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1. 发明申请

US20110118500A1 METHOD FOR PRODUCING OPTICALLY ACTIVE a-IONONE 有权
标题翻译：用于生产光学活性α-离子的方法
公开(公告)号：US20110118500A1
公开(公告)日：2011-05-19
申请号：US13012199
申请日：2011-01-24
申请人： Tetsuya Yamamoto , Kenji Yagi , Kenya Ishida
发明人： Tetsuya Yamamoto , Kenji Yagi , Kenya Ishida
IPC分类号： C07C69/78 , C07C69/533 , C07C69/63 , C07C69/24 , C07C69/708
CPC分类号： C12P7/26 , A23L2/56 , A23L27/204 , A61K8/37 , A61Q11/00 , A61Q13/00 , C07B53/00 , C07B2200/07 , C07C403/08 , C07C403/12 , C07C403/14 , C07C2601/16 , C12G3/06 , C12P41/004
摘要： Provided that a method for inexpensively producing optically active α-ionone with a high yield and a high asymmetric yield and with good workability in a short process, and a perfume composition comprising the optically active α-ionone obtained by the aforementioned method. A method for producing optically active α-ionone, comprising allowing α-ionone as a mixture of optical isomers to react with an esterification agent, and hydrolyzing the obtained α-ionone enol ester; a method for producing optically active α-ionone comprising subjecting α-ionone as a mixture of optical isomers to an asymmetric reduction, allowing the obtained optically active α-ionol to react with an esterification agent to give an optically active α-ionol ester, hydrolyzing the obtained optically active α-ionol ester after purification as necessary, and then oxidizing the obtained optically active α-ionol; and a perfume composition comprising thus obtained optically active α-ionone.
摘要翻译：本发明提供了一种低成本地生产光学活性α-紫罗兰酮的方法，其具有高产率和高不对称产率，并且在短时间内具有良好的可加工性，以及包含通过上述方法获得的光学活性α-紫罗兰酮的香料组合物。一种光学活性α-紫罗兰酮的制造方法，其特征在于，使作为旋光异构体的混合物的α-紫罗烯酮与酯化反应，水解得到的α-紫罗烯酮烯醇酯; 一种光学活性α-紫罗兰酮的制造方法，其特征在于，将α-紫罗烯酮作为光学异构体的混合物进行不对称还原，使得所得光学活性α-离子酚与酯化反应，得到光学活性α-离子醇酯，水解根据需要纯化后得到的光学活性α-离子醇酯，然后氧化所得光学活性α-离子醇; 和包含这样得到的光学活性α-紫罗兰酮的香料组合物。

2. 发明授权

US07902404B2 Method for producing optically active α-ionone 有权
公开(公告)号：US07902404B2
公开(公告)日：2011-03-08
申请号：US11991966
申请日：2006-09-13
申请人： Tetsuya Yamamoto , Kenji Yagi , Kenya Ishida
发明人： Tetsuya Yamamoto , Kenji Yagi , Kenya Ishida
IPC分类号： C07C45/42
CPC分类号： C12P7/26 , A23L2/56 , A23L27/204 , A61K8/37 , A61Q11/00 , A61Q13/00 , C07B53/00 , C07B2200/07 , C07C403/08 , C07C403/12 , C07C403/14 , C07C2601/16 , C12G3/06 , C12P41/004
摘要： Provided that a method for inexpensively producing optically active α-ionone with a high yield and a high asymmetric yield and with good workability in a short process, and a perfume composition comprising the optically active α-ionone obtained by the aforementioned method. A method for producing optically active α-ionone, comprising allowing α-ionone as a mixture of optical isomers to react with an esterification agent, and hydrolyzing the obtained α-ionone enol ester; a method for producing optically active α-ionone comprising subjecting α-ionone as a mixture of optical isomers to an asymmetric reduction, allowing the obtained optically active α-ionol to react with an esterification agent to give an optically active α-ionol ester, hydrolyzing the obtained optically active α-ionol ester after purification as necessary, and then oxidizing the obtained optically active α-ionol; and a perfume composition comprising thus obtained optically active α-ionone.

