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1. 发明授权

US5445902A Method for operating a power generator 失效
标题翻译：运行发电机的方法
公开(公告)号：US5445902A
公开(公告)日：1995-08-29
申请号：US133872
申请日：1993-10-12
申请人： Takao Soma , Tomonori Takahashi , Shinji Kawasaki , Katsuki Yoshioka
发明人： Takao Soma , Tomonori Takahashi , Shinji Kawasaki , Katsuki Yoshioka
IPC分类号： H01M4/86 , H01M8/04 , H01M8/12 , H01M8/02
CPC分类号： H01M8/04089 , H01M8/04007 , H01M8/1231 , Y10T29/49108
摘要： A method for operating a power generator in which a solid oxide fuel cell is used as a power-generating element and an air electrode of the solid oxide fuel cell is composed of lanthanum manganite, the method involving the step of setting a heating rate and a cooling rate at least in a temperature range of 800.degree. C. to 900.degree. C. at not less than 3.degree. C./min. when the fuel cell is heated up to an operating temperature at the time of starting the power generator and when the fuel cell is cooled from the operating temperature at the time of stopping the power generator. Alternatively, the method involves the step of setting a partial pressure of oxygen, at least in a temperature range of 800.degree. C. to 900.degree. C., in an atmosphere to which the air electrode is exposed, to at not less than 10.sup.-15 arms but not more than 10.sup.-1 arms when the fuel cell is heated up to an operating temperature at the time of starting the power generator and when the fuel cell is cooled from the operating temperature at the time of stopping the power generator.
摘要翻译：一种使用固体氧化物型燃料电池作为发电元件的发电机的动作方法以及固体氧化物型燃料电池的空气电极，由亚锰酸镧构成，其特征在于，包括：设定加热速度和冷却速度至少在800℃至900℃的温度范围内，不低于3℃/分钟。当燃料电池在启动发电机时被加热到工作温度，并且当燃料电池从停止发电机时的工作温度冷却时。或者，该方法包括在空气电极暴露的气氛中至少在800℃〜900℃的温度范围内设定氧分压至不小于10度的步骤，当燃料电池被加热到启动发电机时的工作温度，并且当燃料电池从停止发电机时的工作温度冷却时，15臂但不大于10-1臂。

2. 发明授权

US5432024A Porous lanthanum manganite sintered bodies and solid oxide fuel cells 失效
标题翻译：多孔镧亚锰酸盐烧结体和固体氧化物燃料电池
公开(公告)号：US5432024A
公开(公告)日：1995-07-11
申请号：US133873
申请日：1993-10-12
申请人： Takao Soma , Tomonori Takahashi , Shinji Kawasaki , Kazuyo Mori , Yoshihiro Ito , Katsuki Yoshioka
发明人： Takao Soma , Tomonori Takahashi , Shinji Kawasaki , Kazuyo Mori , Yoshihiro Ito , Katsuki Yoshioka
IPC分类号： C04B35/01 , C04B38/00 , H01M4/90 , H01M8/12 , C04B35/03 , H01M4/88
CPC分类号： H01M4/9033 , C04B35/016 , C04B38/0074 , H01M4/9016 , C04B2111/00853
摘要： A porous sintered body composed mainly of lanthanum manganite in which a part of lanthanum atoms at A-sites of the lanthanum manganite are substituted by atoms of a metal selected from the group consisting of alkaline earth metals and rare earth metals. The dimensional shrinkage amount of the porous sintered body in heat cycling between room temperature and 1,000.degree. C. is not more than 0.01% per one heat cycle.
摘要翻译：主要由亚锰酸镧组成的多孔烧结体，其中亚锰酸镧A位的镧原子的一部分被选自碱土金属和稀土金属的金属原子取代。多孔烧结体在室温和1000℃之间的热循环中的尺寸收缩量在每个热循环中不超过0.01％。

