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1. 发明授权

US4837322A Mixtures of sulfurous triazine compounds 失效
标题翻译：亚硫酸三嗪化合物的混合物
公开(公告)号：US4837322A
公开(公告)日：1989-06-06
申请号：US89895
申请日：1987-08-27
申请人： Ulrich Deschler , Georg Hellwig , Rudolf Michel , Peter Kleinschmit , Siegfried Wolff
发明人： Ulrich Deschler , Georg Hellwig , Rudolf Michel , Peter Kleinschmit , Siegfried Wolff
IPC分类号： C07D251/52 , C08K5/34 , C08K5/378 , C08L21/00
CPC分类号： C07D251/52 , C08K5/378
摘要： Mixtures of sulfurous triazine compounds and methods of preparing these compounds with the general formula ##STR1## in which R.sup.1, R.sup.2 =H,R.sup.2 =benzyl,R.sup.2, R.sup.3, R.sup.4 =C.sub.1 -C.sub.8 -alkyl, allyl, C.sub.3 -C.sub.8 cycloalkyl, the latter unsubstituted or substituted with 1-3 methyl groups, 2-hydroxyethyl, 3-hydroxypropyl, 2-hydroxypropyl orR.sup.3 and R.sup.4 (together): C.sub.4 -C.sub.6 -alkylene, --(CH.sub.2 --CHX).sub.2 Y withX=H, CH.sub.3, Y=O,S,S.sub.a : Polysulfide chain with 2-10 S atoms (i.e. 2.ltoreq.a.ltoreq.10), in which the individual polysulfides are present in such concentrations that the statistical average value of "a" is a whole or fractional numerical value in the range from 2 to 5., characterized in that a triazine compound of the general formula ##STR2## in which R.sup.1, R.sup.2, R.sup.3, R.sup.4 have the meanings indicated above is reacted with an ammonium polysulfide or alkali polysulfide and dissolved in a protic polar solvent, especially water, at a temperature of 80.degree. to 140.degree. C.
摘要翻译：亚硫基三嗪化合物的混合物和制备这些具有通式Ⅰ的化合物的方法，其中R1，R2 = H，R2 =苄基，R2，R3，R4 = C1-C8-烷基，烯丙基，C3-C8环烷基，未取代或被1-3个甲基取代的后者，2-羟基乙基，3-羟丙基，2-羟基丙基或R 3和R 4（一起）：C 4 -C 6亚烷基， - （CH 2 -CHX）2 Y，X = CH 3，Y = O，S，Sa：具有2-10个S原子的多硫链（即2

2. 发明授权

US4835297A Method of preparing sulfenic acid chlorides and sulfenic acid esters 失效
标题翻译：制备磺酰氯和亚磺酸酯的方法
公开(公告)号：US4835297A
公开(公告)日：1989-05-30
申请号：US940069
申请日：1986-12-10
申请人： Ulrich Deschler , Rudolf Michel , Peter Kleinschmit , Siegfried Wolff
发明人： Ulrich Deschler , Rudolf Michel , Peter Kleinschmit , Siegfried Wolff
IPC分类号： C07F7/18
CPC分类号： C07F7/1892
摘要： The invention is directed to a method of preparing sulfenic acid chlorides and sulfenic acid esters with hydrolyzable silyl groups in which an oligosulfane containing silyl groups is chlorinated, the sulfenic acid chloride produced is separated and converted by reaction with an alkali alcoholate to the corresponding sulfenic acid ester.
摘要翻译：本发明涉及一种制备具有水解性甲硅烷基的亚磺酰氯和亚磺酸酯的方法，其中含有甲硅烷基的低级亚烷基被氯化，所产生的亚磺酰氯与碱性醇化物反应分离并转化成相应的亚磺酸酯。