3. 发明授权

US08053592B2 Method for producing optically active α-ionone 有权
标题翻译：光学活性α-紫罗兰酮的制造方法
公开(公告)号：US08053592B2
公开(公告)日：2011-11-08
申请号：US13012199
申请日：2011-01-24
申请人： Tetsuya Yamamoto , Kenji Yagi , Kenya Ishida
发明人： Tetsuya Yamamoto , Kenji Yagi , Kenya Ishida
IPC分类号： C07C69/78 , C07C69/533 , C07C69/63
CPC分类号： C12P7/26 , A23L2/56 , A23L27/204 , A61K8/37 , A61Q11/00 , A61Q13/00 , C07B53/00 , C07B2200/07 , C07C403/08 , C07C403/12 , C07C403/14 , C07C2601/16 , C12G3/06 , C12P41/004
摘要： Provided that a method for inexpensively producing optically active α-ionone with a high yield and a high asymmetric yield and with good workability in a short process, and a perfume composition comprising the optically active α-ionone obtained by the aforementioned method. A method for producing optically active α-ionone, comprising allowing α-ionone as a mixture of optical isomers to react with an esterification agent, and hydrolyzing the obtained α-ionone enol ester; a method for producing optically active α-ionone comprising subjecting α-ionone as a mixture of optical isomers to an asymmetric reduction, allowing the obtained optically active α-ionol to react with an esterification agent to give an optically active α-ionol ester, hydrolyzing the obtained optically active α-ionol ester after purification as necessary, and then oxidizing the obtained optically active α-ionol; and a perfume composition comprising thus obtained optically active α-ionone.
摘要翻译：本发明提供了一种低成本地生产光学活性α-紫罗兰酮的方法，其具有高产率和高不对称产率，并且在短时间内具有良好的可加工性，以及包含通过上述方法获得的光学活性α-紫罗兰酮的香料组合物。一种光学活性α-紫罗兰酮的制造方法，其特征在于，使作为旋光异构体的混合物的α-紫罗烯酮与酯化反应，水解得到的α-紫罗烯酮烯醇酯; 一种光学活性α-紫罗兰酮的制造方法，其特征在于，将α-紫罗烯酮作为光学异构体的混合物进行不对称还原，使得所得光学活性α-离子酚与酯化反应，得到光学活性α-离子醇酯，水解根据需要纯化后得到的光学活性α-离子醇酯，然后氧化所得光学活性α-离子醇; 和包含这样得到的光学活性α-紫罗兰酮的香料组合物。

4. 发明申请

US20090216039A1 Method for Producing Optically Active Alpha-Ionone 有权
标题翻译：生产光学活性α-紫罗兰酮的方法
公开(公告)号：US20090216039A1
公开(公告)日：2009-08-27
申请号：US11991966
申请日：2006-09-13
申请人： Tetsuya Yamamoto , Kenji Yagi , Kenya Ishida
发明人： Tetsuya Yamamoto , Kenji Yagi , Kenya Ishida
IPC分类号： C12P7/26 , C07C69/75 , C07C45/42
CPC分类号： C12P7/26 , A23L2/56 , A23L27/204 , A61K8/37 , A61Q11/00 , A61Q13/00 , C07B53/00 , C07B2200/07 , C07C403/08 , C07C403/12 , C07C403/14 , C07C2601/16 , C12G3/06 , C12P41/004
摘要： Provided that a method for inexpensively producing optically active α-ionone with a high yield and a high asymmetric yield and with good workability in a short process, and a perfume composition comprising the optically active α-ionone obtained by the aforementioned method. A method for producing optically active α-ionone, comprising allowing α-ionone as a mixture of optical isomers to react with an esterification agent, and hydrolyzing the obtained α-ionone enol ester; a method for producing optically active α-ionone comprising subjecting α-ionone as a mixture of optical isomers to an asymmetric reduction, allowing the obtained optically active α-ionol to react with an esterification agent to give an optically active α-ionol ester, hydrolyzing the obtained optically active α-ionol ester after purification as necessary, and then oxidizing the obtained optically active α-ionol; and a perfume composition comprising thus obtained optically active α-ionone.
摘要翻译：本发明提供了一种低成本地生产光学活性α-紫罗兰酮的方法，其具有高产率和高不对称产率，并且在短时间内具有良好的可加工性，以及包含通过上述方法获得的光学活性α-紫罗兰酮的香料组合物。一种光学活性α-紫罗兰酮的制造方法，其特征在于，使作为光学异构体的混合物的α-紫罗兰酮与酯化剂反应，水解得到的α-紫罗兰酮烯醇酯; 制备光学活性α-紫罗兰酮的方法，包括将α-紫罗烯酮作为光学异构体的混合物进行不对称还原，使得到的光学活性α-离子酚与酯化反应得到光学活性α-离子醇酯，水解根据需要纯化后得到的光学活性α-离子醇酯，然后氧化得到的光学活性α-离子醇; 和包含由此获得的光学活性α-紫罗兰酮的香料组合物。

