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1. 发明授权

US08614358B2 Process for preparing 2-methyl-3-(4-tert-butylphenyl)propanal with high para-isomer purity 有权
标题翻译：具有高对位异构体纯度的2-甲基-3-（4-叔丁基苯基）丙醛的方法
公开(公告)号：US08614358B2
公开(公告)日：2013-12-24
申请号：US13234809
申请日：2011-09-16
申请人： Ulrich Griesbach , Jörg Botzem , Florian Stecker
发明人： Ulrich Griesbach , Jörg Botzem , Florian Stecker
IPC分类号： C07C45/42
CPC分类号： C07C45/42 , C07C45/515 , C07C45/62 , C07C45/74 , C07C45/82 , C07C45/85 , C25B3/02 , C07C47/542 , C07C47/548 , C07C49/76 , C07C49/11 , C07C47/232 , C07C47/228
摘要： The present invention relates to a process for preparing 2-methyl-3-(4-tert-butyl-phenyl)propanal with high para-isomer purity, and also to a process for preparing 4-tert-butylbenzaldehyde with high para-isomer purity.
摘要翻译：本发明涉及一种具有高对位异构体纯度的2-甲基-3-（4-叔丁基 - 苯基）丙醛的制备方法，还涉及制备具有高对位异构体纯度的4-叔丁基苯甲醛的方法。

2. 发明授权

US08629304B2 Electrochemical method for producing 3-tert-butylbenzaldehyde dimethyl acetal 有权
标题翻译：制备3-叔丁基苯甲醛二甲基缩醛的电化学方法
公开(公告)号：US08629304B2
公开(公告)日：2014-01-14
申请号：US13260650
申请日：2010-03-22
申请人： Florian Stecker , Andreas Fischer , Jörg Botzem , Ulrich Griesbach , Ralf Pelzer
发明人： Florian Stecker , Andreas Fischer , Jörg Botzem , Ulrich Griesbach , Ralf Pelzer
IPC分类号： C07C45/42 , C07C43/115 , C07C43/307
CPC分类号： C25B3/02 , C07C43/174 , C07C43/303 , C07C45/515 , C07C47/542
摘要： The present invention relates to 3-tert-butylbenzaldehyde dimethyl acetal and to 3-tert-butylbenzyl methyl ether and to an electrochemical method for producing 3-tert-butyl-benzaldehyde dimethyl acetal and intermediates passed through in said method.
摘要翻译：本发明涉及3-叔丁基苯甲醛二甲基缩醛和3-叔丁基苄基甲基醚，以及用于制备3-叔丁基苯甲醛二甲基缩醛的电化学方法和所述方法中通过的中间体。

3. 发明申请

US20120016162A1 ELECTROCHEMICAL METHOD FOR PRODUCING 3-TERT-BUTYLBENZALDEHYDE DIMETHYL ACETAL 有权
标题翻译：生产3-叔丁基苄基二甲基乙酰胺的电化学方法
公开(公告)号：US20120016162A1
公开(公告)日：2012-01-19
申请号：US13260650
申请日：2009-03-27
申请人： Florian Stecker , Andreas Fischer , Jörg Botzem , Ulrich Griesbach , Ralf Pelzer
发明人： Florian Stecker , Andreas Fischer , Jörg Botzem , Ulrich Griesbach , Ralf Pelzer
IPC分类号： C07C43/307 , C07C45/42 , C25B3/00 , C07C43/115
CPC分类号： C25B3/02 , C07C43/174 , C07C43/303 , C07C45/515 , C07C47/542
摘要： The present invention relates to 3-tert-butylbenzaldehyde dimethyl acetal and to 3-tert-butylbenzyl methyl ether and to an electrochemical method for producing 3-tert-butyl-benzaldehyde dimethyl acetal and intermediates passed through in said method.
摘要翻译：本发明涉及3-叔丁基苯甲醛二甲基缩醛和3-叔丁基苄基甲基醚，以及用于制备3-叔丁基苯甲醛二甲基缩醛的电化学方法和所述方法中通过的中间体。

