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1. 发明授权

US5736274A Conjugated N-fluoropyridinium salt-containing polymer and use of the same 失效
标题翻译：共轭N-氟代吡啶鎓盐的聚合物及其用途
公开(公告)号：US5736274A
公开(公告)日：1998-04-07
申请号：US817794
申请日：1997-04-18
申请人： Teruo Umemoto , Kenji Adachi , Ginjiro Tomizawa , Sumi Ishihara , Masayuki Nagayoshi
发明人： Teruo Umemoto , Kenji Adachi , Ginjiro Tomizawa , Sumi Ishihara , Masayuki Nagayoshi
IPC分类号： C08F136/14 , C07B39/00 , C07D213/20 , C07D213/22 , C08G61/00 , C08G73/06 , H01M4/137 , H01M4/60 , H01M6/16 , H01M6/18 , H01M10/052 , H01M10/0565 , H01M10/08 , C07D213/89
CPC分类号： C07D213/22 , C07D213/20 , C08G73/0627 , H01M10/052 , H01M10/0565 , H01M4/137 , H01M4/60 , H01M4/608 , H01M6/181 , H01M6/183 , H01M2004/028 , H01M6/164 , H01M6/166
摘要： A polymer containing a recurring unit of a conjugated N-fluoropyridinium salt and an active material for a positive electrode, an electrolyte, a battery material for the positive electrode and a battery which use such a polymer. That polymer provides a battery material and a primary battery or a secondary battery which have high electromotive force, high energy density, high environmental acceptability, a low internal resistance in charging and discharging and strong recoverability of the electromotive force, and can be useful as a fluorinating agent.
摘要翻译： PCT No.PCT / JP95 / 02172 Sec。 371日期1997年4月18日 102（e）日期1997年4月18日PCT提交1995年10月20日PCT公布。公开号WO96 / 12702 PCT。日期1996年5月2日含有共轭N-氟吡啶鎓盐和正极活性物质，电解质，正极用电池材料和使用这种聚合物的电池的重复单元的聚合物。该聚合物提供具有高电动势，高能量密度，高环境可接受性，充放电中的低内阻和电动势的强恢复性的电池材料和一次电池或二次电池，并且可用作氟化剂。

2. 发明授权

US5892035A Process for preparing N,N'-difluorodiazoniabicycloalkane salt, intermediate therefor 失效
标题翻译：制备N，N'-二氟二氮鎓双环链烷烃盐的方法，产品和产品的用途
公开(公告)号：US5892035A
公开(公告)日：1999-04-06
申请号：US809932
申请日：1997-05-15
申请人： Teruo Umemoto , Masayuki Nagayoshi , Ginjiro Tomizawa , Kenji Adachi
发明人： Teruo Umemoto , Masayuki Nagayoshi , Ginjiro Tomizawa , Kenji Adachi
IPC分类号： C07D487/08 , C07B39/00
CPC分类号： C07D487/08
摘要： A process for preparing a N,N'-difluorodiazoniabicycloalkane salt of the formula: ##STR1## by reacting a corresponding diazabicycloalkane or diazabicycloalkane Br.o slashed.nsted acid salt and fluorine in the presence of a Br.o slashed.nsted acid or in the presene or absence of a base, by reacting a corresponding N,N'-difluorodiazoniabicycloalkane salt and an acid or salt, by reacting a corresponding diazabicycloalkane and fluorine in the presence of a Br.o slashed.nsted acid and then reacting an intermediate product and an acid or salt, or by reacting a corresponding diazabicycloalkane Br.o slashed.nsted acid salt and fluorine in the presence or absence of a base and then reacting an intermediate product and an acid or salt.
摘要翻译： PCT No.PCT / JP96 / 02183 Sec。 371日期1997年5月15日 102（e）日期1997年5月15日PCT提交1996年8月2日PCT公布。公开号WO97 / 06170 日期1997年2月20日制备下式的N，N'-二氟二氮鎓双环烷烃盐的方法：通过在Br + 526存在下，使相应的二氮杂双环链烷烃或二氮杂双环链烷Br + 526起始酸盐与氟反应苯甲酸或在预聚合或不存在碱的情况下，通过使相应的N，N'-二氟二氮鎓双环烷烃盐和酸或盐通过在Br + 526 nsted酸存在下使相应的二氮杂双环链烷烃和氟反应，然后使中间产物和酸或盐，或通过在碱的存在或不存在下使相应的二氮杂双环链烷Br + 526起始酸盐和氟反应，然后使中间产物和酸或盐反应。