3. 发明授权

US5489483A Porous sintered bodies and solid oxide fuel cells using such porous sintered bodies as air electrodes 失效
标题翻译：使用这种多孔烧结体作为空气电极的多孔烧结体和固体氧化物燃料电池
公开(公告)号：US5489483A
公开(公告)日：1996-02-06
申请号：US297096
申请日：1994-08-29
申请人： Takao Soma , Tomonori Takahashi , Shinji Kawasaki , Hirotake Yamada , Kazuyo Mori
发明人： Takao Soma , Tomonori Takahashi , Shinji Kawasaki , Hirotake Yamada , Kazuyo Mori
IPC分类号： B01J23/00 , B01J23/34 , C04B35/00 , C04B35/01 , C04B38/00 , H01M4/86 , H01M4/90 , H01M8/02 , H01M8/12 , H01M12/06
CPC分类号： B01J23/002 , B01J23/34 , C04B35/01 , C04B38/00 , H01M4/9016 , H01M4/9033 , B01J2523/00
摘要： A porous sintered body is composed of a perovskite-type composite oxide, wherein A-site of the composite oxide are occupied by one or more kinds of first metallic elements selected from the group consisting of calcium and strontium, one or more kinds of second metal elements selected from the group consisting of rare earth elements and yttrium excluding lanthanum and cerium, and lanthanum, the above one or more kinds of the first metallic elements amount to 5 to 70 mol % of the A-sites, and manganese is contained in B-sites of the composite oxide.
摘要翻译：多孔烧结体由钙钛矿型复合氧化物构成，其中复合氧化物的A位被一种或多种选自钙和锶的第一金属元素占据，一种或多种第二金属选自除了镧和铈之外的稀土元素和钇的元素和镧，上述一种或多种第一金属元素占A位的5至70mol％，并且含有B的B 复合氧化物。

4. 发明授权

US5897970A System for production of high-purity hydrogen, process for production of high-purity hydrogen, and fuel cell system 失效
标题翻译：高纯氢生产系统，高纯氢生产工艺及燃料电池系统
公开(公告)号：US5897970A
公开(公告)日：1999-04-27
申请号：US961502
申请日：1997-10-30
申请人： Manabu Isomura , Takao Soma , Tomonori Takahashi
发明人： Manabu Isomura , Takao Soma , Tomonori Takahashi
IPC分类号： B01D53/22 , B01J19/24 , C01B3/32 , C01B3/34 , C01B3/38 , C01B3/50 , H01M8/00 , H01M8/06 , H01M16/00
CPC分类号： H01M8/0631 , B01J19/2475 , C01B3/32 , C01B3/323 , C01B3/34 , C01B3/38 , C01B3/382 , C01B3/386 , C01B3/501 , H01M8/0612 , B01J2219/0011 , B01J2219/00117 , B01J2219/00159 , C01B2203/0244 , C01B2203/041 , C01B2203/0465 , C01B2203/047 , C01B2203/066 , C01B2203/0811 , C01B2203/0822 , C01B2203/0827 , C01B2203/0844 , C01B2203/0866 , C01B2203/1064 , C01B2203/1076 , C01B2203/1223 , C01B2203/1288 , C01B2203/142 , C01B2203/1604 , C01B2203/82 , Y02P20/126 , Y02P20/128
摘要： There is a system for producing high-purity hydrogen by reforming a hydrocarbon and/or an oxygen atom-containing hydrocarbon to form a reformed gas containing hydrogen and separating the hydrogen from said gas. The system includes a hydrocarbon source, a water source, an oxygen source, a vaporization chamber connecting with the hydrocarbon source, the water source and the oxygen source, and a reforming chamber provided with a catalyst for steam reforming and partial oxidation and a hydrogen-separating membrane. The reforming chamber is thermally connected with the vaporization chamber. A process for producing high-purity hydrogen includes heating a reforming chamber provided with a hydrogen-separating membrane, feeding, into the reforming chamber, hydrocarbon, steam and oxygen or air to give rise to steam reforming and partial oxidation therein to produce a reaction gas, and passing the reaction gas through the hydrogen-separating membrane to recover high-purity hydrogen. The heat possessed by the portion of the reaction gas not permeable into the hydrogen-separating membrane and the heat generated by the partial oxidation are utilized for the heating and reforming of the hydrocarbon, water and oxygen or air.
摘要翻译：存在通过重整烃和/或含氧原子的烃来形成含氢的重整气体并从所述气体中分离出氢气的方法来生产高纯度氢气。该系统包括烃源，水源，氧源，与烃源连接的蒸发室，水源和氧源，以及设置有用于蒸汽重整和部分氧化的催化剂的重整室，分离膜。重整室与蒸发室热连接。一种生产高纯度氢的方法包括加热设置有氢分离膜的重整室，向重整室供给碳氢化合物，蒸气和氧气或空气，引起蒸汽重整和部分氧化，产生反应气体，并使反应气体通过氢分离膜以回收高纯度氢。反应气体不能透过氢分离膜的部分所产生的热量以及由部分氧化产生的热量用于烃，水和氧气或空气的加热和重整。