3. 发明授权

US5206304A Vulcanizable rubber mixtures containing bis-(2,4-organylthio-triazine-6-yl) polysulfides 失效
标题翻译：含有双 - （2,4-有机硫基 - 三嗪-6-基）多硫化物的可硫化橡胶混合物
公开(公告)号：US5206304A
公开(公告)日：1993-04-27
申请号：US751586
申请日：1991-08-22
申请人： Georg Hellwig , Reinhard Stober , Christoph Klatte , Ulrich Deschler , Siegfried Wolff , Udo Gorl
发明人： Georg Hellwig , Reinhard Stober , Christoph Klatte , Ulrich Deschler , Siegfried Wolff , Udo Gorl
IPC分类号： C07D251/38 , C08K5/378
CPC分类号： C08K5/378 , C07D251/38
摘要： Bis(2,4-organylthio-s-triazine-6-yl) polysulfides of the general Formula (I) ##STR1## prepared from compounds of the general formula (II) ##STR2## and from an ammonium or alkali polysulfide and the use of such compounds as accelerators in vulcanizable rubber mixtures.
摘要翻译：由通式（II）化合物＆lt; IMAGE＆gt;和由铵或碱的多硫化物制备的通式（I）＆lt; IMAGE＆gt;的双（2,4-有机硫基-S-三嗪-6-基）多硫化物，的这种化合物，如可硫化橡胶混合物中的促进剂。

4. 发明授权

US4704428A Silyl substituted cyclopentadiene, process for its production and synthetic resin and rubber mixtures containing it 失效
标题翻译：甲硅烷基取代的环戊二烯，其生产方法和含有它的合成树脂和橡胶混合物
公开(公告)号：US4704428A
公开(公告)日：1987-11-03
申请号：US933136
申请日：1986-11-21
申请人： Ulrich Deschler , Peter Panster , Peter Kleinschmit , Siegfried Wolff , Ewe-Hong Tan
发明人： Ulrich Deschler , Peter Panster , Peter Kleinschmit , Siegfried Wolff , Ewe-Hong Tan
IPC分类号： C08L21/00 , C07F7/18 , C08K5/00 , C08K5/5419 , C08K5/5425 , C08K9/06 , C08L1/00 , C08L7/00 , C08L23/00 , C08L27/00 , C08L33/00 , C08L33/02 , C08L101/00 , C08K3/36
CPC分类号： C07F7/1836 , C08K5/5419 , C08K9/06
摘要： The invention is directed to silylalkyl and silylaralkyl substituted cyclopentadienes which have a hydrolyzable group attached to the silicone atom, a process for their production and peroxide cross-linkable synthetic resin and rubber mixtures containing them.
摘要翻译：本发明涉及具有连接到硅氧烷原子的可水解基团的甲硅烷基烷基和甲硅烷基烷基取代的环戊二烯，其生产方法和可过氧化物可交联的合成树脂和含有它们的橡胶混合物。

5. 发明授权

US5073644A Method of preparing pure 3-butenyl triorganooxysilanes, the intermediate products 3,4-dichlorobutyl triorgano-oxysilanes and use of the final products 失效
标题翻译：中间产品3,4-二氯丁基三异氰酸酯和最终产物的使用制备三丁基三异氰酸酯的方法
公开(公告)号：US5073644A
公开(公告)日：1991-12-17
申请号：US375923
申请日：1989-07-06
申请人： Ulrich Deschler , Peter Kleinschmit , Siegfried Wolff , Ewe-Hong Tan
发明人： Ulrich Deschler , Peter Kleinschmit , Siegfried Wolff , Ewe-Hong Tan
IPC分类号： C07F7/18 , C08K5/00 , C08K5/5425
CPC分类号： C07F7/1892 , C07F7/1836 , C07F7/188 , C08K5/5425
摘要： A method of preparing pure 3-butenyl triorgano oxysilanes, the intermediate products 3,4-dichlorobutyl triorgano oxysilanes and the use of the final products in rubber mixtures reinforced with silicic acid and vulcanizable with peroxides. 3,4-dichlorobutene-1 and trichlorosilane are used as initial products.
摘要翻译：制备纯3-丁烯基三有机基氧基硅烷的方法，中间体产物3,4-二氯丁基三有机氧基硅烷，并使用最终产物在用硅酸增强并用过氧化物硫化的橡胶混合物中。 3,4-二氯丁烯-1和三氯硅烷用作初始产品。