3. 发明授权

US5569778A Process for preparing fluorine-containing dicarbonyl compound 失效
标题翻译：含氟二羰基化合物的制备方法
公开(公告)号：US5569778A
公开(公告)日：1996-10-29
申请号：US428133
申请日：1995-04-28
申请人： Teruo Umemoto , Ginjiro Tomizawa
发明人： Teruo Umemoto , Ginjiro Tomizawa
IPC分类号： C07B39/00 , C07C45/63 , C07C49/457 , C07C49/463 , C07C49/813 , C07C67/307 , C07C205/43 , C07C205/45 , C07C67/287
CPC分类号： C07C205/45 , C07B39/00 , C07C205/43 , C07C45/63 , C07C49/457 , C07C49/463 , C07C49/813 , C07C67/307 , C07C2101/08 , C07C2101/14
摘要： A process for preparing a fluorine-containing dicarbonyl compound of the formula: R.sup.1 COCFR.sup.2 COR.sup.3 in which R.sup.1 is a hydrogen atom, or a substituted or unsubstituted alkyl or aryl group; R.sup.2 is a hydrogen atom, a halogen atom, or a substituted or unsubstituted alkyl or aryl group; and R.sup.3 is a hydrogen atom, or a substituted or unsubstituted alkyl, aryl, alkoxy or aryloxy group, provided that at least two of R.sup.1, R.sup.2 and R.sup.3 may together form a part of a cyclic structure with or without a hetero atom, by reacting a dicarbonyl compound of the formula: R.sup.1 COCHR.sup.2 COR.sup.3 in which R.sup.1, R.sup.2 and R.sup.3 are the same as defined above with fluorine (F.sub.2) in at least one solvent selected from the group consisting of halogenated hydrocarbons having 1 to 5 carbon atoms and nitrile compounds, or in a solvent in the presence of a salt, or an acid having pKa of 6 or less.By the above process, the fluorine-containing dicarbonyl compound is industrially prepared in a high yield.
摘要翻译： PCT No.PCT / JP93 / 01584第 371日期：1995年4月28日 102（e）日期1995年4月28日PCT 1993年11月1日PCT公布。第WO94 / 10120 PCT公开日期：1994年5月11日制备下式的含氟二羰基化合物的方法：R1COCFR2COR3，其中R1是氢原子或取代或未取代的烷基或芳基; R2是氢原子，卤素原子或取代或未取代的烷基或芳基; 并且R 3是氢原子或取代或未取代的烷基，芳基，烷氧基或芳氧基，条件是R 1，R 2和R 3中的至少两个可以一起形成具有或不具有杂原子的环状结构的一部分，一种下式的二羰基化合物：R1COCHR2COR3，其中R1，R2和R3与上述定义相同，在至少一种选自碳原子数为1〜5的卤代烃和腈化合物的溶剂中使用氟（F2），或在溶剂中，在盐的存在下，或pKa为6以下的酸。通过上述方法，可以高产率工业上制备含氟二羰基化合物。

4. 发明授权

US5374732A Certain substituted N-fluoropyridiniumsulfonates 失效
标题翻译：某些取代的N-氟吡啶鎓磺酸盐
公开(公告)号：US5374732A
公开(公告)日：1994-12-20
申请号：US922372
申请日：1992-07-31
申请人： Teruo Umemoto , Ginjiro Tomizawa
发明人： Teruo Umemoto , Ginjiro Tomizawa
IPC分类号： C07B39/00 , C07C49/167 , C07D213/71 , C07D213/89 , C07J1/00 , C07D213/20
CPC分类号： C07D213/89 , C07D213/71
摘要： A substituted N-fluoropyridiniumsulfonate of the formula: ##STR1## in which R.sup.1 is a hydrogen atom, a halogen atom or a C.sub.1 -C.sub.4 alkyl or haloalkyl group, and R.sup.2 is a C.sub.1 -C.sub.4 alkyl or haloalkyl group, which is an effective fluorinating agent.
摘要翻译：具有下式的取代的N-氟代吡啶鎓磺酸盐：其中R 1是氢原子，卤素原子或C 1 -C 4烷基或卤代烷基，R 2是C 1 -C 4烷基或卤代烷基，其是有效的氟化剂。

