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1. 发明授权

US5439744A Composite bodies and methods for making same 失效
标题翻译：复合体及其制作方法
公开(公告)号：US5439744A
公开(公告)日：1995-08-08
申请号：US979853
申请日：1993-02-25
申请人： Terry D. Claar , Vilupanur A. Ravi , Philip J. Roach
发明人： Terry D. Claar , Vilupanur A. Ravi , Philip J. Roach
IPC分类号： C04B35/65 , C04B41/50 , C23C10/08 , C04B35/58
CPC分类号： C04B41/5053 , C04B35/652 , C23C10/08 , Y10T428/30 , Y10T428/31678
摘要： This invention relates generally to a novel directed metal oxidation process which is utilized to produce self-supporting bodies. In some of the more specific aspects of the invention, a parent metal (e.g., a parent metal vapor) is induced to react with at least one solid oxidant-containing material to result in the directed growth of a reaction product which is formed from a reaction between the parent metal and the solid oxidant-containing material. The inventive process can be utilized to form bodies having substantially homogeneous compositions, graded compositions, and macrocomposite bodies.
摘要翻译： PCT No.PCT / US91 / 04762 Sec。 371日期：1993年2月25日 102（e）日期1993年2月25日PCT 1991年6月25日提交PCT本发明一般涉及一种用于生产自支撑体的新型定向金属氧化方法。在本发明的一些更具体的方面中，诱导母体金属（例如母体金属蒸汽）与至少一种含固体氧化剂的材料反应，导致反应产物的直接生长，所述反应产物由母体金属和含固体氧化剂的材料之间的反应。本发明的方法可以用于形成具有基本上均匀的组合物，分级组合物和大复合体的本体。

2. 发明授权

US5277933A Method for forming a self-supporting body using vapor-phase parent metals and solid oxidants 失效
标题翻译：使用气相母体金属和固体氧化剂形成自支撑体的方法
公开(公告)号：US5277933A
公开(公告)日：1994-01-11
申请号：US812775
申请日：1991-12-23
申请人： Terry D. Claar , Vilupanur A. Ravi , Philip J. Roach
发明人： Terry D. Claar , Vilupanur A. Ravi , Philip J. Roach
IPC分类号： C04B35/65 , C04B41/50 , C04B41/87 , C04B41/88 , C23C10/06 , C23C10/08 , C23C10/16 , C23C16/00
CPC分类号： C04B41/87 , C04B35/652 , C04B41/5053 , C04B41/5057 , C23C10/08 , C23C10/16
摘要： This invention relates generally to a novel directed metal oxidation process which is utilized to produce self-supporting bodies. In some of the more specific aspects of the invention, a parent metal (e.g., a parent metal vapor) is induced to react with at least one solid oxidant-containing material to result in the directed growth of a reaction product which is formed from a reaction between the parent metal and the solid oxidant-containing material. The inventive process can be utilized to form bodies having substantially homogeneous compositions, graded compositions, and macrocomposite bodies.
摘要翻译：本发明一般涉及用于生产自支撑体的新颖的定向金属氧化方法。在本发明的一些更具体的方面中，诱导母体金属（例如母体金属蒸汽）与至少一种含固体氧化剂的材料反应，导致反应产物的直接生长，所述反应产物由母体金属和含固体氧化剂的材料之间的反应。本发明的方法可以用于形成具有基本上均匀的组合物，分级组合物和大复合体的本体。

