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    • 3. 发明申请
    • METHOD FOR PULLING SILICON SINGLE CRYSTAL
    • 拉丝硅单晶的方法
    • US20100089309A1
    • 2010-04-15
    • US12450961
    • 2008-04-14
    • Satoshi SoetaMasahiro Mori
    • Satoshi SoetaMasahiro Mori
    • C30B15/22
    • C30B29/06C30B15/22
    • The invention is a method for pulling a silicon single crystal, which is a Czochralski method for growing the silicon single crystal by contacting a seed crystal with a melt and by pulling up, including the steps of: contacting the seed crystal with the melt; forming a necking portion under the seed crystal; and forming the silicon single crystal under the necking portion by increasing a diameter, wherein a pulling rate during forming the necking portion is 2 mm/min or less, and the silicon single crystal with the increased diameter is a boron-doped silicon single crystal having a resistivity of 1.5 mΩ·cm or less at a shoulder portion. Therefore, there can be provided a method of pulling a silicon single crystal without generating defects such as scratches at a wafer surface in the case of processing a boron-doped silicon single crystal ingot with a low resistivity produced by CZ method into a wafer.
    • 本发明是一种拉硅单晶的方法,该硅单晶是通过使晶种与熔体接触并通过拉起来生长硅单晶的切克劳斯基法,包括以下步骤:使晶种与熔体接触; 在晶种下形成颈缩部分; 并且通过增加直径在颈缩部分下形成硅单晶,其中在形成颈缩部分期间的拉伸速率为2mm / min以下,并且具有增加的直径的硅单晶是具有硼掺杂的硅单晶,其具有 在肩部的电阻率为1.5m&OHgr·cm或更小。 因此,在通过CZ法制造的具有低电阻率的硼掺杂硅单晶锭加工成晶片的情况下,可以提供拉丝硅单晶的方法,而不会在晶片表面产生诸如划痕之类的缺陷。
    • 4. 发明授权
    • Device and method for producing single crystal
    • 单晶制造装置及方法
    • US5972106A
    • 1999-10-26
    • US776776
    • 1997-02-10
    • Tomohiko OhtaSusumu SonokawaSatoshi SoetaYoshihiro Kodama
    • Tomohiko OhtaSusumu SonokawaSatoshi SoetaYoshihiro Kodama
    • C30B15/14C30B15/20C30B29/40
    • C30B29/40C30B15/14C30B15/206C30B29/06Y10T117/1064Y10T117/1068Y10T117/1072Y10T117/1088
    • A device and method for producing single crystals by the Czohralski method can control the temperature distribution and thermal history of single crystals to improve the production efficiency and quality of single crystals. The device includes a cylinder coaxially surrounding a single crystal pulling rod, having an upper end airtightly connected to the ceiling of a pulling chamber and a lower end close to the surface of a melt in a crucible. A heat insulating element is attached to the lower end of the cylinder, and is surrounded by a surface of the crystal, the inside wall of the crucible and the surface of the melt. The heat insulating element is sized to occupy 30-95% by volume of the space above the melt, and the space has a height corresponding to the radius of the crystal. The heat insulator has a sufficient heat insulating effect, so that even if the diameter of single crystals is increased, the pulling speed of the crystals does not need to be lowered, the uniformity of temperature of the entire crystal-melt interface is improved, and the ratio of single crystallization is not reduced.
