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    • 1. 发明授权
    • In-situ liquid flow rate estimation and verification by sonic flow method
    • 声流法原位液体流量估算与验证
    • US5968588A
    • 1999-10-19
    • US819674
    • 1997-03-17
    • Visweswaren SivaramakrishnanYen-Kun WangFong ChangThanh PhamJeff Plante
    • Visweswaren SivaramakrishnanYen-Kun WangFong ChangThanh PhamJeff Plante
    • C23C16/448C23C16/52C23C16/00
    • C23C16/52C23C16/4481
    • An apparatus for in-situ control of the flow of a liquid precursor into a deposition chamber comprises a liquid injection system having a liquid injection outlet connected to a chamber inlet line upstream of the deposition chamber. The liquid injection system includes a liquid precursor supply, a carrier gas supply, a vaporizer, and a controller managing flows of the liquid precursor and carrier gas to the chamber. A bypass line is connected to the chamber inlet line and includes a bypass valve, a sonic orifice, and a pressure gauge upstream of the sonic orifice. To calibrate the flow of the liquid precursor, a flow of carrier gas is directed into the bypass line at a carrier gas sonic flow rate. A first steady state pressure is measured with the pressure gauge. The liquid precursor is vaporized and directed to the flow of carrier gas into the bypass line. A second steady state pressure is measured with the pressure gauge. Calibration information is computed using the first steady state pressure and second steady state pressure based on sonic flow theory. The calibration information is used to calibrate the controller to correct deviations in the liquid flow rate and achieve a target liquid precursor flow rate for improving wafer uniformity.
    • 用于原位控制液体前体进入沉积室的装置包括液体注射系统,其具有连接到沉积室上游的室入口管的液体注入口。 液体注射系统包括液体前体供应源,载气供应器,蒸发器和控制液体前体和载气流到腔室的控制器。 旁路管路连接到腔室入口管线,并且包括旁通阀,声波孔口和声波孔口上游的压力计。 为了校准液体前体的流动,以载气声音流速将载气流引导到旁路管线中。 用压力表测量第一稳态压力。 液体前体蒸发并引导到载气流入旁通管线。 用压力表测量第二稳态压力。 基于声流理论,使用第一稳态压力和第二稳态压力计算校准信息。 校准信息用于校准控制器以校正液体流速中的偏差,并实现目标液体前体流速以改善晶片均匀性。
    • 9. 发明授权
    • Vaporizing reactant liquids for chemical vapor deposition film processing
    • 用于化学气相沉积膜处理的汽化反应液体
    • US06783118B2
    • 2004-08-31
    • US09919633
    • 2001-07-31
    • Visweswaren SivaramakrishnanJohn M. White
    • Visweswaren SivaramakrishnanJohn M. White
    • B01F304
    • C23C16/4481B01F3/022Y10S261/65
    • The disclosure relates to a vaporizer valve which accepts a carrier gas and a pressurized liquid and forms a mixture of the carrier gas and vaporized liquid. An internal cavity receives the carrier gas through a carrier aperture and the liquid through a liquid aperture, and the mixed gas and vapor are exhausted out of the cavity via a third aperture. A moveable diaphragm disposed adjacent to the liquid aperture forms a vaporization region having a pressure gradient. The liquid passing through this pressure gradient vaporizes due to expansion. By controlling the diaphragm position with a feedback control circuit responsive to a liquid flow rate monitor, the liquid flow rate may be controlled independently of the carrier gas flow rate.
    • 本公开涉及一种蒸发器阀,其接收载气和加压液体并形成载气和汽化液体的混合物。 内腔通过载体孔接收载气,液体通过液体孔接收,并且混合气体和蒸气经由第三孔排出空腔。 邻近液体孔设置的可移动隔膜形成具有压力梯度的蒸发区域。 通过该压力梯度的液体由于膨胀而蒸发。 通过利用响应于液体流速监测器的反馈控制电路来控制隔膜位置,可以独立于载气流量来控制液体流速。