3. 发明授权

US5242710A Methods for making self-supporting composite bodies and articles produced thereby 失效
标题翻译：制造自支撑复合体及其制品的方法
公开(公告)号：US5242710A
公开(公告)日：1993-09-07
申请号：US880479
申请日：1992-05-06
申请人： Terry D. Claar , Vilupanur A. Ravi , Philip J. Roach
发明人： Terry D. Claar , Vilupanur A. Ravi , Philip J. Roach
IPC分类号： C04B35/65 , C04B41/50 , C04B41/87 , C23C10/08 , C23C10/16
CPC分类号： C04B41/87 , C04B35/652 , C04B41/5053 , C04B41/5057 , C23C10/08 , C23C10/16 , Y10S427/103
摘要： This invention relates generally to a novel directed metal oxidation process which is utilized to produce self-supporting bodies. In some of the more specific aspects of the invention, a parent metal vapor is induced to react with a solid oxidant to result in the directed growth of a reaction product which is formed from a reaction between the parent metal vapor and the solid oxidant. The inventive process can be utilized to form bodies having substantially homogeneous compositions, graded compositions, and macrocomposite bodies.
摘要翻译：本发明一般涉及用于生产自支撑体的新颖的定向金属氧化方法。在本发明的一些更具体的方面，诱导母体金属蒸气与固体氧化剂反应，导致由母体金属蒸气和固体氧化剂之间的反应形成的反应产物的定向生长。本发明的方法可以用于形成具有基本上均匀的组合物，分级组合物和大复合体的本体。

4. 发明授权

US5403790A Additives for property modification in ceramic composite bodies 失效
标题翻译：陶瓷复合材料的改性添加剂
公开(公告)号：US5403790A
公开(公告)日：1995-04-04
申请号：US960407
申请日：1993-01-11
申请人： Terry D. Claar , Gerhard H. Schiroky , Kevin P. Pochopien , Vilupanur A. Ravi , James C. Wang , Ratnesh K. Dwivedi
发明人： Terry D. Claar , Gerhard H. Schiroky , Kevin P. Pochopien , Vilupanur A. Ravi , James C. Wang , Ratnesh K. Dwivedi
IPC分类号： C04B35/56 , C04B35/58 , C04B35/65 , C04B41/50 , C04B41/87 , C22C29/00 , C22C29/06 , B22F3/26
CPC分类号： C04B35/563 , C04B35/5622 , C04B35/58078 , C04B35/65 , C04B35/652 , C04B41/5062 , C04B41/87 , C22C29/00 , C22C29/06 , C22C29/062
摘要： This invention relates generally to a novel method of manufacturing a composite body. More particularly, the present invention relates to a method for modifying the resultant properties of a composite body, by, for example, minimizing the amount of porosity present in the composite body. Moreover, additives, whether used alone or in combination, (1) can be admixed with the permeable mass, (2) can be mixed or alloyed with the parent metal, (3) can be placed at an interface between the parent metal and the preform or mass of filler material, (4) or any combination of the aforementioned methods, to modify properties of the resultant composite body. Particularly, additives such as VC, NbC, WC, W.sub.2 B.sub.5, TaC, ZrC, ZrB.sub.2, SiB.sub.6, SiC, MgO, Al.sub.2 O.sub.3, ZrO.sub.2, CeO.sub.2, Y.sub.2 O.sub.3, La.sub.2 O.sub.3, MgAl.sub.2 O.sub.4, HfO.sub.2, ZrSiO.sub.4, Yb.sub.2 O.sub.3 and Mo.sub.2 B.sub.5 can be combined with the permeable mass in an amount of about 5-50 percent by weight, prior to reactively infiltrating the permeable mass. Moreover, an additive may also include substantially pure elemental metals (e.g., Nb, Ti, Hf, V, Ta, Cr, Mo, Al, Cr, Si, Co and W) which may be provided by any of the methods discussed above herein.
摘要翻译： PCT No.PCT / US91 / 04951 Sec。 371日期：1993年1月11日 102（e）日期1993年1月11日PCT PCT 1991年7月12日PCT公布。公开号WO92 / 00933 日本1992年1月23日。本发明一般涉及一种制造复合体的新方法。更具体地说，本发明涉及通过例如最小化复合体中存在的孔隙率来改变复合体的合成性能的方法。此外，无论单独使用还是组合使用，添加剂（1）均可与可渗透物质混合，（2）可与母体金属混合或合金化，（3）可置于母体金属与母体金属之间的界面处填充材料的预制件或质量，（4）或上述方法的任何组合，以改变所得复合材料的性能。特别地，可以将诸如VC，NbC，WC，W2B5，TaC，ZrC，ZrB2，SiB6，SiC，MgO，Al2O3，ZrO2，CeO2，Y2O3，La2O3，MgAl2O4，HfO2，ZrSiO4，Yb2O3和Mo2B5的添加剂与渗透性在反应性渗透可渗透物质之前，其质量为约5-50重量％。此外，添加剂还可以包括可以通过上述任何方法提供的基本上纯的元素金属（例如，Nb，Ti，Hf，V，Ta，Cr，Mo，Al，Cr，Si，Co和W）。