5. 发明申请

US20080171794A1 HUMECTANT COMPOSITION 审中-公开
标题翻译：成分组成
公开(公告)号：US20080171794A1
公开(公告)日：2008-07-17
申请号：US12014925
申请日：2008-01-16
申请人： Tetsuya Yamamoto , Kenya Ishida
发明人： Tetsuya Yamamoto , Kenya Ishida
IPC分类号： A61K31/075 , A61K8/33
CPC分类号： A61K8/345 , A61Q5/00 , A61Q5/02 , A61Q5/12 , A61Q13/00 , A61Q19/00 , A61Q19/10
摘要： The present invention relates to a humectant composition containing, as component (A), at least one member selected from a menthol derivative represented by the following formula (1) and p-menthane-3,8-diol: in which R is an alkylene group having 2 to 5 carbon atoms which may be substituted with at least one member selected from the group consisting of a methyl group and a hydroxyl group, and n is an integer of 1 to 3. The humectant composition of the present invention provides an excellent moisture-retention effect.
摘要翻译：本发明涉及作为组分（A）的至少一种选自由下式（1）表示的薄荷醇衍生物和对 - 薄荷烷-3,8-二醇中的至少一种的组合物：其中R是亚烷基具有2至5个碳原子的基团，其可以被选自甲基和羟基中的至少一种取代，n是1至3的整数。本发明的保湿组合物提供优异的保湿效果。

6. 发明授权

US08846651B2 Lipid composition having excellent shape retention property and product 有权
标题翻译：脂肪组合物具有优异的形状保持性和产品
公开(公告)号：US08846651B2
公开(公告)日：2014-09-30
申请号：US12529272
申请日：2008-02-27
申请人： Kenya Ishida , Chiyomi Birou , Tetsuya Yamamoto
发明人： Kenya Ishida , Chiyomi Birou , Tetsuya Yamamoto
IPC分类号： A61K31/568 , A61Q19/00 , A24B15/10 , A61K8/18 , C11D3/20 , C09K3/00 , A61K8/63 , A23L1/30 , A24B15/30 , A61K47/28 , A23L1/226 , A61K8/34
CPC分类号： A61K47/28 , A23L27/203 , A23L33/11 , A23V2002/00 , A24B15/30 , A61K8/34 , A61K8/63 , A61Q19/00 , A23V2200/208 , A23V2250/21 , A23V2250/18
摘要： It is to provide a technique for preventing aggregation or caking of menthol at the time of its keeping. In addition, it is to provide a lipid composition, which can show excellent thermal stability even in the case of high temperature at the time of keeping menthol and at the time of blending in a product, does not cause mutual aggregation of powders, particles, flakes, pellets, sticks and the like of menthol, and can maintain its shape retention property. From 10 to 50% by mass of sterols are added to and mixed with from 50 to 90% by mass of menthol, and the resultant is melted with heating. Paraffins may be further added and mixed in an amount of 20% by mass or less, based on the lipid composition.
摘要翻译：它是提供一种防止薄荷醇保留时聚集或结块的技术。此外，提供一种脂质组合物，即使在保持薄荷醇时的高温的情况下也能显示优异的热稳定性，并且在产品中混合时，不会引起粉末，颗粒，片，丸，棒等，并能保持其形状保持性。加入10〜50质量％的甾醇并与50〜90质量％的薄荷醇混合，加热熔融。基于脂质组成，石蜡可以进一步添加并混合20质量％以下。

