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1. 发明申请

US20090023923A1 1,3-Bis(Substituted Phenyl)-3-Hydroxypropan-1-One or 2-Propen-1-One Compound, and Salt Thereof 有权
标题翻译： 1,3-二（取代苯基）-3-羟基丙-1-酮或2-丙烯-1-酮化合物及其盐
公开(公告)号：US20090023923A1
公开(公告)日：2009-01-22
申请号：US12087019
申请日：2006-12-25
申请人： Takashi Mizukoshi , Yasuhiro Sakurai , Kazutaka Matoba , Manabu Yaosaka
发明人： Takashi Mizukoshi , Yasuhiro Sakurai , Kazutaka Matoba , Manabu Yaosaka
IPC分类号： C07D239/24 , C07C49/303 , C07C69/76 , C07C233/01 , C07D307/02 , C07C63/06 , C07D213/02
CPC分类号： C07C69/76 , C07C49/813 , C07C49/83 , C07C49/835 , C07C49/84 , C07C65/38 , C07C205/45 , C07C235/84 , C07C237/22 , C07C243/38 , C07C255/56 , C07C257/20 , C07C271/28 , C07C271/64 , C07D213/40 , C07D239/42 , C07D277/28 , C07D307/16
摘要： There is provided a novel process intermediate represented by the general formula (1) or (2): (where, X represents halogen atom, cyano group or the like, Y represents halogen atom, cyano group or the like, R1 represents C1-C6 haloalkyl group or C3-C8 halocycloalkyl group, R2 represents methyl group, halogen atom, cyano group or the like, m represents an integer of 1 to 5, and n represents an integer of 1 to 4).
摘要翻译：提供了由通式（1）或（2）表示的新型加工中间体：（其中，X表示卤素原子，氰基等，Y表示卤素原子，氰基等，R1表示C1-C6 卤代烷基或C 3 -C 8卤代环烷基，R 2表示甲基，卤素原子，氰基等，m表示1〜5的整数，n表示1〜4的整数。

2. 发明授权

US07700808B2 1-3-bis(substituted phenyl)-3-hydroxypropan-1-one or 2-propen-1-one compound, and salt thereof 有权
标题翻译：（取代的苯基）-3-羟基丙-1-酮或2-丙烯-1-酮化合物及其盐
公开(公告)号：US07700808B2
公开(公告)日：2010-04-20
申请号：US12087019
申请日：2006-12-25
申请人： Takashi Mizukoshi , Yasuhiro Sakurai , Kazutaka Matoba , Manabu Yaosaka
发明人： Takashi Mizukoshi , Yasuhiro Sakurai , Kazutaka Matoba , Manabu Yaosaka
IPC分类号： C07C49/303 , C07C69/76 , C07C233/00 , C07C63/06 , C07D239/24 , C07D307/02 , C07D213/02
CPC分类号： C07C69/76 , C07C49/813 , C07C49/83 , C07C49/835 , C07C49/84 , C07C65/38 , C07C205/45 , C07C235/84 , C07C237/22 , C07C243/38 , C07C255/56 , C07C257/20 , C07C271/28 , C07C271/64 , C07D213/40 , C07D239/42 , C07D277/28 , C07D307/16
摘要： There is provided a novel process intermediate represented by the general formula (1) or (2): (where, X represents halogen atom, cyano group or the like, Y represents halogen atom, cyano group or the like, R1 represents C1-C6 haloalkyl group or C3-C8 halocycloalkyl group, R2 represents methyl group, halogen atom, cyano group or the like, m represents an integer of 1 to 5, and n represents an integer of 1 to 4).
摘要翻译：提供了由通式（1）或（2）表示的新型加工中间体：（其中，X表示卤素原子，氰基等，Y表示卤素原子，氰基等，R1表示C1-C6 卤代烷基或C 3 -C 8卤代环烷基，R 2表示甲基，卤素原子，氰基等，m表示1〜5的整数，n表示1〜4的整数。