6. 发明授权

US5164501A Method of preparing pure 3-butenyl triorganooxysilanes, the intermediate products 3,4-dichlorobutyl triorganooxysilanes and use of the final products 失效
标题翻译：制备纯3-丁烯基三有机氧基硅烷的方法，中间产物3,4-二氯丁基三有机氧基硅烷，并使用最终产物
公开(公告)号：US5164501A
公开(公告)日：1992-11-17
申请号：US836713
申请日：1992-02-19
申请人： Ulrich Deschler , Peter Kleinschmit , Siegfried Wolff , Ewe-Hong Tan
发明人： Ulrich Deschler , Peter Kleinschmit , Siegfried Wolff , Ewe-Hong Tan
IPC分类号： C07F7/18 , C08K5/5425
CPC分类号： C07F7/1892 , C07F7/1836 , C07F7/188 , C08K5/5425
摘要： A method of preparing pure 3-butenyl triorgano oxysilanes, the intermediate products 3,4-dichlorobutyl triorgano oxysilanes and the use of the final products in rubber mixtures reinforced with silicic acid and vulcanizable with peroxides. 3,4-dichlorobutene-1 and trichlorosilane are used as initial products.
摘要翻译：制备纯3-丁烯基三有机基氧基硅烷的方法，中间体产物3,4-二氯丁基三有机氧基硅烷，并使用最终产物在用硅酸增强并用过氧化物硫化的橡胶混合物中。 3,4-二氯丁烯-1和三氯硅烷用作初始产品。

7. 发明授权

US4645850A Silyl substituted cyclopentadiene, process for its production and synthetic resin and rubber mixtures containing it 失效
标题翻译：甲硅烷基取代的环戊二烯，其生产方法和含有它的合成树脂和橡胶混合物
公开(公告)号：US4645850A
公开(公告)日：1987-02-24
申请号：US756088
申请日：1985-07-17
申请人： Ulrich Deschler , Peter Panster , Peter Kleinschmit , Siegfried Wolff , Ewe-Hong Tan
发明人： Ulrich Deschler , Peter Panster , Peter Kleinschmit , Siegfried Wolff , Ewe-Hong Tan
IPC分类号： C08L21/00 , C07F7/18 , C08K5/00 , C08K5/5419 , C08K5/5425 , C08K9/06 , C08L1/00 , C08L7/00 , C08L23/00 , C08L27/00 , C08L33/00 , C08L33/02 , C08L101/00 , C07F7/08
CPC分类号： C07F7/1836 , C08K5/5419 , C08K9/06
摘要： The invention is directed to silyl alkyl and silylaralkyl substituted cyclopentadienes which have a hydrolyzable group attached to the silicon atom, a process for their production and peroxide cross-linkable synthetic resin and rubber mixtures containing them.
摘要翻译：本发明涉及具有与硅原子连接的可水解基团的甲硅烷基烷基和甲硅烷基烷基取代的环戊二烯，其生产方法和可过氧化物可交联的合成树脂和含有它们的橡胶混合物。

8. 发明授权

US4704414A Surface modified synthetic, silicatic filler, a process for its production and its use 失效
标题翻译：表面改性合成，硅胶填料，其生产和使用的过程
公开(公告)号：US4704414A
公开(公告)日：1987-11-03
申请号：US764994
申请日：1985-08-12
申请人： Dieter Kerner , Peter Kleinschmit , Alan Parkhouse , Siegfried Wolff
发明人： Dieter Kerner , Peter Kleinschmit , Alan Parkhouse , Siegfried Wolff
IPC分类号： C08K9/06 , C09C3/12 , C08L21/00 , C09C1/28
CPC分类号： C08K9/06 , C09C3/12 , C01P2004/84
摘要： The invention is directed to the modification of synthetic, silicatic fillers with water insoluble sulfur containing organosilicon compounds. For this purpose, the fillers are converted into an aqueous suspension and treated with the organosilicon compounds, optionally in the presence of an emulsifier. The thus modified filler in vulcanized rubber mixtures results in a clear improvement in the industrial properties of the rubber.
摘要翻译：本发明涉及用水不溶性含硫有机硅化合物改性合成硅胶填料。为此目的，将填料转化成水性悬浮液并任选在乳化剂存在下用有机硅化合物处理。硫化橡胶混合物中这样改性的填料导致橡胶工业性能的明显改善。

