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1. 发明授权

US5610194A Insect repelling compositions comprising mixtures of an N-alkyl neoalkanamide and DEET 失效
标题翻译：包含N-烷基新烷酰胺和DEET的混合物的防虫组合物
公开(公告)号：US5610194A
公开(公告)日：1997-03-11
申请号：US662745
申请日：1996-06-10
申请人： Thomas G. Polefka , Pallassana Ramachandran , Robert J. Steltenkamp , Thomas F. Connors , Kevin M. Kinscherf
发明人： Thomas G. Polefka , Pallassana Ramachandran , Robert J. Steltenkamp , Thomas F. Connors , Kevin M. Kinscherf
IPC分类号： A01N37/18 , C11D1/52 , C11D3/32 , C11D3/48
CPC分类号： C11D3/48 , A01N37/18 , C11D1/521 , C11D3/32 , Y10S514/919
摘要： Insect repellent compositions are provided comprising mixtures of:(a) from about 5 to about 95%, by weight, of an N-alkyl neoalkanamide having the formula: ##STR1## wherein R.sub.1 R.sub.2, and R.sub.3 are alkyl groups and the sum of the carbon atoms therein is from 6 to 12, and wherein R.sub.4 is either a hydrogen atom or an alkyl group having one to two carbon atoms, and wherein R.sub.5 is methyl, ethyl, or propyl; and(b) from about 5 to about 95%, by weight, of N,N-diethyl-meta-toluamide (DEET).Preferred repellent composition comprise mixtures of N-methyl neodecanamide (MNDA) and DEET which provide synergistic repellency effects against a variety of insects including cockroaches, silverfish, mosquitoes, flies and ants. The repellent compositions may be applied directly to surfaces to be treated or they may be incorporated in detergent compositions such as laundry detergents, floor and wall cleaners, rug cleaners and shampoos, hair shampoos and liquid and bar soaps.
摘要翻译：提供了驱虫剂组合物，其包含以下混合物：（a）约5至约95重量％的具有下式的N-烷基新烷酰胺：其中R1R2和R3为烷基，其中碳原子为6〜12，其中R4为氢原子或碳原子数1〜2的烷基，其中R5为甲基，乙基或丙基; 和（b）约5至约95重量％的N，N-二乙基 - 间 - 甲苯甲酰胺（DEET）。优选的驱避剂组合物包括N-甲基新癸酰胺（MNDA）和DEET的混合物，其对包括蟑螂，鲶鱼，蚊子，苍蝇和蚂蚁在内的各种昆虫提供协同的排斥作用。驱避剂组合物可以直接施用于待处理的表面，或者它们可以掺入洗涤剂组合物如洗衣洗涤剂，地板和墙面清洁剂，地毯清洁剂和洗发剂，洗发剂和液体和酒吧皂中。

2. 发明授权

US5391578A N-lower alkyl neoalkanamide insect repellents 失效
标题翻译： N-低级烷基新烷酰胺驱虫剂
公开(公告)号：US5391578A
公开(公告)日：1995-02-21
申请号：US884496
申请日：1992-05-15
申请人： Robert J. Steltenkamp
发明人： Robert J. Steltenkamp
IPC分类号： A01N37/18 , A01N37/22 , A61K8/42 , A61Q17/02 , C07C233/04 , C07C233/05 , C07C233/06 , C07C233/07 , C11D1/52 , C11D3/32 , D06M13/402 , D06M16/00
CPC分类号： D06M16/00 , A01N37/18 , A01N37/22 , A61K8/42 , A61Q17/02 , C07C233/05 , C07C233/06 , C07C233/07 , C11D1/521 , C11D3/32 , D06M13/402 , Y10S514/919
摘要： N-lower alkyl neoalkanamides are liquid state isomeric mixtures. Such new compounds are mixtures of isomeric secondary amides which have insect repellent properties, being especially effective against German cockroaches. They may be applied directly to surfaces to be treated and have been found to be sufficiently substantive to such surfaces so as to impart insect repelling properties thereto.
摘要翻译： N-低级烷基新烷酰胺是液态异构体混合物。这些新化合物是具有驱虫性质的异构二级酰胺的混合物，对德国蟑螂特别有效。它们可以直接施加到待处理的表面，并且已被发现对这些表面是足够实质的，从而赋予其驱虫性能。

