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1. 发明授权

US3844824A Process of treating fibrous materials with the reaction product of methylolphosphine adducts and nitrogenous compounds 失效
标题翻译：用甲基磷酰胺和硝基化合物的反应产物处理纤维材料的方法
公开(公告)号：US3844824A
公开(公告)日：1974-10-29
申请号：US30677472
申请日：1972-11-15
申请人： US AGRICULTURE
发明人： REEVES W , DONALDSON D , BENINATE J , DAIGLE D , DRAKE G
IPC分类号： C07F9/50 , C07F9/53 , C08G79/02 , D06M15/431 , D06M15/673 , C09D5/18
CPC分类号： D06M15/673 , C07F9/5004 , C07F9/5304 , C08G79/02 , D06M15/431 , Y10S428/921 , Y10T442/268
摘要： Soluble methylol phosphine adducts which contain one or more methylol phosphine radicals (PCH2OH) are prepared by reacting in a suitable solvent tris(hydroxymethyl)phosphine with an amide or amine which contains one or more hydrogens attached to trivalent nitrogen. These soluble adducts are particularly valuable for the preparation of thermosetting flame resistant polymers by reacting them with nitrogenous compounds which contain two or more hydrogen and methylol groups attached to trivalent nitrogen. The adducts are also valuable for the preparation of flame-, glow-, wrinkle-, and shrink-resistant knit and woven textiles by causing the adducts to react with nitrogenous compounds in or on the textile structure by application of heat.
摘要翻译：含有一个或多个羟甲基膦基（PCH 2 OH）的可溶性羟甲基膦加合物通过在合适的溶剂中将三（羟甲基）膦与含有一个或多个与三价氮连接的氢的酰胺或胺反应来制备。这些可溶性加合物通过与含有两个或多个连接到三价氮的氢和羟甲基的含氮化合物反应来制备热固性阻燃聚合物是特别有价值的。加合物对于制备阻燃，发光，抗皱和抗收缩的针织和纺织织物也是有价值的，它们通过加热使加合物与织物结构中或其上的含氮化合物反应。

2. 发明授权

US3734684A Flame retardant phosphorus containing fibrous products and method for production 失效
标题翻译：含阻燃产品的阻燃磷和生产方法
公开(公告)号：US3734684A
公开(公告)日：1973-05-22
申请号：US3734684D
申请日：1971-05-07
申请人： US AGRICULTURE
发明人： DONALDSON D , DAIGLE D , DRAKE G , REEVES W , BENINATE J
IPC分类号： C14C9/00 , D06M15/431 , D06M15/667 , D06M13/28
CPC分类号： C14C9/00 , D06M15/431 , D06M15/667
摘要： METHYLOL PHOSPHINE, METHYLOL PHOSPHINES IN COMBINATION WITH NITROGENOUS COMPOUNDS OR WATER SOLUBLE ADDUCTS OF THE PHOSPHINE AND NITROGENOUS COMPOUNDS ARE USED TO TREAT ORGANIC FIBROUS DERIVATIVES CONTAINING PRIMARY AND/OR SECONDARY AMINO GROUPS SUCH AS WOOL, LEATHER, NYLON AND AMINIZED COTTONS, ETC., TO PRODUCE FIBROUS DERIVATIVES WHICH ARE FLOW-, WRINKLE-, ROT- AND SHRINK-RESISTANT.

