sub.2 and X.sub.3 are different and respectively represent a hydrogen atom or a halogen atom, by a simultaneous reaction of an etherification and an unsaturated double bond formation, in the presence of a dehydrogenhalide agent and a polar solvent or a combination of a nonpolar solvent and a quaternary ammonium salt or a quaternary phosphonium salt.
摘要翻译：具有下式的苯氧基烯衍生物（III）其中R表示氢原子，Y和Z和Y和Z相同或不同，分别表示氢原子，三氟甲基，卤素原子，低级烷基，硝基或氰基; R1表示氢原子或低级烷基，R2表示羧基，羟甲基，烯丙氧基羰基，低级烷氧基羰基，低级卤代烷氧基羰基，S-低级烷硫基羰基，氨基甲酰基，N-低级烷基氨基甲酰基或N-苯基氨基甲酰基，具有式（I）的酚化合物与具有式“IMAGE”的二卤素化合物，其中R，R 1和R 2如上所定义，X 1表示卤素原子，X 2和X 3分别表示氢原子或卤素原子，通过醚化和不饱和双键形成的同时反应，在脱卤化物剂和极性溶剂或非极性溶剂和季铵盐或季鏻盐的组合的存在下进行。

2. 发明授权

US4254262A Process for producing phenoxycarboxylic acid derivative 失效
标题翻译：生产苯氧基羧酸衍生物的方法
公开(公告)号：US4254262A
公开(公告)日：1981-03-03
申请号：US84164
申请日：1979-10-12
申请人： Wataro Koike , Tadashi Sasuga , Chihiro Yazawa
发明人： Wataro Koike , Tadashi Sasuga , Chihiro Yazawa
IPC分类号： C07C69/66 , A01N37/10 , B01J31/00 , C07B61/00 , C07C51/00 , C07C51/367 , C07C59/125 , C07C59/60 , C07C59/68 , C07C59/70 , C07C67/00 , C07C69/612 , C07C201/00 , C07C205/38 , C07C253/00 , C07C255/54 , C07D213/57 , C07C61/08 , C07C69/767
CPC分类号： C07C51/367
摘要： A phenoxycarboxylic acid derivative having the formula ##STR1## wherein R represents ##STR2## and X.sub.1 represents a hydrogen atom, a halogen atom, a lower alkyl group, trifluoromethyl group, nitro group or cyano group and X.sub.2 represents a hydrogen atom, a halogen atom, a lower alkyl group, nitro group or cyano group, R' represents ##STR3## and R.sub.1 and R.sub.2 are the same and different and respectively represent hydrogen atom or a lower alkyl group, is produced by reacting a phenol compound having the formula ##STR4## with a halogen compound havingX--R'wherein X represents a halogen atom in the presence of a base. The reaction is carried out in the presence of a quarternary ammonium salt or a quaternary phosphonium salt in a nonpolar solvent.
摘要翻译：具有下式的式（III）的苯氧基羧酸衍生物，其中R表示“IMA”，X 1表示氢原子，卤素原子，低级烷基，三氟甲基，硝基或氰基，X 2表示氢原子，卤素原子，低级烷基，硝基或氰基，R'表示“IMA”，R1和R2相同且不同，分别表示氢原子或低级烷基，是通过使苯酚具有式（I）的化合物与具有XR'的卤素化合物反应，其中X表示卤素原子。反应在非极性溶剂中在季铵盐或季鏻盐存在下进行。

3. 发明授权

US4246425A 4-Chloro-3,5-diaminophenyl acetates and curing agent 失效
标题翻译： 4-氯-3,5-二氨基苯基乙酸酯和固化剂
公开(公告)号：US4246425A
公开(公告)日：1981-01-20
申请号：US18613
申请日：1979-03-08
申请人： Wataro Koike , Masami Takayama , Hideaki Ohashi , Chihiro Yazawa
发明人： Wataro Koike , Masami Takayama , Hideaki Ohashi , Chihiro Yazawa
IPC分类号： C08G18/00 , C07C67/00 , C07C227/00 , C07C229/42 , C08G18/10 , C08G18/38 , C08G18/65 , C07C101/44 , C08G18/32
CPC分类号： C08G18/3821 , C08G18/10
摘要： 4-Chloro-3,5-diaminophenyl acetates having the formula ##STR1## wherein R represents an alkyl group are useful as curing agent for polyurethane elastomer and intermediates for pharmaceutical and agrochemical compounds and are produced by simultaneously nitrating hydrolyzing 4-chlorobenzylcyanide and esterifying the resulting 4-chloro-3,5-dinitrophenyl acetic acid and then reducing the resulting ester.
摘要翻译：具有式的4-氯-3,5-二氨基苯基乙酸酯其中R表示烷基可用作聚氨酯弹性体的固化剂和药物和农药化合物的中间体，并且通过同时硝化水解4-氯苄基氰并酯化得到4-氯-3,5-二硝基苯基乙酸，然后还原所得的酯。