3. 发明授权

US5143900A Perfumes containing N-lower alkyl neoalkanamide (s) 失效
标题翻译：含有N-低级烷基新烷酰胺的香料
公开(公告)号：US5143900A
公开(公告)日：1992-09-01
申请号：US665504
申请日：1991-03-06
申请人： Robert J. Steltenkamp , Craig F. Eaton
发明人： Robert J. Steltenkamp , Craig F. Eaton
IPC分类号： A61K8/42 , A61Q13/00 , A61Q17/02 , C11D3/32 , C11D3/50
CPC分类号： C11D3/50 , A61K8/42 , A61Q13/00 , A61Q17/02 , C11D3/32 , Y10S424/10
摘要： Perfumes containing normal perfuming components, such as essential oils, esters, ethers, aldehydes, alcohols, hydrocarbons, ketones and lactones, have the fragrances thereof desirably altered, and often significantly strenghtened, by incorporation with them, as another perfuming component, of a N-lower alkyl neoalkanamide, such as ethyl neodecanamide, or a mixture of such neoalkanamides. It has been found that the neoalkanamides are of desirable fragrances, are stable, even in alkaline media, such as built detergent compositions, maintaining their fragrance notes in the perfumes and in perfumed products during comparatively lengthy storage periods, and are significantly substantive to surfaces contacted by them, even when such contact is made in relatively dilute media, such as aqueous wash water, as when ther neoalkanamide (preferably methyl- or ethyl neodecanamide) is a component of a perfume that has been employed to perfume a detergent composition. Furthermore, experimentation has indicated that the described neoalkanamides act to strengthen the fragrances of other perfuming components of the perfumes.
摘要翻译：包含正常加香成分的香料，如精油，酯，醚，醛，醇，烃，酮和内酯，其香味具有理想的改变，并经常显着增强，通过与它们相结合，作为另一种加香组分的N - 低级烷基新烷酰胺，如新癸酰基乙基乙酯，或这些新烷酰胺的混合物。已经发现，新烷酰胺是所需的香料，即使在碱性介质中也是稳定的，例如建成的洗涤剂组合物，在比较长的储存期间将香料保持在香料和香料中，并且对于所接触的表面具有显着的实质性即使当这样的接触在相对稀释的介质（例如水洗涤水）中进行时，当新烷酰胺（优选甲基或乙基新癸酰胺）是用于香料洗涤剂组合物的香料的组分时。此外，实验已经表明，所描述的新烷酰胺用于加强香料中其它加香成分的香味。

4. 发明授权

US4714559A Antistatic agents which are diamines of trialkylacetic acids and diamines 失效
标题翻译：作为三烷基乙酸和二胺的二胺的抗静电剂
公开(公告)号：US4714559A
公开(公告)日：1987-12-22
申请号：US883193
申请日：1986-07-08
申请人： Robert J. Steltenkamp , Michael A. Camara
发明人： Robert J. Steltenkamp , Michael A. Camara
IPC分类号： C08G69/02 , C08G69/26 , C11D3/37 , D06M3/30
CPC分类号： C08G69/02 , C08G69/26 , C11D3/3719
摘要： Polyamides of trialkylacetic acids and polyamines are new compounds which are of an oily nature at washing temperatures in the 10.degree. to 90.degree. C. range, are capable of being adsorbed from wash and rinse waters by fibrous material, such as laundry, of synthetic fabrics, e.g., polyesters, which laundry is susceptible to being electrostatically charged, and decrease any electrostatic charge or inhibit accumulation thereof on such materials. Such polyamides, e.g., those of neodecanoic acid and ethylene diamine or hexamethylene diamine, N,N'-ethylene-bis-neodecanoamide and N,N'-hexamethylene-bis-neodecanoamide, respectively, can be incorporated in detergent compositions, in compositions for addition to rinse waters and in compositions for application to laundry in a laundry dryer.
摘要翻译：三烷基乙酸和多胺的聚酰胺是在10至90℃范围内的洗涤温度下具有油性的新化合物，能够被纤维材料如衣物从合成织物中吸收到洗涤和冲洗水中，例如聚酯，其易于被静电带电，并且减少任何静电电荷或抑制其在这些材料上的积聚。这些聚酰胺，例如新癸酸和乙二胺或六亚甲基二胺，N，N'-亚乙基 - 双 - 新癸酰胺和N，N'-六亚甲基 - 二新癸酰胺的那些分别可以掺入洗涤剂组合物中，除了在洗衣干衣机中冲洗水和用于洗衣的组合物中。

