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1. 发明授权

US07481988B2 Method for obtaining a high pressure acid gas stream by removal of the acid gases from a fluid stream 有权
标题翻译：通过从流体流中除去酸性气体来获得高压酸性气流的方法
公开(公告)号：US07481988B2
公开(公告)日：2009-01-27
申请号：US10595749
申请日：2004-11-05
申请人： Torsten Katz , Norbert Asprion
发明人： Torsten Katz , Norbert Asprion
IPC分类号： B01D53/48 , B01D53/50 , B01D53/52 , B01D53/54 , B01D53/62
CPC分类号： B01D53/1456 , B01D53/1425 , B01D53/1493 , C10L3/10 , C10L3/102
摘要： A method for obtaining an acid gas stream having a pressure of from 3 to 30 bar by removal of acid gases from a fluid stream containing H2S, the molar fraction of H2S based on the total amount of acid gases being at least 50 mol %, the method comprising bringing the fluid stream into intimate contact with a liquid absorption medium, thus producing a fluid stream substantially freed from acid gases and an acid-gas-loaded liquid absorption medium; separating the fluid stream and the liquid absorption medium; separating, by heating and optionally by expansion or stripping, the liquid absorption medium into an acid gas stream and a regenerated liquid absorption medium; passing the regenerated liquid absorption medium into a heat exchanger and cooling it there by using part of its thermal energy to heat up the acid-gas-loaded liquid absorption medium; and recirculating the regenerated liquid absorption medium.
摘要翻译：一种通过从含有H 2 S的流体流中除去酸性气体来获得压力为3至30巴的酸性气体流的方法，基于酸性气体的总量至少为50摩尔％的H 2 S的摩尔分数，方法包括使流体流与液体吸收介质紧密接触，从而产生基本上不含酸性气体的流体流和载有酸性气体的液体吸收介质; 分离流体物流和液体吸收介质; 通过加热和任选地通过膨胀或汽提将液体吸收介质分离成酸性气体流和再生液体吸收介质; 将再生的液体吸收介质通入热交换器中并通过使用其热能的一部分来冷却其加热含有酸性气体的液体吸收介质; 并再循环再生液体吸收介质。

2. 发明申请

US20070077188A1 Method for obtaining a high pressure acid gas stream by removal of the acid gases from a liquid stream 有权
标题翻译：通过从液体流中除去酸性气体来获得高压酸性气体流的方法
公开(公告)号：US20070077188A1
公开(公告)日：2007-04-05
申请号：US10595749
申请日：2004-11-05
申请人： Torsten Katz , Norbert Asprion
发明人： Torsten Katz , Norbert Asprion
IPC分类号： B01D53/40
CPC分类号： B01D53/1456 , B01D53/1425 , B01D53/1493 , C10L3/10 , C10L3/102
摘要： A method for obtaining an acid gas stream having a pressure of from 3 to 30 bar by removal of the acid gases from a liquid stream comprising as impurities H2S and if appropriate other acid gases, the molar fraction of H2S, based on the total amount of acid gases, being at least 50 mol %, which comprises a) in at least one absorption step, bringing the fluid stream into intimate contact with a liquid absorption medium and thus producing a fluid stream substantially freed from acid gases and an acid-gas-loaded liquid absorption medium (step a), b) separating from one another the fluid stream substantially freed from acid gases and the acid-gas-loaded liquid absorption medium (step b), c) separating, by heating and if appropriate expansion or stripping, the acid-gas-loaded liquid absorption medium into an acid gas stream having a pressure of from 3 to 30 bar and a regenerated liquid absorption medium (step c) d) passing the regenerated liquid absorption medium into a heat exchanger and cooling it there, by using a part of its thermal energy to heat up the acid-gas-loaded liquid absorption medium in step (c) (step d) e) recirculating the regenerated liquid absorption medium to step a) (step e).
摘要翻译：通过从包含作为杂质H 2 S的液体流除去酸性气体以及如果合适的其它酸性气体来获得压力为3至30巴的酸性气体流的方法，摩尔分数基于酸性气体的总量，至少50mol％，其包含a）在至少一个吸收步骤中，使流体流与液体吸收紧密接触从而产生基本上不含酸性气体和载有酸性气体的液体吸收介质的流体流（步骤a），b）将基本上不含酸性气体的流体流和带负载酸性气体的液体吸收介质（步骤b），c）通过加热和如果适当的膨胀或汽提将酸性气体负载的液体吸收介质分离成具有3至30巴的压力的酸性气体流和再生液体吸收介质（步骤 c）d）将再生的液体吸收介质送入热交换器并在其中冷却，通过使用其一部分热能来加热步骤（c）（步骤d）中的负载酸性气体的液体吸收介质（d）e）使再生液体吸收介质再循环到步骤a）（步骤 e）。