4. 发明授权

US4195037A 4-Alkoxy-3,5-diamino-.alpha.,.alpha.,.alpha.-trifluoromethyl-benzene and manufacture thereof and hardener for polyurethane elastomer thereof 失效
标题翻译： 4-烷氧基-3,5-二氨基-α，α，α-三氟甲基苯及其制备方法及其聚氨酯弹性体的固化剂
公开(公告)号：US4195037A
公开(公告)日：1980-03-25
申请号：US948348
申请日：1978-10-04
申请人： Takao Harada , Nobuhide Wada , Hideaki Ohashi , Wataro Koike , Chihiro Yazawa
发明人： Takao Harada , Nobuhide Wada , Hideaki Ohashi , Wataro Koike , Chihiro Yazawa
IPC分类号： C08G18/00 , C07C67/00 , C07C213/00 , C07C217/84 , C08G18/10 , C08G18/38 , C08G18/65 , C07C93/08
CPC分类号： C08G18/3814 , C08G18/10
摘要： 4-Alkoxy-3,5-diamino-.alpha.,.alpha.,.alpha.-trifluoromethylbenzene having the formula ##STR1## wherein R represents an alkyl group.
摘要翻译：具有式“IMAGE”的4-烷氧基-3,5-二氨基-α，α，α-三氟甲基苯，其中R表示烷基。

5. 发明授权

US4342859A Bis(aminophenylthioalkyl)terephthalate and hardener for polyurethane elastomer thereof 失效
标题翻译：对苯二甲酸双（氨基苯硫基烷基）酯和聚氨酯弹性体的固化剂
公开(公告)号：US4342859A
公开(公告)日：1982-08-03
申请号：US153417
申请日：1980-05-27
申请人： Takao Harada , Hideaki Ohashi , Wataro Koike , Chihiro Yazawa , Kazuko Nanjo
发明人： Takao Harada , Hideaki Ohashi , Wataro Koike , Chihiro Yazawa , Kazuko Nanjo
IPC分类号： C08G18/38 , C08G18/32 , C07C69/82
CPC分类号： C08G18/3868
摘要： Bis(aminophenylthioalkyl)terephthalate having the formula ##STR1## wherein R represents a C.sub.1 -C.sub.3 alkyl group. The compounds are useful as hardeners for a polyurethane elastomer.
摘要翻译：对苯二甲酸双（氨基苯硫基烷基）对苯二甲酸酯，其结构式为：其中R代表C1-C3烷基。这些化合物可用作聚氨酯弹性体的硬化剂。

6. 发明授权

US4246392A Method for the preparation of polyurethane elastomers based on polyethyleneglycol-bis(4-aminobenzoates) 失效
标题翻译：基于聚乙二醇 - 双（4-氨基苯甲酸酯）制备聚氨酯弹性体的方法
公开(公告)号：US4246392A
公开(公告)日：1981-01-20
申请号：US950385
申请日：1978-10-11
申请人： Wataro Koike , Masami Takayama , Hideaki Ohashi , Chihiro Yazawa
发明人： Wataro Koike , Masami Takayama , Hideaki Ohashi , Chihiro Yazawa
IPC分类号： C08G18/00 , C08G18/10 , C08G18/32 , C08G18/50 , C08G18/65 , C07C101/62
CPC分类号： C08G18/5027 , C08G18/10 , C08G18/3243
摘要： A method for the preparation of polyurethane elastomers in which polyethyleneglycol-bis(4-aminobenzoate) is used as the curing agent to be admixed with the polyurethane formulations. This curing agent imparts considerably extended pot life to the ready-prepared polyurethane composition to be cured by heating into an elastomer having improved properties.
摘要翻译：使用聚乙二醇 - 双（4-氨基苯甲酸酯）作为固化剂与聚氨酯配方混合的聚氨酯弹性体的制备方法。这种固化剂通过加热成具有改进的性能的弹性体而使待制备的聚氨酯组合物的使用寿命显着延长。

7. 发明授权

US4327204A Process for producing polyurethane elastomer by mixing a hardener composition with an isocyanate composition 失效
标题翻译：通过将固化剂组合物与异氰酸酯组合物混合来制备聚氨酯弹性体的方法
公开(公告)号：US4327204A
公开(公告)日：1982-04-27
申请号：US131555
申请日：1980-03-18
申请人： Yoshijiro Oyaizu , Wataro Koike , Chihiro Yazawa
发明人： Yoshijiro Oyaizu , Wataro Koike , Chihiro Yazawa
IPC分类号： C08G18/00 , C08G18/10 , C08G18/65 , C08G18/72 , C08J9/02
CPC分类号： C08G18/10
摘要： A polyurethane elastomer is produced by mixing a hardener composition containing a polyamine, a long chain polyol having an average molecular weight of 300 to 4,000 and a catalyst with an isocyanate composition comprises a prepolymer having terminal isocyanate group and an average molecular weight of 500 to 5,000 and an organic diisocyanate monomer with or without a triisocyanate monomer and a ratio of isocyanate groups of said prepolymer to amino groups of said polyamine is in a range of 0.6:1 to 1.5:1 and a ratio of a total of isocyanate groups in said isocyanate composition to a sum of amino groups of said polyamine and hydroxyl group of said long chain polyol is in a range of 0.8:1 to 1.4:1.
摘要翻译：通过混合含有聚胺，平均分子量为300〜4,000的长链多元醇和异氰酸酯组合物的催化剂的固化剂组合物来制造聚氨酯弹性体，其包含具有末端异氰酸酯基的预聚物，平均分子量为500〜5000 和具有或不具有三异氰酸酯单体的有机二异氰酸酯单体，并且所述预聚物的异氰酸酯基与所述多胺的氨基的比率在0.6:1至1.5:1的范围内，并且所述异氰酸酯中异氰酸酯基的总量之比所述长链多元醇的所述多胺和羟基的氨基的总和的组成为0.8:1至1.4:1的范围。