5. 发明授权

US5525121A Dioxirane compounds useful for bleaching fabrics 失效
标题翻译：可用于漂白织物的二环系化合物
公开(公告)号：US5525121A
公开(公告)日：1996-06-11
申请号：US455178
申请日：1995-05-31
申请人： Robert J. Heffner , Robert J. Steltenkamp
发明人： Robert J. Heffner , Robert J. Steltenkamp
IPC分类号： D06L3/02 , C11D3/39 , C11D7/54 , C11D17/00 , C11D3/20 , C11D3/395
CPC分类号： C11D3/391 , C11D17/0004
摘要： Bleaching compositions comprising an inorganic peroxygen compound and a bicyclic or tricyclic diketone as an activator for the peroxygen compound. The composition preferably comprises about 1 to about 75% of the peroxygen bleaching compound and about 1 to about 75% of the bicyclic or tricyclic diketone bleaching compound activator. The conventional additives such as surfactants, antifoaming agents, fabric softeners, stabilizers, inorganic builder salts, buffers, enzymes and the like may be present as indicated. The compositions can be formulated as dry concentrated, aqueous solutions, aqueous solutions containing non-aqueous solvents, etc. The compositions are environmentally safe, effective as bleaching agents from below room temperature to higher temperatures, biodegradable and otherwise highly desirable.
摘要翻译：包含无机过氧化合物和双环或三环二酮作为过氧化合物的活化剂的漂白组合物。组合物优选包含约1至约75％的过氧漂白化合物和约1至约75％的双环或三环二酮漂白化合物活化剂。常规的添加剂如表面活性剂，消泡剂，织物柔软剂，稳定剂，无机助洗剂盐，缓冲剂，酶等可以如所指出的那样存在。组合物可以配制成干燥浓缩的水溶液，含有非水溶剂的水溶液等。该组合物是环境安全的，作为漂白剂在低于室温至较高温度下是有效的，可生物降解的和非常需要的。