5. 发明授权

US5614001A Hydrogen separator, hydrogen separating apparatus and method for manufacturing hydrogen separator 失效
标题翻译：氢分离器，氢气分离装置及氢气分离器的制造方法
公开(公告)号：US5614001A
公开(公告)日：1997-03-25
申请号：US445027
申请日：1995-05-19
申请人： Shinichi Kosaka , Osamu Sakai , Tomonori Takahashi , Takao Soma
发明人： Shinichi Kosaka , Osamu Sakai , Tomonori Takahashi , Takao Soma
IPC分类号： B01D53/22 , B01D63/06 , B01D71/02 , C01B3/50 , B01D71/04
CPC分类号： B01D67/0069 , B01D53/22 , B01D63/066 , B01D71/022 , C01B3/505 , B01D2313/04 , B01D2313/06 , B01D2323/12 , C01B2203/0233 , C01B2203/0405 , C01B2203/047 , C01B2203/1223 , C01B2203/1229 , C01B2203/1241 , Y10S55/05
摘要： A hydrogen separator has a porous substrate having a through-hole, and a metal having a hydrogen separating ability coated on the inner surface of the through-hole of the porous substrate to close pores on the inner surface of the through-hole. A method for manufacturing a hydrogen separator by a chemical plating process, includes providing a porous substrate having a through-hole, and forcedly circulating a plating solution containing a metal having a hydrogen separating ability through the through-hole of the substrate. The inner surface of the through-hole is covered with the metal film having the hydrogen separating ability.
摘要翻译：氢分离器具有具有通孔的多孔基材和具有氢分离能力的金属，其涂覆在多孔基材的通孔的内表面上以封闭通孔内表面上的孔。一种通过化学镀处理制造氢分离器的方法，包括提供具有通孔的多孔基材，并且通过基材的通孔强制循环含有具有氢分离能力的金属的镀液。通孔的内表面被具有氢分离能力的金属膜覆盖。

6. 发明授权

US5612012A Method for removing carbon monoxide from reformed gas 失效
标题翻译：从重整气体中除去一氧化碳的方法
公开(公告)号：US5612012A
公开(公告)日：1997-03-18
申请号：US451367
申请日：1995-05-26
申请人： Takao Soma , Tomonori Takahashi , Manabu Isomura
发明人： Takao Soma , Tomonori Takahashi , Manabu Isomura
IPC分类号： B01D53/62 , C01B3/50 , C01B3/58 , H01M8/06 , C01B31/18
CPC分类号： H01M8/0662 , C01B3/501 , C01B3/505 , C01B3/586 , C01B2203/0405 , C01B2203/041 , C01B2203/0445 , C01B2203/047 , C01B2203/0475 , C01B2203/0495 , H01M2300/0082 , H01M8/0612
摘要： A method for removing CO from a reformed gas includes the steps of treating the reformed gas by a hydrogen purifier to decrease a ratio of the concentration of components other than hydrogen to the concentration of hydrogen so that the ratio may be lower than in the reformed gas, and then converting CO contained in the gas treated by the hydrogen purifier into a gas other than CO. CO can be removed from the reformed gas, and simultaneously high-purity hydrogen can also be obtained, which leads to the increase of a fuel efficiency and the inhibition effect of performance deterioration.
摘要翻译：从重整气体中除去CO的方法包括以下步骤：通过氢气净化器处理重整气体以降低氢气以外的组分的浓度与氢气浓度的比例，使得该比例可以比重整气体，然后将由氢气净化器处理的气体中包含的CO转化为CO以外的气体，CO可以从重整气体中除去，同时也可以获得高纯度的氢，这导致燃料效率的提高以及性能恶化的抑制作用。