3. 发明申请

US20100137612A1 METHOD FOR PRODUCTION OF 3-HYDROXYPROPAN-1-ONE COMPOUND FOR PRODUCTION OF 2- PROPEN-1-ONE COMPOUND AND METHOD FOR PRODUCTION OF ISOXAZLINE COMPOUND 有权
标题翻译：用于生产2-丙烯-1-酮化合物的3-羟基丙-1-酮化合物的生产方法和生产ISOXAZLINE化合物的方法
公开(公告)号：US20100137612A1
公开(公告)日：2010-06-03
申请号：US12452347
申请日：2008-06-27
申请人： Manabu Yaosaka , Tomohisa Utsunomiya , Yuji Moriyama , Tomohiro Matsumoto , Kazutaka Matoba
发明人： Manabu Yaosaka , Tomohisa Utsunomiya , Yuji Moriyama , Tomohiro Matsumoto , Kazutaka Matoba
IPC分类号： C07D261/04 , C07C63/06 , C07C45/61
CPC分类号： C07C45/72 , C07C45/66 , C07C45/74 , C07C49/83 , C07C49/835 , C07C51/353 , C07C51/367 , C07C51/377 , C07C65/40 , C07C67/327 , C07C67/343 , C07C67/347 , C07C69/65 , C07C231/12 , C07C253/30 , C07C319/20 , C07D213/30 , C07D213/50 , C07D213/61 , C07D233/14 , C07D249/08 , C07D261/04 , C07D401/04 , C07C323/22 , C07C235/84 , C07C255/56 , C07C69/76 , C07C49/813 , C07C65/38
摘要： There is provided a novel intermediate for producing pesticides. A method for producing 1,3-bis(substituted phenyl)-3-substituted-3-hydroxypropan-1-one compound of Formula (3) comprises reacting an aromatic ketone compound of Formula (4) and a substituted acetophenone compound of Formula (5) as starting raw materials in an organic solvent or water in the presence or absence of an additive in the presence of a base in a suspended state. A method for producing 1,3-bis(substituted phenyl)-3-substituted-2-propen-2-one compound of Formula (2) comprises dehydrating the compound of Formula (3). A method for producing compound (2) in one step comprises reacting compound (4) and compound (5) to obtain compound (3). Further, a method for producing an isoxazoline compound of Formula (1) comprises reacting compound (2) and a hydroxylamine in an aliphatic or an aromatic hydrocarbon solvent which is optionally substituted by a halogen atom by adding an additive selected from a phase-transfer catalyst, a C1-C6 alcohol and an aprotic polar solvent in the presence of a base and water.
摘要翻译：提供了一种生产农药的新型中间体。制备式（3）的1,3-双（取代的苯基）-3-取代-3-羟基丙-1-酮化合物的方法包括使式（4）的芳族酮化合物与式（4）的取代的苯乙酮化合物 5）作为起始原料在有机溶剂或水中，在存在或不存在添加剂的情况下，在悬浮状态的碱存在下进行。制备式（2）的1,3-双（取代的苯基）-3-取代-2-丙烯-2-酮化合物的方法包括使式（3）的化合物脱水。一步法制备化合物（2）的方法包括使化合物（4）和化合物（5）反应得到化合物（3）。此外，制备式（1）的异恶唑啉化合物的方法包括使任选被卤素原子取代的脂族或芳族烃溶剂中的化合物（2）与羟胺反应，加入选自相转移催化剂，C1-C6醇和非质子极性溶剂在碱和水的存在下反应。