3. 发明申请

US20050288912A1 Method and apparatus for simulating mass and heat transfer-controlled separation processes 审中-公开
标题翻译：用于模拟质量传热控制分离过程的方法和装置
公开(公告)号：US20050288912A1
公开(公告)日：2005-12-29
申请号：US11202333
申请日：2005-08-12
申请人： Norbert Asprion , Christoph Grossmann , Bernd Hegner , Jurgen Ruhnke , Torsten Katz
发明人： Norbert Asprion , Christoph Grossmann , Bernd Hegner , Jurgen Ruhnke , Torsten Katz
IPC分类号： G05B17/02 , G06G7/48 , G06G7/50
CPC分类号： G05B17/02
摘要： Method of simulating mass and heat transfer-controlled separation processes using a core-film approach to describe a transfer taking place at a phase boundary (P) in which, for iteratively solving a suitable implicit differential equation system, discretisation of a transitional area (10) of the core-film approach under consideration is carried out, thereby resulting in a differential equation system.
摘要翻译：使用芯膜方法模拟质量传热控制分离过程的方法来描述在相位边界（P）处发生的转移，其中为了迭代地求解适当的隐式微分方程系统，过渡区域的离散化（10 ）进行考虑的核心膜方法，从而得到微分方程系统。

4. 发明申请

US20120070353A1 Process For Separating Off Acidic Gases By Means Of Metal-Organic Frameworks Impregnated With Amines 审中-公开
标题翻译：通过用胺浸渍的金属有机骨架分离酸性气体的方法
公开(公告)号：US20120070353A1
公开(公告)日：2012-03-22
申请号：US13257830
申请日：2010-03-18
申请人： Natalia Trukhan , Ulrich Müller , Johann-Peter Melder , Steven Brughmans , Torsten Katz
发明人： Natalia Trukhan , Ulrich Müller , Johann-Peter Melder , Steven Brughmans , Torsten Katz
IPC分类号： B01D53/40 , C09K3/00 , B01D53/56 , B01D53/52 , B01D53/62 , B01D53/50
CPC分类号： C10L3/10 , B01D53/025 , B01D53/40 , B01D53/62 , B01D2252/2023 , B01D2252/20405 , B01D2252/2041 , B01D2252/20421 , B01D2252/20426 , B01D2252/20431 , B01D2252/20436 , B01D2252/20484 , B01D2253/204 , B01D2253/25 , B01D2256/16 , B01D2256/24 , B01D2257/302 , B01D2257/304 , B01D2257/404 , B01D2257/504 , B01D2258/05 , B01D2258/06 , B01J20/226 , B01J20/2803 , B01J20/28042 , B01J20/28057 , B01J20/3007 , B01J20/3206 , B01J20/3248 , B01J20/3255 , C07F1/005 , C07F3/003 , C07F5/003 , C07F15/025 , C07F15/045 , C07F15/065 , C10L3/102 , Y02C10/08 , Y02P20/152
摘要： The present invention relates to a process for separating off at least one acidic gas from a gas mixture comprising at least one acidic gas, which comprises the step of contacting of the gas mixture with a porous metal-organic framework, where the framework adsorbs the at least one acidic gas and the framework comprises at least one at least bidentate organic compound coordinated to at least one metal ion, wherein the porous metal-organic framework is impregnated with an amine suitable for a gas scrub. The invention further provides such impregnated metal-organic frameworks.
摘要翻译：本发明涉及一种从包含至少一种酸性气体的气体混合物中分离出至少一种酸性气体的方法，该方法包括使气体混合物与多孔金属 - 有机骨架接触的步骤，其中框架吸附在至少一种酸性气体和骨架包含与至少一种金属离子配位的至少一种至少二齿的有机化合物，其中多孔金属 - 有机骨架用适于气体洗涤的胺浸渍。本发明还提供了这种浸渍的金属 - 有机骨架。

