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1. 发明授权

US07087127B2 Method of bonding a window to a substrate using a silane functional adhesive composition 有权
公开(公告)号：US07087127B2
公开(公告)日：2006-08-08
申请号：US10819503
申请日：2004-04-07
申请人： Syed Z. Mahdi , Harry W. Hsieh
发明人： Syed Z. Mahdi , Harry W. Hsieh
IPC分类号： B32B37/12
CPC分类号： C09J175/08 , C03C27/048 , C08G18/10 , C08G18/12 , C08G18/24 , C08G18/4808 , C08G18/4825 , C08G18/718 , C08G65/2642 , C08G65/2651 , C08G65/336 , C08G2190/00 , C08L71/00 , C08L75/04 , C09J5/06 , C09J171/02 , C09J2400/143 , C09J2471/00 , C09J2475/00 , C08G18/307 , C08G18/3893
摘要： The invention is an adhesive composition comprising a) i) a trialkoxysilane functional polyether or polyurethane wherein the polyether or polyurethane has a weight average molecular weight of 6000 or greater and a dialkyltin carboxylate or dialkyltin alcoholate; or ii) a dialkoxysilane functional polyether or polyurethane and a dialkyltin alcoholate; and b) a primary or secondary amino straight chain alkyl trialkoxysilane; wherein the dialkyltin carboxylate or dialkyltin alcoholate is present in an effective amount to facilitate bonding of the adhesive to a substrate of from about 0.1 to about 1.0 percent by weight based on the weight of the adhesive and the primary or secondary amino straight chained alkyl trialkoxysilane is present in an amount which is effective to facilitate bonding of the adhesive to a substrate wherein the amount is from about 0.5 to about 1.2 percent by weight. In another embodiment, the invention is a method of bonding a window in a vehicle. The process comprises applying to a window or a window frame of a structure an adhesive according to the invention; contacting the window with the window frame of a substrate wherein the adhesive is located between the window and the substrate; and allowing the adhesive to cure. This process is especially useful when the substrate is unprimed metal, plastic, fiberglass or a composite, optionally coated with a coating. In another embodiment it is useful when the window is unprimed.

2. 发明授权

US06828403B2 Method of bonding a window to a substrate using a silane functional adhesive composition 失效
标题翻译：使用硅烷官能粘合剂组合物将窗口粘合到基底上的方法
公开(公告)号：US06828403B2
公开(公告)日：2004-12-07
申请号：US10035894
申请日：2001-11-09
申请人： Syed Z. Mahdi , Harry W. Hsieh
发明人： Syed Z. Mahdi , Harry W. Hsieh
IPC分类号： C08G1830
CPC分类号： C09J175/08 , C03C27/048 , C08G18/10 , C08G18/12 , C08G18/24 , C08G18/4808 , C08G18/4825 , C08G18/718 , C08G65/2642 , C08G65/2651 , C08G65/336 , C08G2190/00 , C08L71/00 , C08L75/04 , C09J5/06 , C09J171/02 , C09J2400/143 , C09J2471/00 , C09J2475/00 , C08G18/307 , C08G18/3893
摘要： The invention is an adhesive composition comprising a) i) a trialkoxysilane functional polyether or polyurethane wherein the polyether or polyurethane has a weight average molecular weight of 6000 or greater and a dialkyltin carboxylate or dialkyltin alcoholate; or ii) a dialkoxysilane functional polyether or polyurethane and a dialkyltin alcoholate; and b) a primary or secondary amino straight chain alkyl trialkoxysilane; wherein the dialkyltin carboxylate or dialkyltin alcoholate is present in an effective amount to facilitate bonding of the adhesive to a substrate of from about 0.1 to about 1.0 percent by weight based on the weight of the adhesive and the primary or secondary amino straight chained alkyl trialkoxysilane is present in an amount which is effective to facilitate bonding of the adhesive to a substrate wherein the amount is from about 0.5 to about 1.2 percent by weight.
摘要翻译：本发明是一种粘合剂组合物，其包含：i）三烷氧基硅烷官能的聚醚或聚氨酯，其中所述聚醚或聚氨酯具有6000或更大的重均分子量和二烷基锡羧酸酯或二烷基锡醇盐; orii）二烷氧基硅烷官能的聚醚或聚氨酯和二烷基锡醇盐; 和b）伯或仲氨基直链烷基三烷氧基硅烷;其中所述二烷基锡羧酸酯或二烷基锡醇化物以有效的量存在，以促进粘合剂与基材的粘合，其量为约0.1至约1.0重量％粘合剂和主要或仲氨基直链烷基三烷氧基硅烷以有效促进粘合剂粘合到基材上的量存在，其量为约0.5至约1.2重量％。