4. 发明授权

US08952175B2 Method for production of 3-hydroxypropan-1-one compound, method for production of 2-propen-1-one compound and method for production of isoxazoline compound 有权
标题翻译： 3-羟基丙烷-1-酮化合物的制造方法，2-丙烯-1-酮化合物的制造方法及异恶唑啉化合物的制造方法
公开(公告)号：US08952175B2
公开(公告)日：2015-02-10
申请号：US12452347
申请日：2008-06-27
申请人： Manabu Yaosaka , Tomohisa Utsunomiya , Yuji Moriyama , Tomohiro Matsumoto , Kazutaka Matoba
发明人： Manabu Yaosaka , Tomohisa Utsunomiya , Yuji Moriyama , Tomohiro Matsumoto , Kazutaka Matoba
IPC分类号： C07D261/04 , C07D213/30 , C07C45/72 , C07C45/74 , C07C49/83 , C07C49/835 , C07C51/353 , C07C65/40 , C07C67/347 , C07C69/65 , C07C231/12 , C07C253/30 , C07C319/20 , C07D213/50 , C07D213/61 , C07D233/14 , C07D249/08 , C07D401/04
CPC分类号： C07C45/72 , C07C45/66 , C07C45/74 , C07C49/83 , C07C49/835 , C07C51/353 , C07C51/367 , C07C51/377 , C07C65/40 , C07C67/327 , C07C67/343 , C07C67/347 , C07C69/65 , C07C231/12 , C07C253/30 , C07C319/20 , C07D213/30 , C07D213/50 , C07D213/61 , C07D233/14 , C07D249/08 , C07D261/04 , C07D401/04 , C07C323/22 , C07C235/84 , C07C255/56 , C07C69/76 , C07C49/813 , C07C65/38
摘要： There is provided a novel intermediate for producing pesticides. A method for producing the compound of Formula (3) comprises reacting an aromatic ketone compound of Formula (4) and a substituted acetophenone compound of Formula (5) as starting raw materials in an organic solvent or water in the presence or absence of an additive in the presence of a base in a suspended state. A method may comprise dehydrating the compound of Formula (3). A method for producing compound (2) in one step comprises reacting compound (4) and compound (5) to obtain compound (3). Further, a method for producing an isoxazoline compound of Formula (1) comprises reacting compound (2) and a hydroxylamine in an aliphatic or an aromatic hydrocarbon solvent which is optionally substituted by a halogen atom by adding an additive selected from a phase-transfer catalyst, a C1-C6 alcohol and an aprotic polar solvent in the presence of a base and water.
摘要翻译：提供了一种生产农药的新型中间体。制备式（3）化合物的方法包括使式（4）的芳族酮化合物和式（5）的取代的苯乙酮化合物作为起始原料，在存在或不存在添加剂的情况下，在有机溶剂或水中反应在有悬浮状态的基地的情况下。一种方法可以包括使式（3）的化合物脱水。一步法制备化合物（2）的方法包括使化合物（4）和化合物（5）反应得到化合物（3）。此外，制备式（1）的异恶唑啉化合物的方法包括使任选被卤素原子取代的脂族或芳族烃溶剂中的化合物（2）与羟胺反应，加入选自相转移催化剂，C1-C6醇和非质子极性溶剂在碱和水的存在下反应。