3. 发明授权

US3790639A Process for producing a water-soluble methylol phospine-phenol adduct 失效
标题翻译：生产水溶性甲基苯酚酚类添加剂的方法
公开(公告)号：US3790639A
公开(公告)日：1974-02-05
申请号：US3790639D
申请日：1972-03-28
申请人： US AGRICULTURE
发明人： DAIGLE D , DRAKE G , REEVES W
IPC分类号： C07F9/50 , C08G79/04 , C08G79/06 , D06M13/285 , D06M15/415
CPC分类号： D06M15/415 , C07F9/50 , C08G79/04 , C08G79/06 , D06M13/285 , Y10S260/24
摘要： SOLUBLE METHYLOL PHOSPHINE ADDUCTS ARE PREPARED BY REACTING TRIS(HYDROXYMETHYL)PHOSPHINE WITH SUBSTITUTED OR UNSUBSTITUTED PHENOL WHICH CONTAINS ONE OR MORE HYDROGENS ORTHO OR PARA TO THE PHENOLIC HYDROXYL GROUP. THESE ADDUCTS ARE CONVENIENT AND USEFUL FOR (A) THE PREPARATION OF FLAME RESISTANT POLYMERS AND (B) THE PREPARATION OF FLAME- AND GLOW-RESISTANT ORGANIC FIBROUS MATERIALS AND FLAME-, GLOW-, WRINKLE-, AND SHRINK-RESISTANT WOVEN AND KNIT TEXTILES WHICH CONTAN ABOUT 25% OR MORE CELLULOSIC FIBERS.

4. 发明授权

US3787360A Phosphorus containing aromatic poly-mers and process for producing flame-resistant textiles 失效
标题翻译：含有芳香族聚合物的磷酸盐及生产耐火纺织品的方法
公开(公告)号：US3787360A
公开(公告)日：1974-01-22
申请号：US3787360D
申请日：1972-03-28
申请人： US AGRICULTURE
发明人： REEVES W , DAIGLE D , DRAKE G
IPC分类号： C07F9/50 , C08G79/04 , C08G79/06 , D06M13/285 , D06M15/415 , C08G33/16
CPC分类号： D06M15/415 , C07F9/50 , C08G79/04 , C08G79/06 , D06M13/285 , Y10S260/24
摘要： SOLUBLE METHYLOL PHOSPHINE ADDUCTS ARE PREPARED BY REACTING TRIS(HYDROXYMETHYL)PHOSPHINE WITH SUBSTITUTED OR UNSUBSTITUTED PHENOL WHICH CONTAINS ONE OR MORE HYDROGENS ORTHO OR PARA TO THE PHENOLIC HYDROXYL GROUP. THESE ADDUCTS ARE CONVENIENT AND USEFUL FOR (A) THE PREPARATION OF FLAME RESISTANT POLYMERS AND (B) THE PREPARATION OF FLAME- AND GLOW -RESISTANT ORGANIC FIBROUS MATERIALS AND FLAME-, GLOW-, WRINKLE-, AND SHRINK-RESISTANT WOVEN AND KNIT TEXTILES WHICH CONTAIN ABOUT 25% OR MORE CELLULOSIC FIBERS.

5. 发明授权

US3724243A Chainless mercerizer suitable for use with liquid ammonia 失效
标题翻译：适用于液态氨的无链路适配器
公开(公告)号：US3724243A
公开(公告)日：1973-04-03
申请号：US3724243D
申请日：1971-05-07
申请人： US AGRICULTURE
发明人： COOPER A , REEVES W , CALAMARI T , SCHREIBER S
IPC分类号： D06B7/08 , B05C3/132 , D06C15/08 , D06F45/22
CPC分类号： D06B7/08
摘要： An improved chainless mercerizer utilizing a series of graduated rollers which increase the efficiency of a chainless mercerizer. Each driven roller is constructed incrementally larger in diameter than the previous driven roller in the direction of fabric travel through the mercerizer. The fabric being mercerized is stretched incrementally tighter as it is transferred from one driven roller to the next succeeding one, thereby increasing the forces opposing widthwise shrinkage. The idler rollers have a uniform diameter approximately that of any of the driven rollers.
摘要翻译：一种改进的无链丝光泽剂，利用一系列刻度滚轮，提高了无链丝光泽度的效率。每个从动辊在织物行进通过丝光器的方向上的直径比先前的从动辊的直径更大。被丝光处理的织物随着从一个从动辊转移到下一个从动辊而逐渐拉紧，从而增加了相对于宽度方向收缩的力。惰轮的直径大约等于任何从动辊的直径。