5. 发明授权

US4996320A N-fluoropyridinium salt and process for preparing same 失效
标题翻译： N-氟吡啶鎓盐及其制备方法
公开(公告)号：US4996320A
公开(公告)日：1991-02-26
申请号：US296411
申请日：1989-01-09
申请人： Teruo Umemoto , Kyoichi Tomita , Kosuke Kawada , Ginjiro Tomizawa
发明人： Teruo Umemoto , Kyoichi Tomita , Kosuke Kawada , Ginjiro Tomizawa
IPC分类号： C07B39/00 , C07C17/093 , C07C17/12 , C07C37/62 , C07C41/22 , C07C45/30 , C07C45/51 , C07C45/54 , C07C45/63 , C07C49/167 , C07C49/457 , C07C49/463 , C07C49/693 , C07C49/697 , C07C51/363 , C07C67/307 , C07C231/12 , C07C253/30 , C07C269/06 , C07C315/04 , C07C317/44 , C07C319/20 , C07C323/03 , C07C323/09 , C07C323/52 , C07C323/59 , C07D213/89 , C07D219/02 , C07D219/04 , C07D491/04 , C07F9/58 , C07J1/00 , C07J13/00 , C07J51/00
CPC分类号： C07D213/89 , C07B39/00 , C07C17/093 , C07C17/12 , C07C231/12 , C07C253/30 , C07C269/06 , C07C309/00 , C07C315/04 , C07C319/20 , C07C37/62 , C07C41/22 , C07C45/30 , C07C45/511 , C07C45/512 , C07C45/54 , C07C45/63 , C07C49/167 , C07C49/457 , C07C49/463 , C07C49/693 , C07C49/697 , C07C51/363 , C07C67/307 , C07D219/02 , C07D491/04 , C07J1/0011 , C07J1/0022 , C07J1/0025 , C07J13/005 , C07J51/00
摘要： A pyridine-compound is reacted with fluorine together with a Bronsted acid-compound or Lewis acid to form a N-fluoropyridinium salt which is very active to other compounds but is very selective for the preparation of a desired product and this product is very useful for a fluorine-introducing agent which makes it useful for the preparation of fluoro-compounds such as thyroid inhibitor.
摘要翻译：吡啶化合物与氟与布朗斯台德酸化合物或路易斯酸一起反应以形成对其它化合物非常活泼的N-氟吡啶鎓盐，但对制备所需产物非常有选择性，该产物对于氟引入剂，其可用于制备氟化合物如甲状腺抑制剂。

6. 再颁专利

USRE35177E N-fluoropyridinium salt and process for preparing same 失效
标题翻译： N-氟吡啶鎓盐及其制备方法
公开(公告)号：USRE35177E
公开(公告)日：1996-03-12
申请号：US197711
申请日：1994-02-17
申请人： Teruo Umemoto , Kyoichi Tomita , Kosuke Kawada , Ginjiro Tomizawa
发明人： Teruo Umemoto , Kyoichi Tomita , Kosuke Kawada , Ginjiro Tomizawa
IPC分类号： C07B39/00 , C07C17/093 , C07C17/12 , C07C45/30 , C07C45/51 , C07C45/54 , C07C45/63 , C07C49/167 , C07C49/457 , C07C49/463 , C07C49/693 , C07C49/697 , C07C67/307 , C07C231/12 , C07C253/30 , C07C269/06 , C07C315/04 , C07C317/44 , C07C319/20 , C07C323/03 , C07C323/09 , C07C323/52 , C07C323/59 , C07D213/89 , C07D219/02 , C07D491/04 , C07J1/00 , C07J13/00 , C07J51/00 , C07F9/58 , C07D213/55 , C07D219/04 , C07D491/048
CPC分类号： C07D213/89 , C07B39/00 , C07C17/093 , C07C17/12 , C07C231/12 , C07C253/30 , C07C269/06 , C07C315/04 , C07C319/20 , C07C45/30 , C07C45/511 , C07C45/512 , C07C45/54 , C07C45/63 , C07C49/167 , C07C49/457 , C07C49/463 , C07C49/693 , C07C49/697 , C07C67/307 , C07D219/02 , C07D491/04 , C07J1/0011 , C07J1/0022 , C07J1/0025 , C07J13/005 , C07J51/00
摘要： A pyridine-compound is reacted with fluorine together with a .[.Bronsted.]. .Iadd.Bronsted .Iaddend.acid-compound or Lewis acid to form a N-fluoropyridinium salt which is very active to other compounds but is very selective for the preparation of a desired product and this product is very useful for a fluorine-introducing agent which makes it useful for the preparation of fluoro-compounds such as thyroid inhibitor.
摘要翻译：吡啶化合物与[Bronsted]布朗斯台德酸化合物或路易斯酸一起与氟反应，形成对其它化合物非常有活性的N-氟代吡啶鎓盐，但对制备所需产物非常有选择性，该产物是对于氟引入剂非常有用，其可用于制备氟化合物如甲状腺抑制剂。