3. 发明授权

US6015475A Polyurethane sealant compositions 有权
标题翻译：聚氨酯密封剂组合物
公开(公告)号：US6015475A
公开(公告)日：2000-01-18
申请号：US129856
申请日：1998-08-06
申请人： Harry W. Hsieh , Syed Z. Mahdi
发明人： Harry W. Hsieh , Syed Z. Mahdi
IPC分类号： C03C27/04 , C08G18/10 , C08G18/12 , C08G18/16 , C08G18/18 , C08G18/24 , C08G18/28 , C08G18/48 , C08G18/73 , C09J175/04 , C09K3/10 , C09J4/00
CPC分类号： C08G18/73 , C08G18/10 , C08G18/12 , C08G18/16 , C08G18/161 , C08G18/163 , C08G18/18 , C08G18/1875 , C08G18/289 , C08G18/4812 , C08G2190/00
摘要： In one aspect, this invention is a polyurethane sealant composition comprising (1) a urethane prepolymer having an isocyanate functionality of at least about 2.0 and a weight average molecular weight of at least about 2,000; and (2) a catalytic amount of (a) a substantially active hydrogen free glycol acid salt of a tertiary amine and an organo metallic compound, (b) a mixture of a substantially active hydrogen free glycol acid salt of a tertiary amine and an organo metallic compound and a second organometallic compound, or (c) a mixture of an organometallic compound with dimorpholinodialkyl ether or an dialkylmorpholinodialkyl ether. In another embodiment, the polyurethane sealant composition further comprises (A) a silane, or (B) an adduct of an isocyanate reactive silane and a polyisocyanate, (C) the reaction product of an isocyanate reactive silane or an adduct of an isocyanate reactive silane and a polyisocyanate with a polyisocyanate and an active hydrogen containing compound or a polyurethane prepolymer which has free isocyanate moieties; which reaction product has an average of at least one silane group and at least one isocyanate group per molecule. In another embodiment the invention is a method for bonding glass to a substrate which comprises contacting a sealant according to the invention with glass and another substrate with the sealant disposed between the glass and substrate and thereafter allowing the sealant to cure so as to bind the glass to the substrate. The sealant composition of the invention is useful in bonding glass substrates to metal plastic, fiberglass or composite substrates, which may or may not be painted. It has been discovered to give unexpectedly high lap shear strength when no primer compositions have previously been applied to the painted plastic, metal, fiberglass or composite substrate.
摘要翻译：一方面，本发明是一种聚氨酯密封剂组合物，其包含（1）具有至少约2.0的异氰酸酯官能度和至少约2,000的重均分子量的氨基甲酸酯预聚物; 和（2）催化量的（a）叔胺和有机金属化合物的基本上活性的无氢二醇酸盐，（b）叔胺的基本上活性的无氢二醇酸盐和有机金属的混合物金属化合物和第二有机金属化合物，或（c）有机金属化合物与二吗啉代二烷基醚或二烷基吗啉代二烷基醚的混合物。在另一个实施方案中，聚氨酯密封剂组合物还包含（A）硅烷或（B）异氰酸酯反应性硅烷和多异氰酸酯的加合物，（C）异氰酸酯反应性硅烷或异氰酸酯反应性硅烷的加合物的反应产物和具有多异氰酸酯和含活性氢化合物或具有游离异氰酸酯部分的聚氨酯预聚物的多异氰酸酯; 该反应产物每分子具有至少一个硅烷基团和至少一个异氰酸酯基团的平均值。在另一个实施方案中，本发明是将玻璃粘合到基底上的方法，其包括使根据本发明的密封剂与玻璃和另一基底接触，所述密封剂设置在玻璃和基底之间，然后使密封剂固化以便将玻璃粘合到基底。本发明的密封剂组合物可用于将玻璃基材粘合到金属塑料，玻璃纤维或复合基材上，其可以涂漆或可以不被涂漆。已经发现当没有底漆组合物已经施加到涂漆的塑料，金属，玻璃纤维或复合基材上时，出现意想不到的高搭接剪切强度。