6. 发明授权

US5258408A Process of repelling insects from an area by application of N-alkyl neoalkanamide insect repellent thereto 失效
标题翻译：通过施用N-烷基新烷酰胺驱虫剂从区域排斥昆虫的方法
公开(公告)号：US5258408A
公开(公告)日：1993-11-02
申请号：US685329
申请日：1991-04-15
申请人： Robert J. Steltenkamp
发明人： Robert J. Steltenkamp
IPC分类号： A01N37/18 , A61K8/42 , A61Q17/02 , C07C233/05 , C11D1/52 , C11D3/32 , D06M13/402 , D06M16/00
CPC分类号： D06M16/00 , A01N37/18 , A61K8/42 , A61Q17/02 , C07C233/05 , C11D1/521 , C11D3/32 , D06M13/402 , Y10S424/10 , Y10S514/919
摘要： N-lower alkyl neoalkanamides (N-lower alkyl trialkylacetamides of certain types) of 1 to 4 carbon atoms in the lower alkyl thereof and of 5 to 14 carbon atoms in the neoalkanoyl (or trialkylacetyl) group, e.g., N-methyl- and N-ethyl neodecanamides and N-methyl and N-ethyl neotridecanamides, are new compounds, secondary amides which have insect repellent properties, being especially effective against cockroaches, e.g., the German cockroach. However, they are also useful as repellents for other insects, including American cockroaches, mosquitoes, flies, fleas, ants, and lice. Additionally, they may repel arachnids, such as spiders, ticks and mites. The new neoalkanamides may be synthesized easily, as by reacting a primary lower alkyl amine with a neoalkanoyl halide, e.g. by reacting methyl amine or ethyl amine with neodecanoyl chloride. The most effective of the described amides for insect repellency are normally liquid and are sufficiently volatile to be detectable in air by insects. In insect repelling processes they may be applied directly to surfaces and areas to be made insect repellent or such application may be in detergent compositions of a wide variety of types, which are described in the foregoing specification, and they have been found to be substantive to the treated substrates.
摘要翻译： N-烷基新烷酰胺（某些类型的N-低级烷基三烷基乙酰胺）在其低级烷基中为1至4个碳原子，在新烷酰基（或三烷基乙酰基）中为5至14个碳原子，例如N-甲基 - 和N 乙基新癸酰胺和N-甲基和N-乙基新三酰胺是新的化合物，具有驱虫特性的次级酰胺，对蟑螂特别有效，例如德国蟑螂。然而，它们也可用作其他昆虫的驱虫剂，包括美国蟑螂，蚊子，苍蝇，跳蚤，蚂蚁和虱子。此外，它们可能排斥蛛形纲，如蜘蛛，蜱和螨。新的新烷酰胺可以容易地合成，如通过使低级烷基胺与新烷酰基卤化物反应而得到的。通过甲基胺或乙胺与新癸酰氯反应。所描述的用于驱虫剂的酰胺中最有效的通常是液体，并且具有足够的挥发性，可以通过昆虫在空气中检测到。在排斥昆虫过程中，它们可以直接施用于要被制成驱虫剂的表面和区域，或者这种应用可以在前面的说明书中描述的各种类型的洗涤剂组合物中，并且已经被发现是实质性的处理过的基材。

7. 发明授权

US4804683A N-alkyl neotridecanamide insect repellents 失效
公开(公告)号：US4804683A
公开(公告)日：1989-02-14
申请号：US71305
申请日：1987-07-16
申请人： Robert J. Steltenkamp
发明人： Robert J. Steltenkamp
IPC分类号： A01N37/18 , C11D1/52 , C11D3/32
CPC分类号： A01N37/18 , C11D1/521 , C11D3/32 , Y10S514/919
摘要： N-lower alkyl neoalkanamides of 1 to 4 carbon atoms in the lower alkyl thereof, and of 12 to 14 carbon atoms in the neoalkanoyl group, e.g., N-methyl- and N-ethyl neotridecanamides, are new compounds which have insect repellent properties, being especially effective against cockroaches, e.g., the German and American cockroaches. However, they are also useful as repellents for other insects, including mosquitoes, moths, flies, fleas, ants, and lice. Additionally, they may repel arachnids, such as spiders, ticks and mites. The new neoalkanamides may be synthesized easily, as by reacting a primary lower alkyl amine with a neoalkanoyl halide, e.g., by reacting methyl amine or ethyl amine with neotridecanoyl chloride.The most effective of the described amides for insect repellency, N-methyl neotridecanamide, is normally liquid and is sufficiently volatile to be detectable in air by insects. The neoalkanamides may be applied directly to surfaces to be treated or they may be incorporated in detergent compositions, such as laundry detergents, floor and wall cleaners, rug cleaners and shampoos, hair shampoos, and liquid and bar soaps, and have been found to be sufficiently substantive to the substrate being washed so as to impart insect repelling properties to it. They may be dissolved, dispersed or emulsified (emulsions are considered to be special cases of dispersions) in appropriate liquid media and may be applied to surfaces to be made insect repellent, as by spraying, brushing, wiping or other suitable processes, including "aerosol" spraying from pressurized containers. They have been found to be of long lasting effectiveness, with significant and measurable insect repellency being obtainable for as long as two weeks after application. The described N-lower alkyl neoalkanamides are stable during normal uses, relatively low in manufacturing cost, of high substantivities to substrates, economical to use, unobjectionable, even pleasant in ordor to humans, and safe to humans and animals, and to the environment.