5. 发明授权

US07964758B2 Process for production of 2-(substituted phenyl)-3,3,3-trifluoropropene compound 有权
标题翻译： 2-（取代苯基）-3,3,3-三氟丙烯化合物的制备方法
公开(公告)号：US07964758B2
公开(公告)日：2011-06-21
申请号：US12223657
申请日：2007-02-13
申请人： Kazutaka Matoba , Takashi Mizukoshi , Yuji Moriyama
发明人： Kazutaka Matoba , Takashi Mizukoshi , Yuji Moriyama
IPC分类号： C07C17/32
CPC分类号： C07C17/263 , C07B37/04 , C07C41/30 , C07C231/12 , C07C25/24 , C07C22/08 , C07C233/15 , C07C43/225
摘要： There is provided a novel process for production of a 2-(substituted phenyl) -3,3,3-trifluoropropene. Disclosed is a process for production of a 2-(substituted phenyl)-3,3,3-trifluoropropene compound represented by the formula (7) or a salt thereof The process comprises reacting a compound represented by the formula (1) (X is an alkyl group, etc.) with a compound represented by the formula (2) (Y is a halogen atom, etc.) in the presence of a catalyst represented by the formula (3) (M is an ion of a metal belonging to Group 10 on the elementary periodic table which has an oxidation state number of 1 to 8; G is a unidentate or multidentate ligand; L is a phosphine compound represented by the formula (4) which is bound to the center metal M or is a carbene selected from those represented by the formulae (5) and (6), provided that L's may be same as or different from one another when a is 2 to 5; A represents a univalently or multivalently charged anion; b represents an integer of 1 to 3; a represents an integer of 1 to 5·b; c represents 0 or an integer of 1 to 4·b; and n represents an integer of 1 to 6).
摘要翻译：提供了一种生产2-（取代的苯基）-3,3,3-三氟丙烯的新方法。公开了一种由式（7）表示的2-（取代苯基）-3,3,3-三氟丙烯化合物或其盐的制备方法。该方法包括使式（1）表示的化合物（X为烷基等）与式（2）表示的化合物（Y为卤素原子等）在式（3）表示的催化剂的存在下反应（M为属于氧原子数为1〜8的元素周期表第10族; G为单齿或多齿配位体; L为与中心金属M结合的式（4）所示的膦化合物或者是卡宾选自由式（5）和（6）表示的那些，条件是当a为2至5时，L 1可以彼此相同或不同; A表示单价或多价带电的阴离子; b表示1至 3; a表示1〜5·b的整数，c表示0或1〜4·b的整数，n表示i 1到6的整数）。

6. 发明申请

US20100160683A1 Process for Production of 2-(Substituted Phenyl)-3,3,3-Trifluoropropene Compound 有权
标题翻译： 2-（取代苯基）-3,3,3-三氟丙烯化合物的制备方法
公开(公告)号：US20100160683A1
公开(公告)日：2010-06-24
申请号：US12223657
申请日：2007-02-13
申请人： Kazutaka Matoba , Takashi Mizukoshi , Yuji Moriyama
发明人： Kazutaka Matoba , Takashi Mizukoshi , Yuji Moriyama
IPC分类号： C07C231/12 , C07C17/32 , C07C41/30
CPC分类号： C07C17/263 , C07B37/04 , C07C41/30 , C07C231/12 , C07C25/24 , C07C22/08 , C07C233/15 , C07C43/225
摘要： There is provided a novel process for production of a 2-(substituted phenyl)-3,3,3-trifluoropropene. Disclosed is a process for production of a 2-(substituted phenyl)-3,3,3-trifluoropropene compound represented by the formula (7) or a salt thereof The process comprises reacting a compound represented by the formula (1) (X is an alkyl group, etc.) with a compound represented by the formula (2) (Y is a halogen atom, etc.) in the presence of a catalyst represented by the formula (3) (M is an ion of a metal belonging to Group 10 on the elementary periodic table which has an oxidation state number of 1 to 8; G is a unidentate or multidentate ligand; L is a phosphine compound represented by the formula (4) which is bound to the center metal M or is a carbene selected from those represented by the formulae (5) and (6), provided that L's may be same as or different from one another when a is 2 to 5; A represents a univalently or multivalently charged anion; b represents an integer of 1 to 3; a represents an integer of 1 to 5·b; c represents 0 or an integer of 1 to 4·b; and n represents an integer of 1 to 6).
摘要翻译：提供了一种生产2-（取代的苯基）-3,3,3-三氟丙烯的新方法。公开了一种由式（7）表示的2-（取代苯基）-3,3,3-三氟丙烯化合物或其盐的制备方法。该方法包括使式（1）表示的化合物（X为烷基等）与式（2）表示的化合物（Y为卤素原子等）在式（3）表示的催化剂的存在下反应（M为属于氧原子数为1〜8的元素周期表第10族; G为单齿或多齿配位体; L为与中心金属M结合的式（4）所示的膦化合物或者是卡宾选自由式（5）和（6）表示的那些，条件是当a为2至5时，L 1可以彼此相同或不同; A表示单价或多价带电的阴离子; b表示1至 3; a表示1〜5·b的整数，c表示0或1〜4·b的整数，n表示i 1到6的整数）。

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