4. 发明授权

US06613816B2 Cure on demand adhesives and window module with cure on demand adhesive thereon 有权
标题翻译：固化按需粘合剂和窗口模块，在其上固化需要的粘合剂
公开(公告)号：US06613816B2
公开(公告)日：2003-09-02
申请号：US09875986
申请日：2001-06-07
申请人： Syed Z. Mahdi , Renhe R. Lin , Dwight K. Hoffman , Gordon M. Parker , Harry W. Hsieh
发明人： Syed Z. Mahdi , Renhe R. Lin , Dwight K. Hoffman , Gordon M. Parker , Harry W. Hsieh
IPC分类号： C08G7708
CPC分类号： C09J175/08 , C08G18/10 , C08G18/12 , C08G18/24 , C08G18/246 , C08G18/4808 , C08G18/4825 , C08G18/718 , C08G65/2642 , C08G65/2651 , C08G65/336 , C08G2190/00 , C09J171/02 , Y10T428/31601 , Y10T428/31612 , Y10T428/31645 , C08G18/307 , C08G18/3893
摘要： In one embodiment the invention is An adhesive composition comprising a) a polymer having a flexible backbone and a reactive moiety capable of cross-linking, b) a particle comprising an active agent encapsulated in an encapsulating agent wherein the active agent comprises a catalyst for cross-linking of the reactive moiety, a curing agent for the reactive moiety, an accelerator for the curing reaction or a mixture thereof; and the encapsulating agent comprises a side chain crystallizable polymer wherein the active agent is not substantially extractable from the particle at ambient conditions in a first extraction after particle formation.
摘要翻译：在一个实施方案中，本发明是一种粘合剂组合物，其包含a）具有柔性主链和能够交联的反应性部分的聚合物，b）包含包封在包封剂中的活性剂的颗粒，其中活性剂包含用于交联的催化剂，反应性部分的连接，反应性部分的固化剂，用于固化反应的促进剂或其混合物;并且所述包封剂包含侧链可结晶聚合物，其中活性剂在环境条件下基本上不可从颗粒中提取颗粒形成后的第一次提取。

5. 发明授权

US5852137A Polyurethane sealant compositions 失效
公开(公告)号：US5852137A
公开(公告)日：1998-12-22
申请号：US790635
申请日：1997-01-29
申请人： Harry W. Hsieh , Syed Z. Mahdi
发明人： Harry W. Hsieh , Syed Z. Mahdi
IPC分类号： C03C27/04 , C08G18/10 , C08G18/12 , C08G18/16 , C08G18/18 , C08G18/24 , C08G18/28 , C08G18/48 , C08G18/73 , C09J175/04 , C09K3/10 , C08L75/04
CPC分类号： C08G18/73 , C08G18/10 , C08G18/12 , C08G18/16 , C08G18/161 , C08G18/163 , C08G18/18 , C08G18/1875 , C08G18/289 , C08G18/4812 , C08G2190/00
摘要： In one aspect, this invention is a polyurethane sealant composition comprising (1) a urethane prepolymer having an isocyanate functionality of at least about 2.0 and a weight average molecular weight of at least about 2,000; and (2) a catalytic amount of (a) a substantially active hydrogen free glycol acid salt of a tertiary amine and an organo metallic compound, (b) a mixture of a substantially active hydrogen free glycol acid salt of a tertiary amine and an organo metallic compound and a second organometallic compound, or (c) a mixture of an organometallic compound with dimorpholinodialkyl ether or an dialkylmorpholinodialkyl ether. In another embodiment, the polyurethane sealant composition further comprises (A) a silane, or (B) an adduct of an isocyanate reactive silane and a polyisocyanate, (C) the reaction product of an isocyanate reactive silane or an adduct of an isocyanate reactive silane and a polyisocyanate with a polyisocyanate and an active hydrogen containing compound or a polyurethane prepolymer which has free isocyanate moieties; which reaction product has an average of at least one silane group and at least one isocyanate group per molecule. In another embodiment the invention is a method for bonding glass to a substrate which comprises contacting a sealant according to the invention with glass and another substrate with the sealant disposed between the glass and substrate and thereafter allowing the sealant to cure so as to bind the glass to the substrate. The sealant composition of the invention is useful in bonding glass substrates to metal plastic, fiberglass or composite substrates, which may or may not be painted. It has been discovered to give unexpectedly high lap shear strength when no primer compositions have previously been applied to the painted plastic, metal, fiberglass or composite substrate.