8. 发明授权

US5573700A Liquid household cleaning composition with insect repellent 失效
标题翻译：具有驱虫剂的液体家用清洁组合物
公开(公告)号：US5573700A
公开(公告)日：1996-11-12
申请号：US440598
申请日：1995-05-15
申请人： Robert J. Steltenkamp , John H. Puckhaber, Jr. , Daniel Colodney , Thomas C. Hendrickson
发明人： Robert J. Steltenkamp , John H. Puckhaber, Jr. , Daniel Colodney , Thomas C. Hendrickson
IPC分类号： A01N25/02 , A01N25/30 , A01N37/18 , A01N61/00 , C07C233/05 , C11D1/22 , C11D1/52 , C11D1/72 , C11D1/83 , C11D3/20 , C11D3/32 , C11D3/48 , C11D17/00 , D06M13/402 , D06M16/00 , A01N25/00 , C11D1/00
CPC分类号： D06M16/00 , A01N25/30 , A01N37/18 , A01N61/00 , C07C233/05 , C11D1/521 , C11D1/83 , C11D17/0021 , C11D3/2048 , C11D3/32 , C11D3/48 , D06M13/402 , C11D1/22 , C11D1/72 , Y10S424/10
摘要： An aqueous liquid detergent composition is provided for cleaning a hard surface and for repelling insects therefrom comprising a detersive proportion of a surface active detergent compound, an effective amount of an insect repellent material which is sufficient to repel insect from the hard surface after application of the detergent composition thereto, the liquid detergent composition being substantially free of a liquid hydrocarbon.
摘要翻译：提供一种水性液体洗涤剂组合物，其用于清洁硬表面并用于排斥其中的昆虫，其中包含洗涤剂比例的表面活性洗涤剂化合物，有效量的驱虫剂材料，其足以在施用之后从硬表面排斥昆虫洗涤剂组合物，液体洗涤剂组合物基本上不含液体烃。

9. 发明授权

US5434190A N-aryl and N-cycloalkyl neoalkanamide insect repellents 失效
标题翻译： N-芳基和N-环烷基新烷酰胺驱虫剂
公开(公告)号：US5434190A
公开(公告)日：1995-07-18
申请号：US321379
申请日：1994-10-11
申请人： Robert J. Steltenkamp
发明人： Robert J. Steltenkamp
IPC分类号： A01N37/18 , A01N37/22 , A61K8/42 , A61Q17/02 , C07C233/00 , C07C233/05 , C07C233/06 , C07C233/07 , C11D1/52 , C11D3/32 , D06M13/402 , D06M16/00 , C07C233/57 , C07C233/58
CPC分类号： D06M16/00 , A01N37/18 , A01N37/22 , A61K8/42 , A61Q17/02 , C07C233/05 , C07C233/06 , C07C233/07 , C11D1/521 , C11D3/32 , D06M13/402 , Y10S514/919
摘要： N-monosubstituted neoalkanamides of 11 to 14 carbon atoms wherein the substituent on the amide nitrogen is cyclic (aromatic or cycloaliphatic, such as aryl or cycloalkyl) and of at least five carbon atoms, have been discovered to be insect repellent, providing that any aromatic substituent is unsubstituted at the ortho position and that when the neoalkanoyl moiety is pivaloyl the total number of carbon atoms in the N-cyclic neoalkanamide is at least 12. Such neoalkanamides are useful as repellents against cockroaches, including American, German and Oriental cockroaches, and are also effective against mosquitoes (both Anopheles and Aedes), black flies and carpenter ants, and to some extent against deer ticks. They may be applied to areas, locations and items which are desirably to be kept free of such insects, with applications being direct or of solutions or emulsions thereof, preferably by spraying, or in detergent compositions or other products to be applied to such areas, etc. Because the described neoalkanamides are desirably substantive to surfaces and are usually in liquid state, they give long lasting repellency to such areas, etc., and tests have shown them to be sufficiently long lasting.
摘要翻译：已经发现，其中酰胺氮上的取代基是环状的（芳族或脂环族基团，例如芳基或环烷基）和至少五个碳原子的具有11至14个碳原子的N-单取代的新烷酰胺胺是具有驱虫性的，条件是任何芳族取代基在邻位未被取代，当新烷酰基部分是新戊酰基时，N-环状新烷酰胺中的碳原子总数至少为12.这种新烷酰胺可用作对蟑螂的驱避剂，包括美国，德国和东方蟑螂，以及也有效对抗蚊子（按蚊和艾笛斯），黑蝇和木蚁，在某种程度上对抗鹿蜱。它们可以应用于理想地不含这种昆虫的区域，位置和物品，其应用是直接的或其溶液或乳液，优选通过喷雾，或在洗涤剂组合物或其它产品中施用于这些区域，因为所描述的新烷酰胺理想地对表面是实质的并且通常是液态的，所以它们对这些区域等提供持久的驱虫性，并且测试已经显示它们足够长的持久性。

