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1. 发明授权

US07819964B2 System for bonding glass into a structure 有权
标题翻译：将玻璃粘结成结构的系统
公开(公告)号：US07819964B2
公开(公告)日：2010-10-26
申请号：US11707701
申请日：2007-02-16
申请人： Harry W. Hsieh , Dominic J. Allam , Ziyan Wu
发明人： Harry W. Hsieh , Dominic J. Allam , Ziyan Wu
IPC分类号： C09J5/02
CPC分类号： C09J5/02 , C08J5/124 , C09J2400/143 , C09J2400/146 , C09J2400/226 , C09J2475/00
摘要： The invention is a composition comprising a) one or more organotitanates having four ligands wherein the ligands are hydrocarbyl, optionally containing one or more functional groups having one or more heteroatoms selected from the group comprising oxygen, nitrogen, phosphorus and sulfur wherein two or more of the ligands may form a cyclic structure; b) one or more mercaptosilanes; c) one or more polyaminosilanes; d) one or more secondary aminosilanes; and e) a solvent which dissolves the components of the composition. The composition also includes an organotin compound f). This composition is referred to as a clear primer hereinafter. In another embodiment the invention is a system for bonding glass to a substrate which comprises a clear primer according to the invention; and an adhesive comprising an isocyanate functional prepolymer and a catalyst for the cure of the isocyanate functional prepolymer.
摘要翻译：本发明是一种组合物，其包含a）一种或多种具有四种配体的有机钛酸盐，其中配体是烃基，任选地含有一个或多个具有一个或多个选自氧，氮，磷和硫的杂原子的官能团，其中两个或多个配体可以形成环状结构; b）一种或多种巯基硅烷; c）一种或多种聚氨基硅烷; d）一种或多种仲氨基硅烷; 和e）溶解组合物组分的溶剂。组合物还包括有机锡化合物f）。该组合物在下文中称为透明底漆。在另一个实施方案中，本发明是用于将玻璃粘合到基底上的系统，其包含根据本发明的透明底漆; 以及包含异氰酸酯官能预聚物和用于固化异氰酸酯官能预聚物的催化剂的粘合剂。

2. 发明授权

US07708853B2 System for bonding glass into a structure 有权
标题翻译：将玻璃粘结成结构的系统
公开(公告)号：US07708853B2
公开(公告)日：2010-05-04
申请号：US12195648
申请日：2008-08-21
申请人： Ziyan Wu , Harry W. Hsieh , Daniel P. Heberer , Dominic J. Allam
发明人： Ziyan Wu , Harry W. Hsieh , Daniel P. Heberer , Dominic J. Allam
IPC分类号： C09J5/02 , B60J10/02
CPC分类号： C03C27/048 , C03C27/10 , C09D5/002 , C09J5/02
摘要： The invention is a bonding process using a composition comprising a) one or more organotitanates or zirconates having four ligands wherein the ligands are hydrocarbyl, optionally containing one or more functional groups having one or more heteroatoms selected from the group comprising oxygen, nitrogen, phosphorus and sulfur wherein two or more of the ligands may form a cyclic structure with the proviso that one of the ligands has an acidic moiety; one or more strong organic acids or a mixture thereof; b) one or more alkoxysilanes; c) optionally one or more high molecular weight resins; and d) a solvent which dissolves the components of the composition. This composition is referred to as a clear primer hereinafter. Preferably, the composition comprises both an organotitanate or zirconate and a strong acid.
摘要翻译：本发明是使用组合物的粘合方法，该组合物包含a）一种或多种具有四种配体的有机钛酸酯或锆酸盐，其中配体是烃基，任选地含有一个或多个具有一个或多个选自氧，氮，磷的杂原子的官能团，硫，其中两个或更多个配体可以形成环状结构，条件是配体之一具有酸性部分; 一种或多种强有机酸或其混合物; b）一种或多种烷氧基硅烷; c）任选的一种或多种高分子量树脂; 和d）溶解组合物组分的溶剂。该组合物在下文中称为透明底漆。优选地，组合物包含有机钛酸盐或锆酸盐和强酸。