5. 发明申请

US20120067059A1 PROCESS FOR RECOVERY OF CARBON DIOXIDE FROM A FLUID STREAM, IN PARTICULAR FROM SYNGAS 有权
标题翻译：从流体流中回收二氧化碳的方法，特别是从SYNGAS
公开(公告)号：US20120067059A1
公开(公告)日：2012-03-22
申请号：US13322125
申请日：2010-05-25
申请人： Torsten Katz , Georg Sieder , Koji Tanaka
发明人： Torsten Katz , Georg Sieder , Koji Tanaka
IPC分类号： F02C6/18 , C01B3/22 , C01C1/04 , B01D53/14
CPC分类号： C10K1/08 , Y02C10/06 , Y02E20/16 , Y02E20/18 , Y02E20/185
摘要： A process for removing carbon dioxide from a fluid comprises the steps of: (a) treating the fluid by bringing it into countercurrent contact with a liquid absorbent in a first absorption zone and thereafter in a second absorption zone to absorb at least part of the carbon dioxide contained in the fluid into the absorbent; (b) depressurizing the loaded absorbent to release a first stream of carbon dioxide and yield a partially regenerated absorbent; (c) recycling a first stream of the partially regenerated absorbent into the first absorption zone; (d) heating a second stream of the partially regenerated absorbent to release a second stream of carbon dioxide and yield a regenerated absorbent; (e) recycling the regenerated absorbent into the second absorption zone; (f) condensing water vapour entrained in the second stream of carbon dioxide by cooling the second stream of carbon dioxide and transferring at least part of the heat recovered to the partially regenerated absorbent by indirect heat exchange. The invention provides a two-stage carbon dioxide recovery process wherein the overall energy required for carbon dioxide recovery is reduced and/or wherein at least part of the carbon dioxide is recovered at a pressure higher than atmospheric pressure so as to reduce the energy required for compression of the carbon dioxide, e.g., for sequestration. Also disclosed is a plant for removing carbon dioxide from a fluid.
摘要翻译：从流体中除去二氧化碳的方法包括以下步骤：（a）通过使流体与第一吸收区中的液体吸收剂逆流接触，然后在第二吸收区中以吸收至少部分碳包含在流体中的二氧化碳变成吸收剂; （b）减压负载的吸收剂以释放第一流二氧化碳并产生部分再生的吸收剂; （c）将部分再生的吸收剂的第一流再循环到第一吸收区中; （d）加热部分再生的吸收剂的第二料流以释放第二二氧化碳流并产生再生的吸收剂; （e）将再生的吸收剂再循环到第二吸收区; （f）通过冷却第二二氧化碳流将夹带在第二二氧化碳流中的水蒸汽冷凝，并通过间接热交换将至少部分回收的热量转移到部分再生的吸收剂中。本发明提供二阶段二氧化碳回收方法，其中减少二氧化碳回收所需的总能量和/或其中至少部分二氧化碳在高于大气压的压力下回收，以便减少二氧化碳回收所需的能量压缩二氧化碳，例如用于封存。还公开了一种用于从流体中除去二氧化碳的设备。

6. 发明申请

US20100186590A1 ABSORPTION MEDIUM FOR REMOVING ACID GASES WHICH COMPRISES AMINO ACID AND ACID PROMOTER 有权
标题翻译：用于去除含有氨基酸和酸性促进剂的酸性气体的吸收介质
公开(公告)号：US20100186590A1
公开(公告)日：2010-07-29
申请号：US12695601
申请日：2010-01-28
申请人： Gerald Vorberg , Torsten Katz , Georg Sieder , Christian Riemann , Rupert Wagner , Ute Lichtfers , Erika Dengler
发明人： Gerald Vorberg , Torsten Katz , Georg Sieder , Christian Riemann , Rupert Wagner , Ute Lichtfers , Erika Dengler
IPC分类号： B01D53/14 , C09K3/00
CPC分类号： B01D53/1493 , B01D53/52 , B01D53/62 , B01D2252/20494 , B01D2252/205 , B01D2256/24 , B01D2257/302 , B01D2257/306 , B01D2257/308 , B01D2257/408 , B01D2257/504 , B01D2258/06 , C10L3/10 , C10L3/102 , Y02C10/04
摘要： An absorption medium for removing acid gases from a fluid stream comprises an aqueous solution of a) of at least one metal salt of an aminocarboxylic acid, and b) of at least one acid promoter, wherein the molar ratio of b) to a) is in the range from 0.0005 to 1.0. The acid promoter is selected from mineral acids, carboxylic acids, sulfonic acids, organic phosphonic acids and partial esters thereof. The absorption medium, compared with absorption media based on amino acid salts, has a reduced regeneration energy requirement without significantly reducing the absorption capacity of the solution for acid gases. In a process for removing acid gases from the fluid stream, the fluid stream is brought into contact with the absorption medium.
摘要翻译：用于从流体流中除去酸性气体的吸收介质包含a）至少一种氨基羧酸金属盐的水溶液，和b）至少一种酸促进剂，其中b）与a）的摩尔比为在0.0005至1.0的范围内。酸促进剂选自无机酸，羧酸，磺酸，有机膦酸及其偏酯。与基于氨基酸盐的吸收介质相比，吸收介质具有降低的再生能量需求，而不显着降低酸性气体溶液的吸收能力。在从流体流中除去酸性气体的过程中，流体物流与吸收介质接触。