6. 发明授权

US3845107A Phosphinidynetrimethanol triacetate 失效
标题翻译：磷酸二苯乙醇三乙酸酯
公开(公告)号：US3845107A
公开(公告)日：1974-10-29
申请号：US23136072
申请日：1972-03-02
申请人： US AGRICULTURE
发明人： LANOUX S , ELLZEY S , DRAKE G , REEVES W
IPC分类号： C07F9/50 , D06M13/282 , D06M13/285 , C07C67/00
CPC分类号： D06M13/285 , C07F9/5004 , D06M13/282
摘要： 1. A PROCESS FOR PREPARING PHOSPHINIDYNETRIMETHANOL TRIACETATE, WHICH PROCESS COMPRISES; (A) REACTING ACETIC ANHYDRIDE AND TETRAKIS(HYDROXYMETHYL)PHOSPHONIUM CHLORIDE IN PYRIDINE AT ROOM TEMPERATURE BY DISSOLVING 303 GRAMS (1.59 MOLES) OF SAID TETRAKIS(hYDROXYMETHYL)PHOOSPONIUM CHLORIDE IN 1800 MILLILITERS OF PYRIDINE AT ROOM TEMPERATURE, AND SLOWLY ADDING ABOUT 727 GRAMS (7.13 MOLES) OF ACETIC ANHYDRIDE WHILE STIRRING THE REACTION MIXTURE, TO MAINTAIN A TEMPERATURE OF THE MIXTURE AT BELOW 40*C; (B) CONTINUING THE REACTION UNTIL ALL OF THE TETRAKIS(HYDROXYMETHYL)PHOSPHONIUM CHLORIDE IS CONSUMED, THE SAID ACETIC ANHYDRIDE BEING PRESENT IN EXCESS; (C) REMOVING THE PYRIDINE BY DISTILLATION UNDER VACCUM TO OBTAIN AN OILY RESIDUE; (D) WASHING THE OILY DISTILLATION RESIDUE WITH WATER TO REMOVE UNREACTED STARTING MATERIALS AND UNDESIRED WATER-SOLUBLE PRODUCTS THEREBY OBTAINING A BROWN OIL WHICH SEPARATES; (D) DRYING THE SEPRATED BROWN OIL WITH ANHYDROUS SODIUM SULFATE OR SUITABLE SUBSTITUTE DRYING AGENT THEREFOR; AND (F) DISTILLING THE PRODUCT FROM (E) UNDER VACUUM TO OBTAIN PHOSPHINIDYNETRIMETHANOL TRIACETATE, A COLORLESS PRODUCT.

7. 发明授权

US3796596A Finishing process incorporating improved catalyst systems to produce durable flameproofed cellulosic textile products with an excellent hand 失效
标题翻译：完善工艺，改进的催化剂体系，生产具有优异手感的耐用易燃纤维素纺织品
公开(公告)号：US3796596A
公开(公告)日：1974-03-12
申请号：US3796596D
申请日：1972-05-05
申请人： US AGRICULTURE
发明人： DAIGLE D , PEPPERMAN A , REEVES W , DRAKE G
IPC分类号： D06M15/431 , D06M15/667 , C09D5/18 , C09K3/28
CPC分类号： D06M15/667 , D06M15/431
摘要： IMPROVED CATALYST SYSTEMS HAVE BEEN FOUND THAT CAN BE USED IN PLACE OF THE CATALYST SYSTEMS PREVIOUSLY REQUIRED TO CURE FLAME-RETARDANT FINISHES FOR CELLULOSE TEXTILES. THESE IMPROVED CATALYST SYSTEMS CONSIST OF A MIXTURE OF ALUMINUM CHLORHYDROXIDE AND AN ACID SELECTED FROM THE GROUP PHOSPHORIC ACID, AXALIC ACID, LACTIC ACID OR A MIXTURE SELECTED FROM THE GOLLOWING: ZINC CHLORIDEGLYCOLIC ACID, MAGNESIUM CHLORIDE-CITRIC ACID, AND MAGNESIUM CHLORIDE-GLYCOLIC ACID. UNLIKE CELLULOSIC FABRICS TREATED WITH THE THP-AMIDE OR THPOH-AMIDE FINISHES WITH OR WITHOUT OTHER CATALYST SYSTEMS, FABRICS SIMILARLY PROCESSED WITH THE IMPROVED CATALYST SYSTEM, THAT IS, THE ONES CONTAINING ALUMINUM CHLORHYDROXIDE HAVE LOWER STIFFNESS VALUE AND A MUCH BETTER HAND.