7. 发明授权

US5741474A Process for production of high-purity hydrogen 失效
标题翻译：高纯度氢气生产工艺
公开(公告)号：US5741474A
公开(公告)日：1998-04-21
申请号：US443551
申请日：1995-05-18
申请人： Manabu Isomura , Takao Soma , Tomonori Takahashi
发明人： Manabu Isomura , Takao Soma , Tomonori Takahashi
IPC分类号： B01D53/22 , B01J19/24 , C01B3/32 , C01B3/34 , C01B3/38 , C01B3/50 , H01M8/00 , H01M8/06 , C01B3/02 , C01B3/24 , C01B3/26
CPC分类号： H01M8/0631 , B01J19/2475 , C01B3/32 , C01B3/323 , C01B3/34 , C01B3/38 , C01B3/382 , C01B3/386 , C01B3/501 , H01M8/0612 , B01J2219/0011 , B01J2219/00117 , B01J2219/00159 , C01B2203/0244 , C01B2203/041 , C01B2203/0465 , C01B2203/047 , C01B2203/066 , C01B2203/0811 , C01B2203/0822 , C01B2203/0827 , C01B2203/0844 , C01B2203/0866 , C01B2203/1064 , C01B2203/1076 , C01B2203/1223 , C01B2203/1288 , C01B2203/142 , C01B2203/1604 , C01B2203/82 , Y02P20/126 , Y02P20/128
摘要： There is a system for producing high-purity hydrogen by reforming a hydrocarbon and/or an oxygen atom-containing hydrocarbon to form a reformed gas containing hydrogen and separating the hydrogen from said gas. The system includes a hydrocarbon source, a water source, an oxygen source, a vaporization chamber connecting with the hydrocarbon source, the water source and the oxygen source, and a reforming chamber provided with a catalyst for steam reforming and partial oxidation and a hydrogen-separating membrane. The reforming chamber is thermally connected with the vaporization chamber. A process for producing high-purity hydrogen includes heating a reforming chamber provided with a hydrogen-separating membrane, feeding, into the reforming chamber, hydrocarbon, steam and oxygen or air to give rise to steam reforming and partial oxidation therein to produce a reaction gas, and passing the reaction gas through the hydrogen-separating membrane to recover high-purity hydrogen. The heat possessed by the portion of the reaction gas not permeable into the hydrogen-separating membrane and the heat generated by the partial oxidation are utilized for the heating and reforming of the hydrocarbon, water and oxygen or air.
摘要翻译：存在通过重整烃和/或含氧原子的烃来形成含氢的重整气体并从所述气体中分离出氢气的方法来生产高纯度氢气。该系统包括烃源，水源，氧源，与烃源连接的蒸发室，水源和氧源，以及设置有用于蒸汽重整和部分氧化的催化剂的重整室，分离膜。重整室与蒸发室热连接。一种生产高纯度氢的方法包括加热设置有氢分离膜的重整室，向重整室供给碳氢化合物，蒸气和氧气或空气，引起蒸汽重整和部分氧化，产生反应气体，并使反应气体通过氢分离膜以回收高纯度氢。反应气体不能透过氢分离膜的部分所产生的热量以及由部分氧化产生的热量用于烃，水和氧气或空气的加热和重整。

8. 发明授权

US4795724A Silicon nitride sintered bodies and process for manufacturing the same 失效
标题翻译：氮化硅烧结体及其制造方法
公开(公告)号：US4795724A
公开(公告)日：1989-01-03
申请号：US58115
申请日：1987-06-04
申请人： Takao Soma , Tomonori Takahashi
发明人： Takao Soma , Tomonori Takahashi
IPC分类号： C04B35/584 , C04B35/593 , C04B35/58
CPC分类号： C04B35/584 , C04B35/5935
摘要： Silicon nitride sintered bodies are disclosed, which each consist essentially of Si, O, N, and at least two kinds of rare earth elements selected from Y, Er, Tm, Yb, and Lu the bodies comprising not less than 70% by weight of Si.sub.3 N.sub.4. The ratio of the molar amount of all the rare earth elements contained in the sintered body calculated as moles of Ln.sub.2 O.sub.3, Ln being a rare earth element selected from Y, Er. Tm, Yb and Lu divided by the molar amount of oxygen calculated as moles of SiO.sub.2 is within the range of from 0.4 to 1.3. The amount of oxygen calculated as moles of SiO.sub.2 is obtained by subtracting the amount of oxygen contained in all the Ln.sub.2 O.sub.3, all the rare earth elements contained in said sintered body being considered as molecules of Ln.sub.2 O.sub.3 from the amount of oxygen contained in the sintered body and converting the remaining amount of oxygen into moles of SiO.sub.2. Any one of the rare earth elements contained in the sintered body accounts for not more than 95 mol % of all the rare earth elements contained in the sintered body. An intergranular phase of Si.sub.3 N.sub.4 grains contained in the sintered body is substantially of a crystalline phase and not less than 50% of the crystalline phase of the intergranular phase is a crystalline phases of an apatite structure. A process for manufacturing such silicon nitride sintered bodies is also disclosed.
摘要翻译：公开了氮化硅烧结体，其各自主要由Si，O，N和至少两种选自Y，Er，Tm，Yb和Lu的稀土元素组成，所述稀土元素包含不小于70重量％ Si3N4。烧结体中所含的所有稀土元素的摩尔量的比例，以Ln2O3的摩尔数计，Ln为选自Y，Er的稀土元素。 Tm，Yb和Lu除以以SiO 2摩尔计算的氧的摩尔量在0.4至1.3的范围内。以SiO2的摩尔数计算的氧的量通过从烧结体中所含的氧的量中减去所有Ln 2 O 3中包含的所有烧结体中包含的所有烧结体中的氧被认为是Ln 2 O 3的分子而得到的氧的量，将剩余的氧量转化为SiO 2的摩尔数。包含在烧结体中的稀土元素中的任一种占烧结体中所含的全部稀土元素的不超过95mol％。包含在烧结体中的Si 3 N 4晶粒的晶间相基本上是结晶相，晶间相的结晶相的50％以上是磷灰石结构的结晶相。还公开了制造这种氮化硅烧结体的方法。