    • PCT No.PCT / JP95 / 02514 Sec。 371日期1997年2月10日 102(e)日期1997年2月10日PCT提交1995年12月8日PCT公布。 公开号WO97 / 21853 日期:1997年6月19日Czohralski法制备单晶的装置和方法可以控制单晶的温度分布和热历史,提高单晶的生产效率和质量。 该装置包括同轴地围绕单晶拉杆的圆筒,其具有气密地连接到拉动室的顶部的上端和靠近坩埚中的熔体表面的下端。 绝热元件附着在圆筒的下端,被坩埚的表面,坩埚的内壁和熔体的表面所包围。 绝热元件的尺寸设定为占据熔体上方空间的30-95%(体积),并且该空间的高度对应于晶体的半径。 绝热体具有充分的隔热效果,即使单晶的直径增大,也不需要降低晶体的拉伸速度,提高整个晶体熔融界面的温度均匀性, 单一结晶的比例不降低。
    • 6. 发明申请
    • Graphite heater for producing single crystal, single crystal productin system and single crystal productin method
    • 石墨加热器,用于生产单晶,单晶产品系统和单晶产品方法
    • US20050205004A1
    • 2005-09-22
    • US10516347
    • 2003-12-08
    • Masahiro SakuradaIzumi FusegawaSatoshi SoetaMakoto Iida
    • Masahiro SakuradaIzumi FusegawaSatoshi SoetaMakoto Iida
    • C30B15/14C30B35/00C30B1/00
    • C30B15/14Y10T117/10
    • The present invention discloses a graphite heater for producing a single crystal used when producing a single crystal by the Czochralski method which comprises at least a terminal part to which electric current is supplied and a cylindrical heat generating part by resistance heating and are provided so as to surround a crucible for containing a raw material melt wherein the heat generating part has heat generating slit parts formed by being provided with upper slits extending downward from the upper end and lower slits extending upwards from the lower end by turns, and a length of at least one slit of the upper slits differs from others and/or a length of at least one slit of the lower slits differs from others so that a heat generating distribution of the heat generating part may be changed. Thereby, there can be provided a graphite heater for producing a single crystal which makes it possible to produce a silicon single crystal with high productivity when the silicon single crystal is pulled in a predetermined defect-free region or a predetermined defect region.
    • 本发明公开了一种石墨加热器,用于生产通过切克劳斯基法生产单晶时使用的单晶,该方法至少包括供给电流的端子部分和电阻加热的圆柱形发热部分, 围绕用于容纳原料熔体的坩埚,其中发热部具有通过从上端向下延伸的上部狭缝形成的发热狭缝部和由下端向上延伸的下部狭缝,并且至少具有长度 上缝隙的一个狭缝与其他狭缝不同,和/或下狭缝的至少一个狭缝的长度不同,从而可以改变发热部分的发热分布。 因此,可以提供一种用于制造单晶的石墨加热器,当在预定的无缺陷区域或预定缺陷区域中拉伸硅单晶时,可以以高生产率制造单晶硅。
    • 7. 发明授权
    • Graphite heater for producing single crystal, apparatus for producing single crystal, and method for producing single crystal
    • 用于制造单晶的石墨加热器,单晶的制造装置以及单晶的制造方法
    • US07258744B2
    • 2007-08-21
    • US10516347
    • 2003-12-08
    • Masahiro SakuradaIzumi FusegawaSatoshi SoetaMakoto Iida
    • Masahiro SakuradaIzumi FusegawaSatoshi SoetaMakoto Iida
    • C30B35/00C30B15/20
    • C30B15/14Y10T117/10
    • The present invention discloses a graphite heater for producing a single crystal used when producing a single crystal by the Czochralski method which comprises at least a terminal part to which electric current is supplied and a cylindrical heat generating part by resistance heating and are provided so as to surround a crucible for containing a raw material melt wherein the heat generating part has heat generating slit parts formed by being provided with upper slits extending downward from the upper end and lower slits extending upwards from the lower end by turns, and a length of at least one slit of the upper slits differs from others and/or a length of at least one slit of the lower slits differs from others so that a heat generating distribution of the heat generating part may be changed. Thereby, there can be provided a graphite heater for producing a single crystal which makes it possible to produce a silicon single crystal with high productivity when the silicon single crystal is pulled in a predetermined defect-free region or a predetermined defect region.