7. 发明授权

US08795415B2 Process for recovery of carbon dioxide from a fluid stream, in particular from syngas 有权
标题翻译：从流体流，特别是合成气回收二氧化碳的方法
公开(公告)号：US08795415B2
公开(公告)日：2014-08-05
申请号：US13322125
申请日：2010-05-25
申请人： Torsten Katz , Georg Sieder , Koji Tanaka
发明人： Torsten Katz , Georg Sieder , Koji Tanaka
IPC分类号： B01D53/14
CPC分类号： C10K1/08 , Y02C10/06 , Y02E20/16 , Y02E20/18 , Y02E20/185
摘要： A process for removing carbon dioxide from a fluid comprises the steps of: (a) treating the fluid by bringing it into countercurrent contact with a liquid absorbent in a first absorption zone and thereafter in a second absorption zone to absorb at least part of the carbon dioxide contained in the fluid into the absorbent; (b) depressurizing the loaded absorbent to release a first stream of carbon dioxide and yield a partially regenerated absorbent; (c) recycling a first stream of the partially regenerated absorbent into the first absorption zone; (d) heating a second stream of the partially regenerated absorbent to release a second stream of carbon dioxide and yield a regenerated absorbent; (e) recycling the regenerated absorbent into the second absorption zone; (f) condensing water vapor entrained in the second stream of carbon dioxide by cooling the second stream of carbon dioxide and transferring at least part of the heat recovered to the partially regenerated absorbent by indirect heat exchange. The invention provides a two-stage carbon dioxide recovery process wherein the overall energy required for carbon dioxide recovery is reduced and/or wherein at least part of the carbon dioxide is recovered at a pressure higher than atmospheric pressure so as to reduce the energy required for compression of the carbon dioxide, e.g., for sequestration. Also disclosed is a plant for removing carbon dioxide from a fluid.
摘要翻译：从流体中除去二氧化碳的方法包括以下步骤：（a）通过使流体与第一吸收区中的液体吸收剂逆流接触，然后在第二吸收区中以吸收至少部分碳包含在流体中的二氧化碳变成吸收剂; （b）减压负载的吸收剂以释放第一流二氧化碳并产生部分再生的吸收剂; （c）将部分再生的吸收剂的第一流再循环到第一吸收区中; （d）加热部分再生的吸收剂的第二料流以释放第二二氧化碳流并产生再生的吸收剂; （e）将再生的吸收剂再循环到第二吸收区; （f）通过冷却第二二氧化碳流将夹带在第二二氧化碳流中的水蒸汽冷凝，并通过间接热交换将至少部分回收的热量转移到部分再生的吸收剂中。本发明提供二阶段二氧化碳回收方法，其中减少二氧化碳回收所需的总能量和/或其中至少部分二氧化碳在高于大气压的压力下回收，以便减少二氧化碳回收所需的能量压缩二氧化碳，例如用于封存。还公开了一种用于从流体中除去二氧化碳的设备。

8. 发明申请

US20110033354A1 ABSORPTION MEDIUM FOR REMOVING ACID GASES FROM A FLUID STREAM 有权
标题翻译：用于从流体流中去除酸性气体的吸收介质
公开(公告)号：US20110033354A1
公开(公告)日：2011-02-10
申请号：US12850041
申请日：2010-08-04
申请人： Christian Riemann , Torsten Katz , Georg Sieder , Gerald Vorberg , Erika Dengler
发明人： Christian Riemann , Torsten Katz , Georg Sieder , Gerald Vorberg , Erika Dengler
IPC分类号： B01D53/40 , C09K3/00 , B01D53/14
CPC分类号： B01D53/1456 , B01D53/1487 , B01D53/1493 , B01D2257/302 , B01D2257/304 , B01D2257/306 , B01D2257/308 , B01D2257/504 , B01D2258/05 , B01D2258/06 , C12M47/18 , Y02E50/346 , Y02P20/59
摘要： An absorption medium for removing acid gases from a fluid stream comprises an aqueous solution (A) of an alkali metal salt of an N,N-di-C1-C4-alkylaminocarboxylic acid and (B) N-hydroxyethylpiperazine. The absorption medium has a low vapor pressure and an increased resistance to oxygen. Preferred fluid streams are combustion exhaust gases or biogas.
摘要翻译：用于从流体流中除去酸性气体的吸收介质包含N，N-二-C1- C4烷基氨基羧酸和（B）N-羟乙基哌嗪的碱金属盐的水溶液（A）。吸收介质具有低蒸气压和增加的耐氧性。优选的流体流是燃烧废气或沼气。