9. 发明授权

US4801414A Production of silicon nitride sintered body 失效
标题翻译：生产氮化硅烧结体
公开(公告)号：US4801414A
公开(公告)日：1989-01-31
申请号：US12160
申请日：1987-02-09
申请人： Takao Soma , Tomonori Takahashi
发明人： Takao Soma , Tomonori Takahashi
IPC分类号： C04B35/584 , C04B35/593 , C04B41/00 , C04B41/80 , C04B33/32
CPC分类号： C04B41/009 , C04B35/5935 , C04B41/0072 , C04B41/80
摘要： A process is disclosed for producing silicon nitride sintered bodies. The process comprises the steps of molding a formulated starting material of silicon nitride, firing a thus obtained molding to obtain a fired body having a desired shape, and then thermally treating the fired body in such an atmosphere that has an oxygen partial pressure higher than that in a firing atmosphere and suppresses a weight increment in oxidation to not more than 0.1 mg/cm.sup.2. Working may be done to obtain the desired shape of the fired body after the firing but before the thermal treatment.
摘要翻译：公开了一种用于生产氮化硅烧结体的方法。该方法包括以下步骤：模制配制的氮化硅原料，焙烧如此获得的模制物，以获得具有所需形状的烧制体，然后在氧分压高于其中的氧气分压的气氛中对烧成体进行热处理。在烧成气氛中，抑制氧化重量增加至0.1mg / cm 2以下。可以进行工作以在烧制之后但是在热处理之前获得所需的烧制体的形状。

10. 发明授权

US4747984A Production of silicon nitride sintered body 失效
标题翻译：生产氮化硅烧结体
公开(公告)号：US4747984A
公开(公告)日：1988-05-31
申请号：US932204
申请日：1986-11-18
申请人： Takao Soma , Tomonori Takahashi
发明人： Takao Soma , Tomonori Takahashi
IPC分类号： C04B35/584 , C04B35/593 , C04B35/64
CPC分类号： C04B35/584 , C04B35/5935
摘要： A process for manufacturing a silicon nitride sintered body comprises molding a mixed powder of a silicon nitride starting material and a sintering aid and firing a thus obtained molding. The firing is carried out in an N.sub.2 atmosphere or a mixed atmosphere of N.sub.2 and an inert gas to which CO.sub.2 or a mixed gas of CO.sub.2 and CO is added. Thereby, an O.sub.2 partial pressure is increased to restrain the evaporation of SiO.sub.2 and nitriding of SiO.sub.2 during the firing. The silicon nitride sintered body suffers almost no deterioration of the fired surface resulting from the evaporation of SiO.sub.2 and the nitriding of SiO.sub.2, and exhibits substantially equal four point bending strength and oxidation resistance with respect to the fired surface and the inside thereof.
摘要翻译：一种氮化硅烧结体的制造方法，其特征在于，将氮化硅原料和烧结助剂的混合粉末成形，烧成由此得到的成形体。烧成是在N 2的气氛或N 2的混合气氛和CO 2或CO 2和CO的混合气体中添加的惰性气体中进行的。由此，增加O2分压，以抑制SiO 2的蒸发和焙烧期间的SiO 2的氮化。氮化硅烧结体几乎没有由于SiO 2的蒸发和SiO 2的氮化而引起的烧结表面的劣化，并且相对于烧结表面及其内部表现出大致相等的四点弯曲强度和抗氧化性。

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