9. 发明授权

US4444936A Bis-(silylethyl)-oligosulphides and process for their production 失效
标题翻译：双（甲硅烷基乙基） - 二硫化物及其生产方法
公开(公告)号：US4444936A
公开(公告)日：1984-04-24
申请号：US461432
申请日：1983-01-27
申请人： Rudolf Schwarz , Peter Kleinschmit , Christa Liedtke , Siegfried Wolff
发明人： Rudolf Schwarz , Peter Kleinschmit , Christa Liedtke , Siegfried Wolff
IPC分类号： C08L7/00 , C07F7/08 , C07F7/12 , C07F7/18 , C08G75/02 , C08G75/14 , C08K5/5425 , C08K5/548 , C08L21/00 , C08L23/00 , C08L33/00 , C08L33/02 , C08L101/00 , C08K5/06
CPC分类号： C08K5/548 , C07F7/12 , C07F7/182 , C08G75/02 , C08G75/14
摘要： Novel bis-(silylethyl)-oligosulphides are obtained by reacting a vinyl silane of the formula (CH.sub.2 .dbd.CH).sub.m --SiR.sub.n.sup.1 R.sub.4--(m+n) in which R represents chlorine, bromine, iodine, C.sub.1 --C.sub.3 -alkoxy, 2-methoxyethoxy, 2-ethoxyethoxy or hydroxy, R.sup.1 represents C.sub.1 --C.sub.3 -alkyl, phenyl or C.sub.5 --C.sub.7 -cycloalkyl, n is 0, 1 or 2, m is 1 or 2 and m+n is 1, 2 or 3 with sulphur as well as in a given case hydrogen sulphide in molar ratios of vinyl silane to sulphur of from 1:2.5 to 1:10 and vinyl silane to hydrogen sulphide of from 1:0 to 1:5 at temperatures between about 100.degree. and 200.degree. C. under pressure of from 1 to 25 bars (total pressure at the reaction) temperature) and in the presence of sulphidation catalysts known per se, in a given case followed by hydrolysis or partial hydrolysis of the reaction products. The bis-(silylethyl)-oligosulphides are used as reinforcing additives (adhesive agents) in crosslinkable rubber mixtures containing silicate fillers and in a given case carbon black as well as in a given case sulphur and other customary constituents.
摘要翻译：通过使式（CH2 = CH）m-SiRn1R4-（m + n）的乙烯基硅烷（其中R表示氯，溴，碘，C1-C3-烷氧基，2-甲基苯基）甲氧基乙氧基，2-乙氧基乙氧基或羟基，R1代表C1-C3-烷基，苯基或C5-C7-环烷基，n是0,1或2，m是1或2，m + n是1,2或3，以及在给定情况下，在约100至200℃的温度下，乙烯基硅烷与硫的摩尔比为1:2.5至1:10的硫化氢和乙烯基硅烷至硫化氢的摩尔比为1:0至1:5 在1至25巴（反应总压力）温度的压力下，在本身已知的硫化催化剂的存在下，在给定的情况下，随后水解或部分水解反应产物。双（甲硅烷基乙基） - 二硫化物用作含有硅酸盐填料的交联性橡胶混合物中的增强添加剂（粘合剂），在给定情况下用于炭黑以及在给定情况下硫和其它常规组分。

10. 发明授权

US4514231A Natural oxidic or silicate filler modified on the surface, a process for its production 失效
标题翻译：表面改性的天然氧化物或硅酸盐填料，其生产工艺
公开(公告)号：US4514231A
公开(公告)日：1985-04-30
申请号：US602768
申请日：1984-04-23
申请人： Dieter Kerner , Peter Kleinschmit , Alan Parkhouse , Siegfried Wolff
发明人： Dieter Kerner , Peter Kleinschmit , Alan Parkhouse , Siegfried Wolff
IPC分类号： C08L7/00 , C08K9/00 , C08K9/04 , C08K9/06 , C08L21/00 , C08L23/00 , C08L33/00 , C08L33/02 , C08L101/00 , C09C1/42 , C09C3/00 , C09C3/12
CPC分类号： C09C3/12 , C08K9/06 , C09C1/42 , C01P2004/84
摘要： The invention is directed to the modification of natural oxidic or silicate fillers with water insoluble sulfur containing organosilicon compounds. For this purpose, the fillers are converted into an aqueous suspension and treated with the organosilicon compounds, in a given case in the presence of an emulsifier.
摘要翻译：本发明涉及用水不溶性含硫有机硅化合物改性天然氧化物或硅酸盐填料。为此，将填料转化为水性悬浮液，并在有机硅化合物的情况下在乳化剂存在下进行处理。

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