9. 发明授权

US08455693B2 Process for preparing 2-(2-tert-butylaminoethoxy)ethanol (tert-butylaminodiglycol, TBADG) 有权
标题翻译：制备2-（2-叔丁基氨基乙氧基）乙醇（叔丁基氨基二甘醇，TBADG）
公开(公告)号：US08455693B2
公开(公告)日：2013-06-04
申请号：US13112161
申请日：2011-05-20
申请人： Roland Bou Chedid , Johann-Peter Melder , Steven Brughmans , Torsten Katz
发明人： Roland Bou Chedid , Johann-Peter Melder , Steven Brughmans , Torsten Katz
IPC分类号： C07C209/16
CPC分类号： C07C213/08 , Y02P20/582 , C07C217/08
摘要： A process for preparing 2-(2-tert-butylaminoethoxy)ethanol (tert-butylaminodiglycol, TBADG) by reacting diethylene glycol (DG) with tert-butylamine (TBA) in the presence of hydrogen and of a copper catalyst, by effecting the reaction at a temperature in the range from 160 to 220° C. in the presence of a copper- and aluminum oxide-containing catalyst, where the catalytically active material of the catalyst, before the reduction thereof with hydrogen, comprises 20 to 75% by weight of aluminum oxide (Al2O3), 20 to 75% by weight of oxygen compounds of copper, calculated as CuO, and ≦5% by weight of oxygen compounds of nickel, calculated as NiO.
摘要翻译：通过在氢气和铜催化剂的存在下使二甘醇（DG）与叔丁胺（TBA）反应，通过进行反应来制备2-（2-叔丁基氨基乙氧基）乙醇（叔丁基氨基二甘醇，TBADG）在含有铜和氧化铝的催化剂的存在下，在160-220℃的温度下，催化剂的催化活性物质在用氢还原之前包含20-75重量％的氧化铝（Al 2 O 3），20〜75重量％的作为CuO计算的铜的氧化合物，和5重量％的以NiO计的镍的氧化合物。

10. 发明授权

US08269037B2 Absorption medium for removing acid gases which comprises amino acid and acid promoter 有权
标题翻译：用于除去含有氨基酸和酸促进剂的酸性气体的吸收介质
公开(公告)号：US08269037B2
公开(公告)日：2012-09-18
申请号：US12695601
申请日：2010-01-28
申请人： Gerald Vorberg , Torsten Katz , Georg Sieder , Christian Riemann , Rupert Wagner , Ute Lichtfers , Erika Dengler
发明人： Gerald Vorberg , Torsten Katz , Georg Sieder , Christian Riemann , Rupert Wagner , Ute Lichtfers , Erika Dengler
IPC分类号： C07F9/38 , C07C229/04 , B01D53/40
CPC分类号： B01D53/1493 , B01D53/52 , B01D53/62 , B01D2252/20494 , B01D2252/205 , B01D2256/24 , B01D2257/302 , B01D2257/306 , B01D2257/308 , B01D2257/408 , B01D2257/504 , B01D2258/06 , C10L3/10 , C10L3/102 , Y02C10/04
摘要： An absorption medium for removing acid gases from a fluid stream comprises an aqueous solution of a) of at least one metal salt of an aminocarboxylic acid, and b) of at least one acid promoter, wherein the molar ratio of b) to a) is in the range from 0.0005 to 1.0. The acid promoter is selected from mineral acids, carboxylic acids, sulfonic acids, organic phosphonic acids and partial esters thereof. The absorption medium, compared with absorption media based on amino acid salts, has a reduced regeneration energy requirement without significantly reducing the absorption capacity of the solution for acid gases. In a process for removing acid gases from the fluid stream, the fluid stream is brought into contact with the absorption medium.
摘要翻译：用于从流体流中除去酸性气体的吸收介质包含a）至少一种氨基羧酸金属盐的水溶液，和b）至少一种酸促进剂，其中b）与a）的摩尔比为在0.0005至1.0的范围内。酸促进剂选自无机酸，羧酸，磺酸，有机膦酸及其偏酯。与基于氨基酸盐的吸收介质相比，吸收介质具有降低的再生能量需求，而不显着降低酸性气体溶液的吸收能力。在从流体流中除去酸性气体的过程中，流体物流与吸收介质接触。

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