6. 发明授权

US06355127B1 Cure on demand adhesives and window module with cure on demand adhesive thereon 有权
标题翻译：固化按需粘合剂和窗口模块，在其上固化需要的粘合剂
公开(公告)号：US06355127B1
公开(公告)日：2002-03-12
申请号：US09300342
申请日：1999-04-27
申请人： Syed Z. Mahdi , Renhe R. Lin , Dwight K. Hoffman , Gordon M. Parker , by Michael Parker , Harry W. Hsieh
发明人： Syed Z. Mahdi , Renhe R. Lin , Dwight K. Hoffman , Gordon M. Parker , by Michael Parker , Harry W. Hsieh
IPC分类号： B32B3126
CPC分类号： C09J175/08 , C08G18/10 , C08G18/12 , C08G18/24 , C08G18/246 , C08G18/4808 , C08G18/4825 , C08G18/718 , C08G65/2642 , C08G65/2651 , C08G65/336 , C08G2190/00 , C09J171/02 , Y10T428/31601 , Y10T428/31612 , Y10T428/31645 , C08G18/307 , C08G18/3893
摘要： In one embodiment the invention is An adhesive composition comprising a) a polymer having a flexible backbone and a reactive moiety capable of cross-linking, b) a particle comprising an active agent encapsulated in an encapsulating agent wherein the active agent comprises a catalyst for cross-linking of the reactive moiety, a curing agent for the reactive moiety, an accelerator for the curing reaction or a mixture thereof; and the encapsulating agent comprises a side chain crystallizable polymer wherein the active agent is not substantially extractable from the particle at ambient conditions in a first extraction after particle formation. This composition is used in binding two subtracters together.
摘要翻译：在一个实施方案中，本发明是一种粘合剂组合物，其包含a）具有柔性主链和能够交联的反应性部分的聚合物，b）包含包封在包封剂中的活性剂的颗粒，其中活性剂包含用于交联的催化剂，反应性部分的连接，反应性部分的固化剂，固化反应的促进剂或其混合物; 并且包封剂包括侧链可结晶聚合物，其中活性剂在颗粒形成之后的第一次萃取中在环境条件下基本上不可从颗粒中提取。该组合物用于将两个减法器结合在一起。

7. 发明授权

US6001214A Polyurethane sealant compositions 有权
公开(公告)号：US6001214A
公开(公告)日：1999-12-14
申请号：US129857
申请日：1998-08-06
申请人： Harry W. Hsieh , Syed Z. Mahdi
发明人： Harry W. Hsieh , Syed Z. Mahdi
IPC分类号： C03C27/04 , C08G18/10 , C08G18/12 , C08G18/16 , C08G18/18 , C08G18/24 , C08G18/28 , C08G18/48 , C08G18/73 , C09J175/04 , C09K3/10
CPC分类号： C08G18/73 , C08G18/10 , C08G18/12 , C08G18/16 , C08G18/161 , C08G18/163 , C08G18/18 , C08G18/1875 , C08G18/289 , C08G18/4812 , C08G2190/00
摘要： In one aspect, this invention is a polyurethane sealant composition comprising (1) a urethane prepolymer having an isocyanate functionality of at least about 2.0 and a weight average molecular weight of at least about 2,000; and (2) a catalytic amount of (a) a substantially active hydrogen free glycol acid salt of a tertiary amine and an organo metallic compound, (b) a mixture of a substantially active hydrogen free glycol acid salt of a tertiary amine and an organo metallic compound and a second organometallic compound, or (c) a mixture of an organometallic compound with dimorpholinodialkyl ether or an dialkylmorpholinodialkyl ether. In another embodiment, the polyurethane sealant composition further comprises (A) a silane, or (B) an adduct of an isocyanate reactive silane and a polyisocyanate, (C) the reaction product of an isocyanate reactive silane or an adduct of an isocyanate reactive silane and a polyisocyanate with a polyisocyanate and an active hydrogen containing compound or a polyurethane prepolymer which has free isocyanate moieties; which reaction product has an average of at least one silane group and at least one isocyanate group per molecule. In another embodiment the invention is a method for bonding glass to a substrate which comprises contacting a sealant according to the invention with glass and another substrate with the sealant disposed between the glass and substrate and thereafter allowing the sealant to cure so as to bind the glass to the substrate. The sealant composition of the invention is useful in bonding glass substrates to metal plastic, fiberglass or composite substrates, which may or may not be painted. It has been discovered to give unexpectedly high lap shear strength when no primer compositions have previously been applied to the painted plastic, metal, fiberglass or composite substrate.

8. 发明申请

US20080199607A1 System for bonding glass into a structure 有权
公开(公告)号：US20080199607A1
公开(公告)日：2008-08-21
申请号：US11707701
申请日：2007-02-16
申请人： Harry W. Hsieh , Dominic J. Allam , Ziyan Wu
发明人： Harry W. Hsieh , Dominic J. Allam , Ziyan Wu
IPC分类号： C07F7/18 , B05D5/06
CPC分类号： C09J5/02 , C08J5/124 , C09J2400/143 , C09J2400/146 , C09J2400/226 , C09J2475/00
摘要： The invention is a composition comprising a) one or more organotitanates having four ligands wherein the ligands are hydrocarbyl, optionally containing one or more functional groups having one or more heteroatoms selected from the group comprising oxygen, nitrogen, phosphorus and sulfur wherein two or more of the ligands may form a cyclic structure; b) one or more mercaptosilanes; c) one or more polyaminosilanes; d) one or more secondary aminosilanes; and e) a solvent which dissolves the components of the composition. This composition is referred to as a clear primer hereinafter. In another embodiment the invention is a system for bonding glass to a substrate which comprises a clear primer according to the invention; and an adhesive comprising an isocyanate functional prepolymer and a catalyst for the cure of the isocyanate functional prepolymer.