4. 发明申请

US20120071696A1 PROCESS FOR PREPARING 2-METHYL-3-(4-TERT-BUTYLPHENYL)PROPANAL WITH HIGH PARA-ISOMER PURITY 有权
标题翻译：制备具有高PARA-ISOMER PURITY的2-甲基-3-（4-叔丁基苯基）丙酸的方法
公开(公告)号：US20120071696A1
公开(公告)日：2012-03-22
申请号：US13234809
申请日：2011-09-16
申请人： Urlich Griesbach , Jörg Botzem , Florian Stecker
发明人： Urlich Griesbach , Jörg Botzem , Florian Stecker
IPC分类号： C07C45/42
CPC分类号： C07C45/42 , C07C45/515 , C07C45/62 , C07C45/74 , C07C45/82 , C07C45/85 , C25B3/02 , C07C47/542 , C07C47/548 , C07C49/76 , C07C49/11 , C07C47/232 , C07C47/228
摘要： The present invention relates to a process for preparing 2-methyl-3-(4-tert-butyl-phenyl)propanal with high para-isomer purity, and also to a process for preparing 4-tert-butylbenzaldehyde with high para-isomer purity.
摘要翻译：本发明涉及一种具有高对位异构体纯度的2-甲基-3-（4-叔丁基 - 苯基）丙醛的制备方法，还涉及制备具有高对位异构体纯度的4-叔丁基苯甲醛的方法。

5. 发明授权

US08367875B2 Process for the preparation of m-substituted alkyltoluenes by isomerization with ionic liquids as catalysts 有权
标题翻译：通过用离子液体作为催化剂异构化制备间取代的烷基甲苯的方法
公开(公告)号：US08367875B2
公开(公告)日：2013-02-05
申请号：US13024786
申请日：2011-02-10
申请人： Andreas Lanver , Klaus Ebel , Karl Beck , Ralf Pelzer , Jörg Botzem , Ulrich Griesbach
发明人： Andreas Lanver , Klaus Ebel , Karl Beck , Ralf Pelzer , Jörg Botzem , Ulrich Griesbach
IPC分类号： C07C45/45 , C07C5/22
CPC分类号： C07C45/62 , C07C5/2732 , C07C45/74 , C07C2527/126 , C07C15/02 , C07C47/228 , C07C47/232
摘要： The invention relates to a process for the preparation of m-substituted alkyltoluenes of the formula (I) in which R1 is C1-C5-alkyl, wherein a p-substituted alkyltoluene of the formula (II) in which R1 has the meaning given under formula (I), is isomerized in the presence of ionic liquids to give an m-substituted alkyltoluene of the formula (I). The m-substituted alkyltoluenes obtainable according to the invention are starting compounds for the preparation of fragrances and aroma substances.
摘要翻译：本发明涉及一种制备其中R 1为C 1 -C 5 - 烷基的式（I）的间位取代的烷基甲苯的方法，其中式（II）的对取代烷基甲苯其中R 1具有下面给出的含义式（I）的化合物在离子液体的存在下异构化，得到式（I）的间位取代的烷基甲苯。根据本发明可获得的m取代的烷基甲苯是用于制备香料和香料物质的起始化合物。

6. 发明申请

US20120209031A1 METHOD FOR PRODUCING M-SUBSTITUTED PHENYLALKANOLS BY MEANS OF ISOMERIZATION 失效
标题翻译：通过异构化制备M取代的苯乙醇的方法
公开(公告)号：US20120209031A1
公开(公告)日：2012-08-16
申请号：US13503488
申请日：2010-10-19
申请人： Andreas Lanver , Klaus Ebel , Karl Beck , Ralf Pelzer , Jörg Botzem , Ulrich Griesbach
发明人： Andreas Lanver , Klaus Ebel , Karl Beck , Ralf Pelzer , Jörg Botzem , Ulrich Griesbach
IPC分类号： C07C29/56 , C07C47/228 , C07C45/51
CPC分类号： C07C29/56 , C07C45/29 , C11B9/0061 , C07C33/20 , C07C47/228
摘要： The invention relates to a process for the preparation of m-substituted phenylalkanols of the formula (I) in which R1 is C1-C5-alkyl and R2, R3, R4 and R5, independently of one another, are hydrogen or methyl, wherein a p-substituted phenylalkanol of the formula (II) in which R1, R2, R3, R4 and R5 having the meanings given under formula (I), is isomerized in the presence of a Friedel-Crafts catalyst to give an m-substituted phenylalkanol of the formula (I). From the m-substituted phenylalkanols of the formula (I) it is possible to form, by oxidation or dehydrogenation, as products of value, the corresponding aldehydes, which are known as fragrances and aroma chemicals.
摘要翻译：本发明涉及一种制备式（I）的间位取代的苯基烷醇的方法，其中R 1为C 1 -C 5 - 烷基，R 2，R 3，R 4和R 5彼此独立地为氢或甲基，其中a 式（II）的对取代的苯基链烷醇，其中具有式（I）给出的含义的R 1，R 2，R 3，R 4和R 5在Friedel-Crafts催化剂存在下异构化得到m-取代的苯基烷醇式（I）。从式（I）的间位取代的苯基烷醇可以通过氧化或脱氢形成作为有价值的产物，相应的醛被称为香料和芳香化学品。