8. 发明授权

US3769307A Fluoroamide-amino polymers and process for imparting oleophobic yet hydrophilic properties to fibrous materials 失效
标题翻译：氟代氨基聚合物及其制备方法将烯烃水凝胶性质转化成纤维材料
公开(公告)号：US3769307A
公开(公告)日：1973-10-30
申请号：US3769307D
申请日：1970-09-18
申请人： US AGRICULTURE
发明人： MOREAU J , DRAKE G , REEVES W
IPC分类号： C08G73/02 , D06M13/408 , D06M15/61 , C09F7/00
CPC分类号： D06M13/408 , C08G73/0213 , C08G73/0233 , D06M15/61 , D06M2101/06 , D06M2200/00 , D06M2200/11 , Y10T442/227
摘要： CERTAIN NEAT LIQUID PERFLUOROALKYL ESTERS WERE REACTED WITH CERTAIN NEAT L IQUID POLYAMINES CONTAINING A PRIMARY: SECONDARY:TERTIARY AMINE RATIO OF 1:2:1 TO PRODUCE NEW LIQUID POLYMERIC FLUOROAMIDO-AMINO COMPOUNDS. THE NEW COMPOUNDS WERE DISSOLVED IN CERTAIN SOLVENTS AND APPLIED TO COTTON FABRICS THEREBY IMPARTING TO THE TREATED FABRICS OLEOPHOBICITY WITH RETAINED HYDROPHILICITY WHICH WAS DURAABLE TO REPEATED LAUNDERING.

9. 发明授权

US3754860A Wrinkle resistance finishes for cotton fabric using citric acid derivatives for soil release 失效
标题翻译：用于土壤释放的柠檬酸衍生物的棉织物的抗皱整理
公开(公告)号：US3754860A
公开(公告)日：1973-08-28
申请号：US3754860D
申请日：1971-11-05
申请人： US AGRICULTURE
发明人： FRICK J , GAUTREAUX G , REEVES W , PIERCE A
IPC分类号： D06M15/423 , D06M15/54 , D06M15/56 , D06M15/58
CPC分类号： D06M15/423
摘要： A process for producing wrinkle-resistant cotton fabric that does not increase the difficulty of laundering; said process comprises the addition of citric acid or monoesters of citric acid to the usual finishing formulations containing a crosslinking agent for cellulose with or without a softening agent.

10. 发明授权

US3849067A Process for the mercerization of cotton fabrics with liquid ammonia and ammonia/amine solutions 失效
标题翻译：棉花织物与液氨和氨/胺解决方案的合成工艺
公开(公告)号：US3849067A
公开(公告)日：1974-11-19
申请号：US14135971
申请日：1971-05-07
申请人： US AGRICULTURE
发明人： SCHREIBER S , COOPER A , CALAMARI T , REEVES W
IPC分类号： D06M11/61 , D06M1/06 , D06M1/10
CPC分类号： D06M11/61 , D06M2101/06
摘要： Woven and knit cotton fabrics with improved strength, smooth drying appearance, dimensional stability, abrasion resistance, and hand have been produced by rapid and continuous tension mercerization with liquid ammonia using an improved chainless mercerizer.
摘要翻译：通过使用改进的无链丝光泽剂，通过液氨的快速和连续张力丝光已经产生了具有改善的强度，干燥外观，尺寸稳定性，耐磨性和手感的编织和针织棉织物。

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