8. 发明授权

US4057555A Process for producing saccharin 失效
标题翻译：生产糖精的方法
公开(公告)号：US4057555A
公开(公告)日：1977-11-08
申请号：US677256
申请日：1976-04-15
申请人： Wataro Koike , Takahiro Kimoto , Sadayoshi Matsui
发明人： Wataro Koike , Takahiro Kimoto , Sadayoshi Matsui
IPC分类号： C07D275/06 , C07D327/04
CPC分类号： C07D275/06 , C07D327/04
摘要： 1,2-Benzoisothiazole-3-on-1, 1-dioxide having the formula ##STR1## wherein X represents hydrogen, halogen, nitro, lower alkyl or lower alkoxy and Y represents hydrogen, halogen, lower alkyl, or lower alkoxy is prepared by reacting phosgene with an o-sulfobenzoic acid compound having the formula: ##STR2## or an alkali metal salt or alkaline earth metal salt thereof in the presence of dimethylformamide, thereby producing a mixture of a dichlorotolylsultone and a chlorosulfonylbenzoylchloride; (b) reacting the reaction products of step (a) with an alcohol of the formula ROH wherein R represents a lower alkyl group; and then (c) reacting the product of step (b) with ammonia.
摘要翻译：其中X表示氢，卤素，硝基，低级烷基或低级烷氧基，Y表示氢，卤素，低级烷基或低级烷氧基的1,2-苯并异噻唑-3-基-1,2-二氧化物通过在二甲基甲酰胺存在下使光气与具有下式的邻磺基苯甲酸化合物或其碱金属盐或碱土金属盐反应，由此制备二氯二磺酰基内酯与氯磺酰苯甲酰氯的混合物; （b）使步骤（a）的反应产物与式ROH的醇反应，其中R表示低级烷基; 然后（c）使步骤（b）的产物与氨反应。

9. 发明授权

US4211723A Process for producing chlorosulfonylbenzoylchloride 失效
标题翻译：氯磺酰苯甲酰氯生产工艺
公开(公告)号：US4211723A
公开(公告)日：1980-07-08
申请号：US917255
申请日：1978-06-20
申请人： Wataro Koike , Takahiro Kimoto , Sadayoshi Matsui
发明人： Wataro Koike , Takahiro Kimoto , Sadayoshi Matsui
IPC分类号： C07D327/04 , C07C63/14 , C07C143/52
CPC分类号： C07D327/04 , C07C309/00
摘要： Chlorosulfonylbenzoylchloride having the formula ##STR1## wherein X is hydrogen, halogen or nitro is prepared by reacting phosgene with an aromatic sulfocarboxylic acid having the formula ##STR2## or an alkali metal salt or alkaline earth metal salt thereof in the presence of dimethylformamide.
摘要翻译：具有式“IMAGE”的氯磺酰基苯甲酰氯，其中X是氢，卤素或硝基，是通过在二甲基甲酰胺存在下使光气与具有式“IMAGE”的芳族磺基羧酸或其碱金属盐或碱土金属盐反应而制备的。

10. 发明授权

US4097426A Curing agents for polyurethane foams and elastomers and process of use 失效
标题翻译：聚氨酯泡沫和弹性体的固化剂和使用过程
公开(公告)号：US4097426A
公开(公告)日：1978-06-27
申请号：US735101
申请日：1976-10-26
申请人： Wataro Koike , Masami Takayama , Hideaki Ohashi , Sadayoshi Matsui
发明人： Wataro Koike , Masami Takayama , Hideaki Ohashi , Sadayoshi Matsui
IPC分类号： C08G18/00 , C08G18/10 , C08G18/38 , C08G18/54 , C08G18/65 , C08G18/14 , C08G18/32 , C09K3/00
CPC分类号： C08G18/3814 , C08G18/10
摘要： A curing agent for polyurethane which has a melting point at most 110.degree. C and comprises a mixture of at least two compounds of the general formula: ##STR1## Wherein n is zero or a positive integer. This curing agent has a low solidifying point and good solubility in solvents and thus is excellent in workability. This curing agent is used for the production of polyurethane highly stabilized in quality.
摘要翻译：聚氨酯固化剂，其熔点至多为110℃，并且包含至少两种通式为：其中n为0或正整数的化合物的混合物。

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