9. 发明授权

US07819964B2 System for bonding glass into a structure 有权
标题翻译：将玻璃粘结成结构的系统
公开(公告)号：US07819964B2
公开(公告)日：2010-10-26
申请号：US11707701
申请日：2007-02-16
申请人： Harry W. Hsieh , Dominic J. Allam , Ziyan Wu
发明人： Harry W. Hsieh , Dominic J. Allam , Ziyan Wu
IPC分类号： C09J5/02
CPC分类号： C09J5/02 , C08J5/124 , C09J2400/143 , C09J2400/146 , C09J2400/226 , C09J2475/00
摘要： The invention is a composition comprising a) one or more organotitanates having four ligands wherein the ligands are hydrocarbyl, optionally containing one or more functional groups having one or more heteroatoms selected from the group comprising oxygen, nitrogen, phosphorus and sulfur wherein two or more of the ligands may form a cyclic structure; b) one or more mercaptosilanes; c) one or more polyaminosilanes; d) one or more secondary aminosilanes; and e) a solvent which dissolves the components of the composition. The composition also includes an organotin compound f). This composition is referred to as a clear primer hereinafter. In another embodiment the invention is a system for bonding glass to a substrate which comprises a clear primer according to the invention; and an adhesive comprising an isocyanate functional prepolymer and a catalyst for the cure of the isocyanate functional prepolymer.
摘要翻译：本发明是一种组合物，其包含a）一种或多种具有四种配体的有机钛酸盐，其中配体是烃基，任选地含有一个或多个具有一个或多个选自氧，氮，磷和硫的杂原子的官能团，其中两个或多个配体可以形成环状结构; b）一种或多种巯基硅烷; c）一种或多种聚氨基硅烷; d）一种或多种仲氨基硅烷; 和e）溶解组合物组分的溶剂。组合物还包括有机锡化合物f）。该组合物在下文中称为透明底漆。在另一个实施方案中，本发明是用于将玻璃粘合到基底上的系统，其包含根据本发明的透明底漆; 以及包含异氰酸酯官能预聚物和用于固化异氰酸酯官能预聚物的催化剂的粘合剂。

10. 发明授权

US07708853B2 System for bonding glass into a structure 有权
标题翻译：将玻璃粘结成结构的系统
公开(公告)号：US07708853B2
公开(公告)日：2010-05-04
申请号：US12195648
申请日：2008-08-21
申请人： Ziyan Wu , Harry W. Hsieh , Daniel P. Heberer , Dominic J. Allam
发明人： Ziyan Wu , Harry W. Hsieh , Daniel P. Heberer , Dominic J. Allam
IPC分类号： C09J5/02 , B60J10/02
CPC分类号： C03C27/048 , C03C27/10 , C09D5/002 , C09J5/02
摘要： The invention is a bonding process using a composition comprising a) one or more organotitanates or zirconates having four ligands wherein the ligands are hydrocarbyl, optionally containing one or more functional groups having one or more heteroatoms selected from the group comprising oxygen, nitrogen, phosphorus and sulfur wherein two or more of the ligands may form a cyclic structure with the proviso that one of the ligands has an acidic moiety; one or more strong organic acids or a mixture thereof; b) one or more alkoxysilanes; c) optionally one or more high molecular weight resins; and d) a solvent which dissolves the components of the composition. This composition is referred to as a clear primer hereinafter. Preferably, the composition comprises both an organotitanate or zirconate and a strong acid.
摘要翻译：本发明是使用组合物的粘合方法，该组合物包含a）一种或多种具有四种配体的有机钛酸酯或锆酸盐，其中配体是烃基，任选地含有一个或多个具有一个或多个选自氧，氮，磷的杂原子的官能团，硫，其中两个或更多个配体可以形成环状结构，条件是配体之一具有酸性部分; 一种或多种强有机酸或其混合物; b）一种或多种烷氧基硅烷; c）任选的一种或多种高分子量树脂; 和d）溶解组合物组分的溶剂。该组合物在下文中称为透明底漆。优选地，组合物包含有机钛酸盐或锆酸盐和强酸。

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