7. 发明申请

US20120209030A1 PROCESS FOR PREPARING M- OR P-SUBSTITUTED PHENYLALKANOLS BY ALKYLATION 有权
标题翻译：通过烷基化制备M取代或P-取代的苯基甘露醇的方法
公开(公告)号：US20120209030A1
公开(公告)日：2012-08-16
申请号：US13503515
申请日：2010-10-14
申请人： Andreas Lanver , Klaus Ebel , Karl Beck , Ralf Pelzer , Jörg Botzem , Ulrich Griesbach
发明人： Andreas Lanver , Klaus Ebel , Karl Beck , Ralf Pelzer , Jörg Botzem , Ulrich Griesbach
IPC分类号： C07C45/29 , C07C29/32
CPC分类号： C07C29/32 , C07C29/56 , C07C45/29 , C07C33/20 , C07C47/228
摘要： The invention relates to a process for the preparation of m- or p-substituted phenylalkanols of the formula (I) in which R1 is bonded to the phenyl ring in the m- or p-position and is C1-C5-alkyl, and R2, R3, R4 and R5, independently of one another, are hydrogen or methyl, wherein an unsubstituted phenylalkanol of the formula (II) in which R2, R3, R4 and R5 have the meanings given under formula (I) is alkylated together with a C1-C5-alkyl halide of the formula (III) R1-Hal (III), in which R1 has the meaning given under formula (I) and Hal is halogen, in the presence of a Friedel-Crafts catalyst to give an m- or p-alkyl-substituted phenylalkanol of the formula (I), then the reaction mixture is worked-up and the desired m- or p-alkyl-substituted phenylalkanol of the formula (I) is separated off, the other formed by-products are returned to the reaction mixture and these are isomerized in the presence of a Friedel-Crafts catalyst to give the desired m- or p-alkyl-substituted phenylalkanol. From the m- or p-alkyl-substituted phenylalkanols of the formula (I), it is possible to form, by oxidation or dehydrogenation, as products of value, the corresponding aldehydes, which play an interesting role as fragrances and aroma chemicals.
摘要翻译：本发明涉及一种制备式（I）的间 - 或对 - 取代的苯烷醇的方法，其中R 1与m-或p-位上的苯环键合并且是C1-C5-烷基，R2 R 3，R 4和R 5彼此独立地为氢或甲基，其中R 2，R 3，R 4和R 5具有式（I）所示含义的式（II）的未取代的苯基烷醇与其中R 1具有式（I）所示含义，Hal为卤素的式（III）R1-Hal（Ⅲ）的C1-C5烷基卤化物，在Friedel-Crafts催化剂存在下，得到m- 或式（I）的对烷基取代的苯基链烷醇，然后将反应混合物处理并分离所需的式（I）的间 - 或对 - 烷基取代的苯基烷醇，另一个形成的副产物返回到反应混合物中，并将它们在Friedel-Crafts催化剂存在下异构化，得到所需的间 - 或对 - 烷基取代的苯基 kanol 从式（I）的间 - 或对 - 烷基取代的苯烷醇，可以通过氧化或脱氢形成作为有价值的产物，相应的醛作为香料和香气化学品起着重要的作用。

8. 发明申请

US20110196176A1 PROCESS FOR THE PREPARATION OF M-SUBSTITUTED ALKYLTOLUENES BY ISOMERIZATION WITH IONIC LIQUIDS AS CATALYSTS 有权
标题翻译：通过与作为催化剂的离子液体异构化制备M取代的烷基甲苯的方法
公开(公告)号：US20110196176A1
公开(公告)日：2011-08-11
申请号：US13024786
申请日：2011-02-10
申请人： Andreas Lanver , Klaus Ebel , Karl Beck , Ralf Pelzer , Jörg Botzem , Ulrich Griesbach
发明人： Andreas Lanver , Klaus Ebel , Karl Beck , Ralf Pelzer , Jörg Botzem , Ulrich Griesbach
IPC分类号： C07C45/45 , C07C5/22
CPC分类号： C07C45/62 , C07C5/2732 , C07C45/74 , C07C2527/126 , C07C15/02 , C07C47/228 , C07C47/232
摘要： The invention relates to a process for the preparation of m-substituted alkyltoluenes of the formula (I) in which R1 is C1-C5-alkyl, wherein a p-substituted alkyltoluene of the formula (II) in which R1 has the meaning given under formula (I), is isomerized in the presence of ionic liquids to give an m-substituted alkyltoluene of the formula (I). The m-substituted alkyltoluenes obtainable according to the invention are starting compounds for the preparation of fragrances and aroma substances.
摘要翻译：本发明涉及一种制备其中R 1为C 1 -C 5 - 烷基的式（I）的间位取代的烷基甲苯的方法，其中式（II）的对取代烷基甲苯其中R 1具有下面给出的含义式（I）的化合物在离子液体的存在下异构化，得到式（I）的间位取代的烷基甲苯。根据本发明可获得的m取代的烷基甲苯是用于制备香料和香料物质的起始化合物。