5. 发明授权

US5400947A Joining methods for ceramic composite bodies 失效
标题翻译：陶瓷复合体的接合方法
公开(公告)号：US5400947A
公开(公告)日：1995-03-28
申请号：US960406
申请日：1993-01-11
申请人： James C.-K. Wang , Terry D. Claar , Philip J. Roach , Gerhard H. Schiroky
发明人： James C.-K. Wang , Terry D. Claar , Philip J. Roach , Gerhard H. Schiroky
IPC分类号： C04B35/65 , C04B37/00 , C04B37/02 , B23K103/16
CPC分类号： C04B37/021 , C04B35/652 , C04B37/001 , C04B37/006 , C04B37/026 , C04B2235/6562 , C04B2235/6581 , C04B2237/124 , C04B2237/125 , C04B2237/127 , C04B2237/36 , C04B2237/403 , C04B2237/406 , C04B2237/50 , C04B2237/568 , C04B2237/60 , C04B2237/61 , C04B2237/704 , C04B2237/708 , C04B2237/72 , C04B2237/76 , C04B2237/765 , C04B2237/82 , Y10T29/49988
摘要： This invention relates generally to a novel method for joining at least one first self-supporting body to at least one second self-supporting body which is similar in composition to or different in composition from said at least one first self-supporting body and to novel products which result from such joining. In some of its more specific aspects, this invention relates to different techniques for joining ceramic matrix composite bodies to other ceramic matrix composite bodies of similar characteristics and for joining ceramic matrix composite bodies to bodies which have different characteristics (e.g., metals). The ceramic matrix composite bodies of this invention are produced by a reactive infiltration of a molten parent metal into a bed or mass containing at least one of a boron source material, a carbon source material, and a nitrogen source material and, optionally, one or more inert fillers.
摘要翻译： PCT No.PCT / US91 / 04956 Sec。 371日期：1993年1月11日 102（e）日期1993年1月11日PCT 1991年1月11日PCT申请。本发明总体上涉及一种将至少一个第一自支撑体连接到至少一个第二自支撑体的新方法，该第二自支撑体的组成类似与所述至少一个第一自支撑体的组成或组成不同，以及由这种连接产生的新产品。在其一些更具体的方面，本发明涉及将陶瓷基质复合体与其它具有相似特性的陶瓷基体复合体接合并将陶瓷基体复合体与具有不同特性（例如金属）的体接合的不同技术。本发明的陶瓷基质复合体是通过将熔融母体金属反应性渗入含有硼源材料，碳源材料和氮源材料中的至少一种的床或物质而产生的，以及任选的一种或更多的惰性填料。