    • 本发明公开了一种石墨加热器,用于生产通过切克劳斯基法生产单晶时使用的单晶,该方法至少包括供给电流的端子部分和电阻加热的圆柱形发热部分, 围绕用于容纳原料熔体的坩埚,其中发热部具有通过从上端向下延伸的上部狭缝形成的发热狭缝部和由下端向上延伸的下部狭缝,并且至少具有长度 上缝隙的一个狭缝与其他狭缝不同,和/或下狭缝的至少一个狭缝的长度不同,从而可以改变发热部分的发热分布。 因此,可以提供一种用于制造单晶的石墨加热器,当在预定的无缺陷区域或预定缺陷区域中拉伸硅单晶时,可以以高生产率制造单晶硅。
    • 8. 发明授权
    • Method for pulling silicon single crystal
    • 拉硅单晶的方法
    • US08652254B2
    • 2014-02-18
    • US12450961
    • 2008-04-14
    • Satoshi SoetaMasahiro Mori
    • Satoshi SoetaMasahiro Mori
    • C30B15/22
    • C30B29/06C30B15/22
    • The invention is a method for pulling a silicon single crystal, which is a Czochralski method for growing the silicon single crystal by contacting a seed crystal with a melt and by pulling up, including the steps of: contacting the seed crystal with the melt; forming a necking portion under the seed crystal; and forming the silicon single crystal under the necking portion by increasing a diameter, wherein a pulling rate during forming the necking portion is 2 mm/min or less, and the silicon single crystal with the increased diameter is a boron-doped silicon single crystal having a resistivity of 1.5 mΩ·cm or less at a shoulder portion. Therefore, there can be provided a method of pulling a silicon single crystal without generating defects such as scratches at a wafer surface in the case of processing a boron-doped silicon single crystal ingot with a low resistivity produced by CZ method into a wafer.
    • 本发明是一种拉硅单晶的方法,该硅单晶是通过使晶种与熔体接触并通过拉起来生长硅单晶的切克劳斯基法,包括以下步骤:使晶种与熔体接触; 在晶种下形成颈缩部分; 并且通过增加直径在颈缩部分下形成硅单晶,其中在形成颈缩部分期间的拉伸速率为2mm / min以下,并且具有增加的直径的硅单晶是具有硼掺杂的硅单晶,其具有 肩部的电阻率为1.5mΩ·cm以下。 因此,在通过CZ法制造的具有低电阻率的硼掺杂硅单晶锭加工成晶片的情况下,可以提供拉丝硅单晶的方法,而不会在晶片表面产生诸如划痕之类的缺陷。
    • 10. 发明授权
    • Seed crystal holder
    • 种子晶体座
    • US5851287A
    • 1998-12-22
    • US804146
    • 1997-02-20
    • Satoshi Soeta
    • Satoshi Soeta
    • C30B15/32C30B35/00
    • C30B15/32Y10S117/90Y10T117/10Y10T117/1032Y10T117/1072
    • A seed crystal holder is used to grow a single crystal in an intended direction. In order to grow a single crystal in an intended direction by a crystal pulling method, a seed crystal is accurately cut out along a crystal orientation, and this seed crystal is accurately held in a predetermined attitude by the seed crystal holder. A seed crystal insertion bore having a rectangular cross-section is formed in the body of the seed crystal holder. A seed crystal having a taper surface at one edge is inserted into the seed crystal insertion bore. The inserted seed crystal is pressed at its taper surface by a taper surface of a block, so that two surfaces of the seed crystal are fixedly pressed against two inner surfaces of the seed crystal insertion bore. The other end of the block is covered with a block-retaining ring, so that the block does not come off the seed crystal holder.
    • 种子晶体保持器用于在预期方向上生长单晶。 为了通过晶体拉伸法在预期的方向上生长单晶,可以将晶种沿着晶体取向精确地切出,并且通过籽晶保持器将晶种准确地保持在预定的姿态。 具有矩形横截面的晶种插入孔形成在晶种保持器的主体中。 在一个边缘具有锥形表面的籽晶插入晶种插入孔中。 插入的晶种在其锥形表面被块的锥形表面压制,使得晶种的两个表面被固定地压在晶种插入孔的两个内表面上。 块的另一端覆盖有块保持环,使得块不会从晶种座脱落。