3. 发明申请

US20090205769A1 SYSTEM FOR BONDING GLASS INTO A STRUCTURE 有权
标题翻译：将玻璃粘结成结构的系统
公开(公告)号：US20090205769A1
公开(公告)日：2009-08-20
申请号：US12195648
申请日：2008-08-21
申请人： Ziyan Wu , Harry W. Hsieh , Daniel P. Heberer , Dominic J. Allam
发明人： Ziyan Wu , Harry W. Hsieh , Daniel P. Heberer , Dominic J. Allam
IPC分类号： B32B37/12
CPC分类号： C03C27/048 , C03C27/10 , C09D5/002 , C09J5/02
摘要： The invention is a composition comprising a) one or more organotitanates or zirconates having four ligands wherein the ligands are hydrocarbyl, optionally containing one or more functional groups having one or more heteroatoms selected from the group comprising oxygen, nitrogen, phosphorus and sulfur wherein two or more of the ligands may form a cyclic structure with the proviso that one of the ligands has an acidic moiety; one or more strong organic acids or a mixture thereof; b) one or more alkoxysilanes; c) optionally one or more high molecular weight resins; and d) a solvent which dissolves the components of the composition. This composition is referred to as a clear primer hereinafter. Preferably, the composition comprises both an organotitanate or zirconate and a strong acid.
摘要翻译：本发明是一种组合物，其包含a）一种或多种具有四种配体的有机钛酸酯或锆酸盐，其中配体是烃基，任选地含有一个或多个具有一个或多个选自氧，氮，磷和硫的杂原子的官能团，其中两个或更多的配体可以形成环状结构，条件是配体之一具有酸性部分; 一种或多种强有机酸或其混合物; b）一种或多种烷氧基硅烷; c）任选的一种或多种高分子量树脂; 和d）溶解组合物组分的溶剂。该组合物在下文中称为透明底漆。优选地，组合物包含有机钛酸盐或锆酸盐和强酸。

4. 发明授权

US07494540B2 System for bonding glass into a structure 有权
标题翻译：将玻璃粘结成结构的系统
公开(公告)号：US07494540B2
公开(公告)日：2009-02-24
申请号：US11012606
申请日：2004-12-15
申请人： Ziyan Wu , Harry W. Hsieh , Daniel P. Heberer , Dominic J. Allam
发明人： Ziyan Wu , Harry W. Hsieh , Daniel P. Heberer , Dominic J. Allam
IPC分类号： C09J5/02 , C09J175/00
CPC分类号： C03C27/048 , C03C27/10 , C09D5/002 , C09J5/02
摘要： The invention is a composition comprising a) one or more organotitanates or zirconates having four ligands wherein the ligands are hydrocarbyl, optionally containing one or more functional groups having one or more heteroatoms selected from the group comprising oxygen, nitrogen, phosphorus and sulfur wherein two or more of the ligands may form a cyclic structure with the proviso that one of the ligands has an acidic moiety; one or more strong organic acids or a mixture thereof; b) one or more alkoxysilanes; c) optionally one or more high molecular weight resins; and d) a solvent which dissolves the components of the composition. This composition is referred to as a clear primer hereinafter. Preferably, the composition comprises both an organotitanate or zirconate and a strong acid.
摘要翻译：本发明是一种组合物，其包含a）一种或多种具有四种配体的有机钛酸酯或锆酸盐，其中配体是烃基，任选地含有一个或多个具有一个或多个选自氧，氮，磷和硫的杂原子的官能团，其中两个或更多的配体可以形成环状结构，条件是配体之一具有酸性部分; 一种或多种强有机酸或其混合物; b）一种或多种烷氧基硅烷; c）任选的一种或多种高分子量树脂; 和d）溶解组合物组分的溶剂。该组合物在下文中称为透明底漆。优选地，组合物包含有机钛酸盐或锆酸盐和强酸。

5. 发明授权

US07416599B2 System for bonding glass into a structure 有权
标题翻译：将玻璃粘结成结构的系统
公开(公告)号：US07416599B2
公开(公告)日：2008-08-26
申请号：US11008426
申请日：2004-12-10
申请人： Harry W. Hsieh , Daniel P. Heberer , Dominic J. Allam , Ziyan Wu
发明人： Harry W. Hsieh , Daniel P. Heberer , Dominic J. Allam , Ziyan Wu
IPC分类号： E06B3/56 , C09J5/02 , C09J175/00
CPC分类号： C09J175/04 , C03C27/048 , C08G18/10 , C08G18/307
摘要： The invention is a composition comprising a) one or more organotitanates having four ligands wherein the ligands are hydrocarbyl, optionally containing one or more functional groups having one or more heteroatoms selected from the group comprising oxygen, nitrogen, phosphorus and sulfur wherein two or more of the ligands may form a cyclic structure; b) one or more mercaptosilanes; c) one or more polyaminosilanes; d) one or more secondary aminosilanes; and e) a solvent which dissolves the components of the composition. This composition is referred to as a clear primer hereinafter. In another embodiment the invention is a system for bonding glass to a substrate which comprises a clear primer according to the invention; and an adhesive comprising an isocyanate functional prepolymer and a catalyst for the cure of the isocyanate functional prepolymer.
摘要翻译：本发明是一种组合物，其包含a）一种或多种具有四种配体的有机钛酸盐，其中配体是烃基，任选地含有一个或多个具有一个或多个选自氧，氮，磷和硫的杂原子的官能团，其中两个或多个配体可以形成环状结构; b）一种或多种巯基硅烷; c）一种或多种聚氨基硅烷; d）一种或多种仲氨基硅烷; 和e）溶解组合物组分的溶剂。该组合物在下文中称为透明底漆。在另一个实施方案中，本发明是用于将玻璃粘合到基底上的系统，其包含根据本发明的透明底漆; 以及包含异氰酸酯官能预聚物和用于固化异氰酸酯官能预聚物的催化剂的粘合剂。