10. 发明授权

US5182304A N-lower alkyl neodecanamide insect repellents 失效
标题翻译： N-低级烷基新癸酰胺驱虫剂
公开(公告)号：US5182304A
公开(公告)日：1993-01-26
申请号：US612747
申请日：1990-11-13
申请人： Robert J. Steltenkamp
发明人： Robert J. Steltenkamp
IPC分类号： A01N37/18 , A61K8/42 , A61Q17/02 , C07C233/05 , C11D1/52 , C11D3/32 , D06M13/402 , D06M16/00
CPC分类号： D06M16/00 , A01N37/18 , A61K8/42 , A61Q17/02 , C07C233/05 , C11D1/521 , C11D3/32 , D06M13/402 , Y10S514/919
摘要： N-lower alkyl neoalkanamides (N-lower alkyl trialkylacetamides of certain types) of 1 to 4 carbon atoms in the lower alkyl thereof and of 5 to 14 carbon atoms in the neoalkanoyl (or trialkylacetyl) group, e.g., N-methyl- and N-ethyl neodecanamides and N-methyl and N-ethyl neotridecanamides, are new compounds, secondary amides which have insect repellent properties, being especially effective against cockroaches, e.g., the German cockroach. However, they are also useful as repellents for other insects, including American cockroaches, mosquitoes, flies, fleas, ants, and lice. Additionally, they may repel arachnids, such as spiders, ticks and mites. The new neoalkanamides may be synthesized easily, as by reacting a primary lower alkyl amine with a neoalkanoyl halide, e.g. by reacting methyl amine or ethyl amine with neodecanoyl chloride.The most effective of the described amides for insect repellency are normally liquid and are sufficiently volatile to be detectable in air by insects. They may be applied directly to surfaces to be treated or they may be incorporated in detergent compositions, such as built laundry detergents, floor and wall cleaners, rug cleaners and shampoos, hair shampoos, and liquid and bar soaps, and have been found to be sufficiently substantive to the substrate being washed so as to impart insect repelling properties to it.
摘要翻译： N-烷基新烷酰胺（某些类型的N-低级烷基三烷基乙酰胺）在其低级烷基中为1至4个碳原子，在新烷酰基（或三烷基乙酰基）中为5至14个碳原子，例如N-甲基 - 和N 乙基新癸酰胺和N-甲基和N-乙基新三酰胺是新的化合物，具有驱虫特性的次级酰胺，对蟑螂特别有效，例如德国蟑螂。然而，它们也可用作其他昆虫的驱虫剂，包括美国蟑螂，蚊子，苍蝇，跳蚤，蚂蚁和虱子。此外，它们可能排斥蛛形纲，如蜘蛛，蜱和螨。新的新烷酰胺可以容易地合成，如通过使低级烷基胺与新烷酰基卤化物反应。通过甲基胺或乙胺与新癸酰氯反应。所描述的用于驱虫剂的酰胺中最有效的通常是液体，并且具有足够的挥发性，可以通过昆虫在空气中检测到。它们可以直接施加到待处理的表面上，或者它们可以并入洗涤剂组合物中，例如建成的衣物洗涤剂，地板和墙壁清洁剂，地毯清洁剂和洗发剂，洗发剂和液体和酒吧皂，并且已经被发现是对被洗涤的底物足够实质，以赋予其驱虫性能。

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