6. 发明授权

US5133494A Method for joining ceramic composite bodies and articles formed thereby 失效
标题翻译：陶瓷复合体和由此形成的制品的接合方法
公开(公告)号：US5133494A
公开(公告)日：1992-07-28
申请号：US803709
申请日：1991-12-04
申请人： James C. Wang , Terry D. Claar , Philip J. Roach
发明人： James C. Wang , Terry D. Claar , Philip J. Roach
IPC分类号： C04B35/65 , C04B37/00 , C04B37/02
CPC分类号： C04B37/026 , C04B35/652 , C04B37/001 , C04B37/006 , C04B37/021 , C04B2235/6562 , C04B2235/6581 , C04B2237/124 , C04B2237/125 , C04B2237/127 , C04B2237/36 , C04B2237/40 , C04B2237/402 , C04B2237/403 , C04B2237/406 , C04B2237/50 , C04B2237/56 , C04B2237/60 , C04B2237/61 , C04B2237/704 , C04B2237/708 , C04B2237/72 , C04B2237/76 , C04B2237/765 , C04B2237/82
摘要： This invention relates generally to a novel method for joining at least one first self-supporting body, to at least one second self-supporting body which is similar in composition to or different in composition from said at least one first self-supporting body and to novel products which result from such joining. In some of its more specific aspects, this invention relates to different techniques for joining ceramic matrix composite bodies to other ceramic matrix composite bodies of similar characteristics and for joining ceramic matrix composite bodies to bodies which have different characteristics (e.g., metals). The ceramic matrix composite bodies of this invention are produced by a reactive infiltration of a molten parent metal into a bed or mass containing a boron source material and a carbon source material (e.g., boron carbide) and/or a boron source material and a nitrogen source material (e.g., boron nitride) and, optionally, one or more inert fillers.
摘要翻译：本发明一般涉及将至少一个第一自支撑体与至少一个与所述至少一个第一自支撑体的组成相似或不同的至少一个第二自支撑体接合的新方法，以及这种加入产生的新产品。在其一些更具体的方面，本发明涉及将陶瓷基质复合体与其它具有相似特性的陶瓷基体复合体接合并将陶瓷基体复合体与具有不同特性（例如金属）的体接合的不同技术。本发明的陶瓷基体复合体是通过将熔融母体金属反应性浸入含有硼源材料和碳源材料（例如碳化硼）和/或硼源材料和氮源材料（例如，氮化硼）和任选的一种或多种惰性填料。

7. 发明授权

US5437833A Method of modifying ceramic composite bodies by a post-treatment process and articles produced thereby 失效
公开(公告)号：US5437833A
公开(公告)日：1995-08-01
申请号：US218386
申请日：1994-03-25
申请人： Terry D. Claar , Gerhard H. Schiroky , William B. Johnson
发明人： Terry D. Claar , Gerhard H. Schiroky , William B. Johnson
IPC分类号： C04B35/65 , C04B41/50 , C04B41/87 , C22C29/00 , B22F7/02 , C04B35/56 , C04B35/58 , C04B35/653
CPC分类号： C04B41/009 , C04B35/652 , C04B41/5062 , C04B41/87 , C22C29/00
摘要： This invention relates generally to a novel method of manufacturing a composite body, such as a ZrB.sub.2 --ZrC--Zr (optional) composite body, by utilizing a post-treatment process and to the novel products made thereby. More particularly, the invention relates to a method of modifying a composite body comprising one or more boron-containing compounds (e.g., a boride or a boride and a carbide) which has been made by the reactive infiltration of a molten parent metal into a bed or mass containing boron carbide, and optionally one or more inert fillers, to form the body.

8. 发明授权

US4512388A High-temperature direct-contact thermal energy storage using phase-change media 失效
标题翻译：使用相变介质的高温直接接触式热能储存
公开(公告)号：US4512388A
公开(公告)日：1985-04-23
申请号：US506030
申请日：1983-06-20
申请人： Terry D. Claar , Randy J. Petri
发明人： Terry D. Claar , Randy J. Petri
IPC分类号： C09K5/06 , F28D20/02 , F24H7/04 , F28D17/00 , F28F23/00
CPC分类号： F28D20/023 , C09K5/063 , Y02E60/145 , Y02E70/30 , Y02P20/13 , Y10T428/2982 , Y10T428/2991 , Y10T428/2993
摘要： A high-temperature direct-contact thermal energy storage element for use in a system for storage and retrieval of thermal energy in the range of about 400.degree. to about 3000.degree. F. The thermal energy is directly stored, without heat exchange tubes in composite latent/sensible heat thermal energy storage media utilizing the heat of fusion and high-temperature stability of alkaline metal and alkaline earth carbonates, chlorides, nitrates, nitrites, fluorides, hydroxides and sulfates and metal, metallic alloys and mixtures thereof maintained within a porous support-structure material which itself is capable of storage as sensible heat. The thermal energy storage according to the invention may be effectively utilized for storage of thermal energy derived from solar, industrial waste, process heat, and high-temperature gas reactor energy sources and retrieved for a wide variety of uses such as combustion air preheating, drying, space heating, heating of process gases, power generating heat engines and the like.
摘要翻译：一种高温直接接触式热能储存元件，用于在约400°至约3000°F范围内储存和回收热能的系统中。热能直接储存，无复合潜热的换热管使用熔融热和碱金属和碱土金属碳酸盐，氯化物，硝酸盐，亚硝酸盐，氟化物，氢氧化物和硫酸盐的金属，金属合金及其混合物的热敏热存储介质，其保持在多孔载体 - 结构材料本身能够作为显热存储。根据本发明的热能储存可以有效地用于储存源自太阳能，工业废物，工艺热和高温气体反应堆能源的热能，并且可用于多种用途，如燃烧空气预热，干燥，空间加热，工艺气体的加热，发电热机等。