6. 发明申请

US20080199607A1 System for bonding glass into a structure 有权
公开(公告)号：US20080199607A1
公开(公告)日：2008-08-21
申请号：US11707701
申请日：2007-02-16
申请人： Harry W. Hsieh , Dominic J. Allam , Ziyan Wu
发明人： Harry W. Hsieh , Dominic J. Allam , Ziyan Wu
IPC分类号： C07F7/18 , B05D5/06
CPC分类号： C09J5/02 , C08J5/124 , C09J2400/143 , C09J2400/146 , C09J2400/226 , C09J2475/00
摘要： The invention is a composition comprising a) one or more organotitanates having four ligands wherein the ligands are hydrocarbyl, optionally containing one or more functional groups having one or more heteroatoms selected from the group comprising oxygen, nitrogen, phosphorus and sulfur wherein two or more of the ligands may form a cyclic structure; b) one or more mercaptosilanes; c) one or more polyaminosilanes; d) one or more secondary aminosilanes; and e) a solvent which dissolves the components of the composition. This composition is referred to as a clear primer hereinafter. In another embodiment the invention is a system for bonding glass to a substrate which comprises a clear primer according to the invention; and an adhesive comprising an isocyanate functional prepolymer and a catalyst for the cure of the isocyanate functional prepolymer.

7. 发明申请

US20060124225A1 System for bonding glass into a structure 有权
公开(公告)号：US20060124225A1
公开(公告)日：2006-06-15
申请号：US11012606
申请日：2004-12-15
申请人： Ziyan Wu , Harry Hsieh , Daniel Heberer , Dominic Allam
发明人： Ziyan Wu , Harry Hsieh , Daniel Heberer , Dominic Allam
IPC分类号： B60J1/00
CPC分类号： C03C27/048 , C03C27/10 , C09D5/002 , C09J5/02
摘要： The invention is a composition comprising a) one or more organotitanates or zirconates having four ligands wherein the ligands are hydrocarbyl, optionally containing one or more functional groups having one or more heteroatoms selected from the group comprising oxygen, nitrogen, phosphorus and sulfur wherein two or more of the ligands may form a cyclic structure with the proviso that one of the ligands has an acidic moiety; one or more strong organic acids or a mixture thereof; b) one or more alkoxysilanes; c) optionally one or more high molecular weight resins; and d) a solvent which dissolves the components of the composition. This composition is referred to as a clear primer hereinafter. Preferably, the composition comprises both an organotitanate or zirconate and a strong acid.

8. 发明申请

US20050126683A1 System for bonding glass into a structure 有权
标题翻译：将玻璃粘结成结构的系统
公开(公告)号：US20050126683A1
公开(公告)日：2005-06-16
申请号：US11008426
申请日：2004-12-10
申请人： Harry Hsieh , Daniel Heberer , Dominic Allam , Ziyan Wu
发明人： Harry Hsieh , Daniel Heberer , Dominic Allam , Ziyan Wu
IPC分类号： B32B17/10 , C03C27/04 , C08G18/10 , C09J175/04 , B60J1/00 , B32B31/00
CPC分类号： C09J175/04 , C03C27/048 , C08G18/10 , C08G18/307
摘要： The invention is a composition comprising a) one or more organotitanates having four ligands wherein the ligands are hydrocarbyl, optionally containing one or more functional groups having one or more heteroatoms selected from the group comprising oxygen, nitrogen, phosphorus and sulfur wherein two or more of the ligands may form a cyclic structure; b) one or more mercaptosilanes; c) one or more polyaminosilanes; d) one or more secondary aminosilanes; and e) a solvent which dissolves the components of the composition. This composition is referred to as a clear primer hereinafter. In another embodiment the invention is a system for bonding glass to a substrate which comprises a clear primer according to the invention; and an adhesive comprising an isocyanate functional prepolymer and a catalyst for the cure of the isocyanate functional prepolymer.
摘要翻译：本发明是一种组合物，其包含a）一种或多种具有四种配体的有机钛酸盐，其中配体是烃基，任选地含有一个或多个具有一个或多个选自氧，氮，磷和硫的杂原子的官能团，其中两个或多个配体可以形成环状结构; b）一种或多种巯基硅烷; c）一种或多种聚氨基硅烷; d）一种或多种仲氨基硅烷; 和e）溶解组合物组分的溶剂。该组合物在下文中称为透明底漆。在另一个实施方案中，本发明是用于将玻璃粘合到基底上的系统，其包含根据本发明的透明底漆; 以及包含异氰酸酯官能预聚物和用于固化异氰酸酯官能预聚物的催化剂的粘合剂。