9. 发明授权

US08686193B2 Method for producing M-substituted phenylalkanols by means of isomerization 失效
标题翻译：通过异构化制备M取代的苯基链烷醇的方法
公开(公告)号：US08686193B2
公开(公告)日：2014-04-01
申请号：US13503488
申请日：2010-10-19
申请人： Andreas Lanver , Klaus Ebel , Karl Beck , Ralf Pelzer , Jörg Botzem , Ulrich Griesbach
发明人： Andreas Lanver , Klaus Ebel , Karl Beck , Ralf Pelzer , Jörg Botzem , Ulrich Griesbach
IPC分类号： C07C45/51 , C07C29/56 , C07C47/22 , A61K8/18
CPC分类号： C07C29/56 , C07C45/29 , C11B9/0061 , C07C33/20 , C07C47/228
摘要： The invention relates to a process for the preparation of m-substituted phenylalkanols of the formula (I) in which R1 is C1-C5-alkyl and R2, R3, R4 and R5, independently of one another, are hydrogen or methyl, wherein a p-substituted phenylalkanol of the formula (II) in which R1, R2, R3, R4 and R5 having the meanings given under formula (I), is isomerized in the presence of a Friedel-Crafts catalyst to give an m-substituted phenylalkanol of the formula (I). From the m-substituted phenylalkanols of the formula (I) it is possible to form, by oxidation or dehydrogenation, as products of value, the corresponding aldehydes, which are known as fragrances and aroma chemicals.
摘要翻译：本发明涉及一种制备式（I）的间位取代的苯基烷醇的方法，其中R 1为C 1 -C 5 - 烷基且R 2，R 3，R 4和R 5彼此独立地为氢或甲基，其中a 式（II）的对取代的苯基链烷醇，其中具有式（I）给出的含义的R 1，R 2，R 3，R 4和R 5在Friedel-Crafts催化剂存在下异构化得到m-取代的苯基烷醇式（I）。从式（I）的间位取代的苯基烷醇可以通过氧化或脱氢形成作为有价值的产物，相应的醛被称为香料和芳香化学品。

10. 发明申请

US20120059177A1 METHOD FOR PRODUCING 2-SUBSTITUTED TETRAHYDROPYRANOLS 有权
标题翻译：生产2-取代的四氢呋喃的方法
公开(公告)号：US20120059177A1
公开(公告)日：2012-03-08
申请号：US13321417
申请日：2010-05-11
申请人： Gabriele Gralla , Ralf Pelzer , Klaus Ebel , Ulrich Griesbach , Jörg Botzem
发明人： Gabriele Gralla , Ralf Pelzer , Klaus Ebel , Ulrich Griesbach , Jörg Botzem
IPC分类号： C07D309/10
CPC分类号： C07D309/12
摘要： The present invention relates to a process for the preparation of 2-substituted 4-hydroxy-4-methyltetrahydropyranols by reacting 3-methylbut-3-en-1-ol (isoprenol) with the corresponding aldehydes in the presence of a strongly acidic cation exchanger. Specifically, the present invention relates to a corresponding process for the preparation of 2-isobutyl-4-hydroxy-4-methyltetrahydropyran by reacting isoprenol with isovaleraldehyde.
摘要翻译：本发明涉及通过使3-甲基丁-3-烯-1-醇（异戊二烯）与相应的醛在强酸性阳离子交换剂存在下反应制备2-取代的4-羟基-4-甲基四氢吡喃醇的方法。具体地说，本发明涉及通过异戊二烯与异戊醛反应制备2-异丁基-4-羟基-4-甲基四氢吡喃的相应方法。

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