7. 发明授权

US06855850B2 Method of manufacturing fluorine compounds, and a method of recovering or regenerating precursors of fluorinating agents 失效
标题翻译：制备氟化合物的方法，以及回收或再生氟化剂前体的方法
公开(公告)号：US06855850B2
公开(公告)日：2005-02-15
申请号：US10426726
申请日：2003-05-01
申请人： Kenji Adachi , Ginjiro Tomizawa , Satoshi Oishi
发明人： Kenji Adachi , Ginjiro Tomizawa , Satoshi Oishi
IPC分类号： C07D487/08 , C07B39/00 , C07C45/51 , C07C45/63 , C07C49/687 , C07C49/697 , C07C209/86 , C07C211/62 , C07D213/22 , C07D213/89 , C07F5/02 , C07C45/00 , C07C22/00 , C07D221/02 , C07D241/00
CPC分类号： C07C49/697 , C07B39/00 , C07C45/512
摘要： To provide a practical method of manufacturing fluorine compounds in a small number of steps that can carry out fluorination reaction of substrates using easily available fluorinating agents that can be inexpensively produced industrially, and recover precursors of the fluorinating agents generated accompanying the reaction quantitatively in an easy operation, and a method of recovery and regeneration of the precursors of the fluorinating agents.N-Fluoro-quaternary-nitrogen-onium tetrafluoroborate salts represented by the general formula (1) as the fluorinating agents are used. N-Hydro-quaternary-nitrogen-onium tetrafluoroborate salts represented by the general formula (2) generated accompanying the reaction are separated and recovered from the reaction mixture by means of depositing as crystals by the addition of solvents with a low affinity to the salts to the reaction mixture after the reaction.
摘要翻译：为了提供以少量步骤制造氟化合物的实用方法，可以使用容易得到的可在工业上廉价生产的氟化剂进行底物的氟化反应，并以容易的方式定量回收伴随反应产生的氟化剂的前体操作，以及回收和再生氟化剂前体的方法。使用由通式（1）表示的作为氟化剂的N-氟 - 季 - 氮鎓鎓四氟硼酸盐。N-水 - 季氮通过在反应后向反应混合物中加入低亲和性的溶剂沉积晶体，从反应混合物中分离并回收由通式（2）表示的四氟硼酸盐鎓盐。

8. 发明授权

US07442829B2 Fluorine-containing monomer, fluorine-containing polymer and surface treating agent 有权
标题翻译：含氟单体，含氟聚合物和表面处理剂
公开(公告)号：US07442829B2
公开(公告)日：2008-10-28
申请号：US10594148
申请日：2005-03-25
申请人： Ikuo Yamamoto , Yutaka Ohira , Yoshio Funakoshi , Shinichi Minami , Ginjiro Tomizawa
发明人： Ikuo Yamamoto , Yutaka Ohira , Yoshio Funakoshi , Shinichi Minami , Ginjiro Tomizawa
IPC分类号： A61K31/195 , C07C229/48 , C07C61/08
CPC分类号： C07C317/18 , C07C229/30 , C07C255/23 , C07C323/12 , C08F214/18 , Y10T428/23986 , Y10T442/20 , Y10T442/2287
摘要： Disclosed is a fluorine-containing polymer having: (A) a repeating unit derived from a fluorine-containing monomer which is represented by the following formula: CH2═C(—X)—C(═O)—Y—[—(CH2)m-Z-]p—(CH2)n—Rf (I) (B) a repeating unit derived from a monomer containing no fluorine atom, and if necessary (C) a repeating unit derived from a crosslinkable monomer. This fluorine containing polymer has excellent water repellency, oil repellency and antifouling property.
摘要翻译：公开了一种含氟聚合物，其具有：（A）由下式表示的含氟单体衍生的重复单元：＆lt;线内配方说明=“在线式”末端=“铅” -C（ - ） - （ - O）-Y - [ - （CH 2）2） - [ （I）<βin-line-formula description =“In-line Formulas”end =“尾”→（B）衍生自不含氟原子的单体的重复单元，必要时（C）来自交联性单体的重复单元。该含氟聚合物具有优异的防水性，拒油性和防污性。