7. 发明授权

US08632792B2 Cooling sensation agent composition and sensory stimulation agent composition 失效
标题翻译：冷却感觉剂组合物和感觉刺激剂组合物
公开(公告)号：US08632792B2
公开(公告)日：2014-01-21
申请号：US12936160
申请日：2009-04-01
申请人： Kenya Ishida , Takashi Aida , Tetsuya Yamamoto
发明人： Kenya Ishida , Takashi Aida , Tetsuya Yamamoto
IPC分类号： A61K8/02 , A61K31/335 , A61K31/265 , A61K31/22 , A61K31/23 , A01N25/34 , A23L1/22 , A23L1/221 , C07C69/96 , C07C69/00 , C07C69/52 , C07D317/00
CPC分类号： C07D317/36 , A23L27/203 , A23L27/2052 , A61K8/0208 , A61K8/37 , A61K8/4973 , A61K2800/244 , A61Q5/02 , A61Q11/00 , A61Q13/00 , A61Q15/00 , A61Q19/00 , A61Q19/10 , C07C69/24 , C07C69/96 , C07C2601/14
摘要： A cooling sensation agent composition with a prolonged cool sensation effect is provided comprising at least one compound selected from the group consisting of aceia or ketal derivatives of 3-(1-menthoxy)propan-1,2-diol represented by Formula (1), single or mixed carbonic esters ol one or two kinds ol alcohols represented by Formula (2), and carboxylic esters represented by Formula (4). A sensory stimulation agoni composition, a flavor or fragrance composition, a beverage or food product, a perfume or cosmetic product, a toiletry product, a daily utensil product or grocery, a fiber, a fiber product, a cloth or a medicine comprising the cooling sensation agent composition; a production method thereof; a cooling processing method of a fiber, fiber product or a cloth, comprising compounding the cooling sensation agent; and new compounds are also provided.
摘要翻译：提供具有延长的凉爽感觉效果的冷却感觉剂组合物，其包含至少一种选自由式（1）表示的3-（1-薄荷氧基）丙-1,2-二醇的乙酰亚胺或缩酮衍生物，由式（2）表示的一种或两种醇类的单一或混合碳酸酯和由式（4）表示的羧酸酯。感觉刺激激动剂组合物，风味剂或香料组合物，饮料或食品，香料或化妆品，化妆品，日用具产品或杂货，纤维，纤维制品，布或包含冷却感觉剂组成; 其制造方法; 纤维，纤维制品或布的冷却处理方法，包括配合冷却感觉剂; 并提供新的化合物。

8. 发明申请

US20100093682A1 LIPID COMPOSITION HAVING EXCELLENT SHAPE RETENTION PROPERTY AND PRODUCT 有权
标题翻译：具有优异形状保持性能和产品的脂肪组合物
公开(公告)号：US20100093682A1
公开(公告)日：2010-04-15
申请号：US12529272
申请日：2008-02-27
申请人： Kenya Ishida , Chiyomi Birou , Tetsuya Yamamoto
发明人： Kenya Ishida , Chiyomi Birou , Tetsuya Yamamoto
IPC分类号： A61K31/568 , A61Q19/00 , A24B15/10 , A61K8/18 , C11D3/20 , C09K3/00
CPC分类号： A61K47/28 , A23L27/203 , A23L33/11 , A23V2002/00 , A24B15/30 , A61K8/34 , A61K8/63 , A61Q19/00 , A23V2200/208 , A23V2250/21 , A23V2250/18
摘要： It is to provide a technique for preventing aggregation or caking of menthol at the time of its keeping. In addition, it is to provide a lipid composition, which can show excellent thermal stability even in the case of high temperature at the time of keeping menthol and at the time of blending in a product, does not cause mutual aggregation of powders, particles, flakes, pellets, sticks and the like of menthol, and can maintain its shape retention property. From 10 to 50% by mass of sterols are added to and mixed with from 50 to 90% by mass of menthol, and the resultant is melted with heating. Paraffins may be further added and mixed in an amount of 20% by mass or less, based on the lipid composition.
摘要翻译：它是提供一种防止薄荷醇保留时聚集或结块的技术。此外，提供一种脂质组合物，即使在保持薄荷醇时的高温的情况下也能显示优异的热稳定性，并且在产品中混合时，不会引起粉末，颗粒，片，丸，棒等，并能保持其形状保持性。加入10〜50质量％的甾醇并与50〜90质量％的薄荷醇混合，加热熔融。基于脂质组成，石蜡可以进一步添加并混合20质量％以下。