9. 发明授权

US5296419A Self-supporting composite bodies 失效
标题翻译：自支撑复合体
公开(公告)号：US5296419A
公开(公告)日：1994-03-22
申请号：US16629
申请日：1993-02-12
申请人： Danny R. White , Terry D. Claar
发明人： Danny R. White , Terry D. Claar
IPC分类号： C04B35/583 , C04B35/58 , C04B35/65 , C22C1/10
CPC分类号： C04B35/653 , C04B35/58007 , C04B35/58014 , C04B35/58028 , C04B35/5805 , C04B35/58064 , C04B35/58071 , C04B35/58078 , C04B35/581 , C04B35/584 , C04B35/632 , C04B35/652 , Y10T428/12007
摘要： Self-supporting bodies are produced by reactive infiltration of a parent metal into a boron nitride material typically resulting in a body comprising a boron-containing compound, a nitrogen-containing compound and metal. The mass to be infiltrated may contain one or more inert fillers admixed with the boron nitride, to produce a composite by reactive infiltration, which composite comprises a matrix which embeds the filler material. The matrix, in a composite body containing filler material, comprises one or more of metal, a boron-containing compound and a nitrogen-containing compound. The relative amounts of reactants and process conditions may be altered or controlled to yield a body containing varying volume percents of ceramic, metal and/or porosity. The mass to be infiltrated can be contained within a refractory vessel having a venting means included therein.
摘要翻译：通过将母体金属反应性渗透到氮化硼材料中而产生自支撑体，通常产生包含含硼化合物，含氮化合物和金属的体。待渗透的物质可以包含一种或多种与氮化硼混合的惰性填料，以通过反应性渗透产生复合材料，该复合材料包括嵌入填料的基质。含有填料的复合体中的基体包含一种或多种金属，含硼化合物和含氮化合物。可以改变或控制反应物和工艺条件的相对量，以产生包含不同体积百分比的陶瓷，金属和/或孔隙的体。待渗透的物质可以包含在其中包括排气装置的耐火容器中。

10. 发明授权

US5275982A Method of modifying ceramic composite bodies by a post-treatment process and articles produced thereby 失效
标题翻译：通过后处理工艺改变陶瓷复合体的方法和由此制备的制品
公开(公告)号：US5275982A
公开(公告)日：1994-01-04
申请号：US948188
申请日：1992-09-21
申请人： Terry D. Claar , William B. Johnson , Robert A. Rapp
发明人： Terry D. Claar , William B. Johnson , Robert A. Rapp
IPC分类号： C04B35/58 , C04B35/65 , C04B41/50 , C04B41/51 , C04B35/10
CPC分类号： C04B35/58064 , C04B35/5607 , C04B35/652 , C04B35/653 , C04B41/5053 , C04B41/51
摘要： The present invention relates to a novel method of manufacturing a composite body, such as a ZrB.sub.2 --ZrC--Zr composite body, by utilizing a post-treatment technique which may improve the oxidation resistance of the composite body. Moreover, the invention relates to novel products made according to the process. The novel process modifies at least a portion of a composite body by exposing said body to a source of second metal.
摘要翻译：本发明涉及通过利用可以提高复合体的抗氧化性的后处理技术来制造复合体如ZrB2-ZrC-Zr复合体的新方法。此外，本发明涉及根据该方法制备的新产品。该新颖工艺通过将所述主体暴露于第二金属源来修饰复合体的至少一部分。

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