9. 发明申请

US20070202761A1 Fluorine-Containing Monomer, Fluorine-Containing Polymer And Surface Treating Agent 有权
标题翻译：含氟单体，含氟聚合物和表面处理剂
公开(公告)号：US20070202761A1
公开(公告)日：2007-08-30
申请号：US10594148
申请日：2005-03-25
申请人： Ikuo Yamamoto , Yutaka Ohira , Yoshio Funakoshi , Shinichi Minami , Ginjiro Tomizawa
发明人： Ikuo Yamamoto , Yutaka Ohira , Yoshio Funakoshi , Shinichi Minami , Ginjiro Tomizawa
IPC分类号： B32B27/04 , C08F14/18
CPC分类号： C07C317/18 , C07C229/30 , C07C255/23 , C07C323/12 , C08F214/18 , Y10T428/23986 , Y10T442/20 , Y10T442/2287
摘要： Disclosed is a fluorine-containing polymer having: (A) a repeating unit derived from a fluorine-containing monomer which is represented by the following formula: CH2═C(-X)-C(═O)-Y-[-(CH2)m-Z-]p-(CH2)n—Rf (I) (B) a repeating unit derived from a monomer containing no fluorine atom, and if necessary (C) a repeating unit derived from a crosslinkable monomer. This fluorine containing polymer has excellent water repellency, oil repellency and antifouling property.
摘要翻译：公开了一种含氟聚合物，其具有：（A）由下式表示的含氟单体衍生的重复单元：＆lt;线内配方说明=“在线式”末端=“铅” -C（ - ） - （ - O）-Y - [ - （CH 2）2） - [ （I）<βin-line-formula description =“In-line Formulas”end =“尾”→（B）衍生自不含氟原子的单体的重复单元，必要时（C）来自交联性单体的重复单元。该含氟聚合物具有优异的防水性，拒油性和防污性。

10. 发明授权

US06787053B2 Cleaning gases and etching gases 有权
标题翻译：清洁气体和蚀刻气体
公开(公告)号：US06787053B2
公开(公告)日：2004-09-07
申请号：US10129115
申请日：2002-05-13
申请人： Akira Sekiya , Yuki Mitsui , Ginjiro Tomizawa , Katsuya Fukae , Yutaka Ohira , Taisuke Yonemura
发明人： Akira Sekiya , Yuki Mitsui , Ginjiro Tomizawa , Katsuya Fukae , Yutaka Ohira , Taisuke Yonemura
IPC分类号： C03C1500
CPC分类号： C23C16/4405 , H01L21/3065 , H01L21/31116 , Y02C20/30 , Y02P70/605
摘要： The first chamber cleaning gas and the first silicon-containing film-etching gas of the present invention comprise at least one compound selected from the group consisting of FCOF, CF3OCOF and CF3OCF2OCOF, and O2 in the specific amount, and optionally other gases. The second chamber cleaning gas and the second silicon-containing film-etching gas comprise CF3COF, C3F7COF or CF2(COF)2 and O2 in specific amounts, and optionally may comprise other gases. The chamber cleaning gases and silicon-containing film etching gases of the present invention have a low global warming potential and hardly generate substances in the exhaust gases such as CF4, etc, which are harmful to the environment and have been perceived as contributing to global warming. Therefore, the gases are friendly to the global environment, and have easy handling and excellent exhaust gas treating properties. Further, the chamber cleaning gases of the invention have excellent cleaning rate.
摘要翻译：本发明的第一室清洁气体和第一含硅膜蚀刻气体包含至少一种选自FCOF，CF 3 OCOF和CF 3 OCF 2 COOF的化合物，以及特定量的O 2和任选的其它气体。第二室清洁气体和第二含硅膜蚀刻气体包含CF 3 COF，C 3 F 7 COF或CF 2（COF）2和特定量的O 2，并且任选地可以包含其它气体。本发明的室清洁气体和含硅膜蚀刻气体具有低的全球变暖潜能，并且几乎不产生对环境有害并被认为有助于全球变暖的CF4等废气中的物质。因此，气体对于全球环境友好，具有易于处理和优异的废气处理性能。此外，本发明的室清洁气体具有优异的清洗率。

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