9. 发明申请

US20110117147A1 COOLING SENSATION AGENT COMPOSITION AND SENSORY STIMULATION AGENT COMPOSITION 失效
标题翻译：冷却感觉剂组合物和感觉刺激剂组合物
公开(公告)号：US20110117147A1
公开(公告)日：2011-05-19
申请号：US12936160
申请日：2009-04-01
申请人： Kenya Ishida , Takashi Aida , Tetsuya Yamamoto
发明人： Kenya Ishida , Takashi Aida , Tetsuya Yamamoto
IPC分类号： A61K8/49 , A61K8/55 , A61Q11/00 , C07C69/96 , C07D317/22 , A61Q17/00 , A61K31/357
CPC分类号： C07D317/36 , A23L27/203 , A23L27/2052 , A61K8/0208 , A61K8/37 , A61K8/4973 , A61K2800/244 , A61Q5/02 , A61Q11/00 , A61Q13/00 , A61Q15/00 , A61Q19/00 , A61Q19/10 , C07C69/24 , C07C69/96 , C07C2601/14
摘要： The invention relates to a cooling sensation agent composition with a prolonged cool sensation effect comprising at least one compound selected from Formula (1) wherein each of A and B is a hydrogen atom or a hydrocarbon group which may have one or more substituents, in which A and B are not hydrogen atoms simultaneously, and the total number of carbon atoms in A and B is in the range of 6 to 18; and Formulae (2) to (4) wherein R1, R2, and R3 each represent a residue of an alcohol selected from 1-menthol, 1-isopulegol, 3-(1-menthoxy)propan-1,2-diol, 2-(1-menthoxy)ethan-1-ol, 3-(1-menthoxy)propan-1-ol, 2-methyl-3-(1-menthoxy)propan-1,2-diol and para-menthan-3,8-diol), and R4 represents a residue of a branched or straight-chain, cyclic or linear, or saturated or unsaturated alcohol having 6 to 18 carbon atoms that may have one or more aromatic rings that may have a condensed ring and substituent groups such as hydroxyl and ether groups; and R6 represents a hydrocarbon group having 11 to 19 carbon atoms that may be branched and contain one or more unsaturated bonds. The invention also relates to a sensory stimulation agent composition comprising the cooling sensation agent composition; a flavor or fragrance composition, a beverage or food product, a perfume or cosmetic product, a toiletry product, a daily utensil product or grocery, a fiber, a fiber product, a cloth or a medicine comprising the cooling sensation agent composition or the sensory stimulation agent composition; a production method thereof; a cooling processing method of a fiber, fiber product or a cloth, comprising compounding the cooling sensation agent composition or the sensory stimulation agent composition; and new compounds.
摘要翻译：本发明涉及具有延长的凉爽感觉效果的冷却感觉剂组合物，其包含至少一种选自式（1）的化合物，其中A和B各自为氢原子或可具有一个或多个取代基的烃基，其中 A和B不同时为氢原子，A和B中碳原子总数为6〜18; 和式（2）至（4）其中R 1，R 2和R 3各自表示选自1-薄荷醇，1-异胡耳醇，3-（1-薄荷氧基）丙-1,2-二醇，2- （1-薄荷氧基）乙-1-醇，3-（1-薄荷氧基）丙-1-醇，2-甲基-3-（1-薄荷氧基）丙-1,2-二醇和对 - 薄荷烷-3,8 - 二醇），R4代表具有6-18个碳原子的支链或直链，环状或直链或饱和或不饱和醇的残基，其可具有一个或多个可具有稠环的芳环和取代基如作为羟基和醚基团; R6表示可以具有支链并含有一个以上的不饱和键的碳原子数为11〜19的烃基。本发明还涉及包含冷却感觉剂组合物的感觉刺激剂组合物; 香料或香料组合物，饮料或食品，香水或化妆品，化妆品，日常用品或杂货，纤维，纤维制品，布或包含该冷却感觉组合物或感官的药物刺激剂组成; 其制造方法; 纤维，纤维制品或布的冷却处理方法，其包括将冷却感觉剂组合物或感觉刺激剂组合物混合; 和新化合物。

10. 发明申请

US20110077309A1 HUMECTANT COMPOSITION 审中-公开
标题翻译：成分组成
公开(公告)号：US20110077309A1
公开(公告)日：2011-03-31
申请号：US12959670
申请日：2010-12-03
申请人： Tetsuya Yamamoto , Kenya Ishida
发明人： Tetsuya Yamamoto , Kenya Ishida
IPC分类号： A61K47/42 , A61K47/10 , A61K47/14 , A61K47/22 , A61K47/36 , A61K47/46 , A61Q5/12 , A61Q19/00 , A61P17/00 , A61K8/33 , A61Q13/00
CPC分类号： A61K8/345 , A61Q5/00 , A61Q5/02 , A61Q5/12 , A61Q13/00 , A61Q19/00 , A61Q19/10
摘要： The present invention relates to a humectant composition containing, as component (A), at least one member selected from a menthol derivative represented by the following formula (1) and p-menthane-3,8-diol: in which R is an alkylene group having 2 to 5 carbon atoms which may be substituted with at least one member selected from the group consisting of a methyl group and a hydroxyl group, and n is an integer of 1 to 3. The humectant composition of the present invention provides an excellent moisture-retention effect.
摘要翻译：本发明涉及作为组分（A）的至少一种选自由下式（1）表示的薄荷醇衍生物和对 - 薄荷烷-3,8-二醇中的至少一种的组合物：其中R是亚烷基具有2至5个碳原子的基团，其可以被选自甲基和羟基中的至少一种取代，n是1至3的整数。本发明的保湿组合物提供优异的保湿效果。

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