9. 发明授权

US06875303B2 Method of bonding a window to a substrate without a primer 有权
标题翻译：将窗口粘合到没有底漆的基材上的方法
公开(公告)号：US06875303B2
公开(公告)日：2005-04-05
申请号：US10304425
申请日：2002-11-26
申请人： Andon Samurkas , Ziyan Wu , Sean C. Tobin , Daniel P. Heberer
发明人： Andon Samurkas , Ziyan Wu , Sean C. Tobin , Daniel P. Heberer
IPC分类号： B60J1/02 , B08B7/00 , B32B17/10 , C03C27/04 , C08L75/04 , C09J5/02 , C09J175/04 , C09J201/00 , H05H1/24
CPC分类号： C09J5/02 , B08B7/00 , C03C27/048 , C08L75/04 , C09J2400/143 , C09J2475/00
摘要： The invention is a process for bonding glass to a substrate without the need to prime the surface of the substrate. The process comprises, first, treating the surface of the substrate with air plasma, applying to the surface of the substrate or to the surface of the glass an adhesive capable of bonding to the treated substrate and glass, and contacting the glass and the substrate with the adhesive disposed between the substrate and the glass, and allowing the adhesive to cure. Preferably the substrate is coated with a coating. Preferred adhesives are polyurethane or silane functional elastomeric adhesives.The process of the invention allows bonding of glass to a substrate without the need to use a primer on the substrate prior to application of the adhesive. The process is especially effective in facilitating the bonding of glass to coated substrates, especially substrates coated with acid resistant coatings such as PPG's carbamate coating or DuPont's Gen III, IV and VI coatings.
摘要翻译：本发明是一种将玻璃粘合到基材上的方法，而不需要填充基材的表面。该方法包括：首先用空气等离子体处理衬底的表面，向衬底的表面或玻璃表面施加能够与经处理的衬底和玻璃结合的粘合剂，并将玻璃和衬底与粘合剂设置在基板和玻璃之间，并允许粘合剂固化。优选地，用涂层涂覆基材。优选的粘合剂是聚氨酯或硅烷官能的弹性体粘合剂。本发明的方法允许将玻璃粘合到基材上，而不需要在施加粘合剂之前在基材上使用底漆。该方法在促进玻璃与涂覆的基材，特别是涂覆有耐酸涂层如PPG的氨基甲酸酯涂层或DuPont的Gen III，IV和VI涂层的基材之间特别有效。

10. 发明授权

US06512033B1 Polyurethane sealant compositions 有权
标题翻译：聚氨酯密封剂组合物
公开(公告)号：US06512033B1
公开(公告)日：2003-01-28
申请号：US09498084
申请日：2000-02-04
申请人： Ziyan Wu
发明人： Ziyan Wu
IPC分类号： C08J552
CPC分类号： C09K3/1021 , C08G18/12 , C08G2190/00 , Y10T428/31547 , Y10T428/31678 , C08G18/289 , C08G18/307 , C08G18/792
摘要： In one aspect, this invention is a polyurethane sealant composition comprising (1) a urethane prepolymer having an isocyante functionality of at least about 2.0 and a weight average molecular weight of at least about 2,000; (2) a catalytic amount of a tin compound which catalyzes the reaction of isocyanate moieties with water or an active hydrogen containing compound; and (3) a stabilizing amount of an organophosphite which has an alkaryl ligand or both an aliphatic ligand and an aromatic ligand. The prepolymer may further comprises silane functionality or the composition may further comprise a compound or polymer which contains silane moieties and is compatible with the polyurethane prepolymer. The invention is also a method for bonding glass to a substrate which comprises contacting a sealant according to the invention with glass and another substrate with the sealant disposed between the glass and substrate and thereafter allowing the sealant to cure so as to bond the glass to the substrate.
摘要翻译：一方面，本发明是一种聚氨酯密封剂组合物，其包含（1）具有至少约2.0的异氰酸官能度和至少约2,000的重均分子量的氨基甲酸酯预聚物;（2）催化量的锡化合物，催化异氰酸酯部分与水或含活性氢化合物的反应; 和（3）稳定量的具有烷芳基配体或脂族配体和芳族配体两者的有机亚磷酸酯。预聚物还可以包含硅烷官能团，或者该组合物还可以包含含有硅烷部分并与聚氨酯预聚物相容的化合物或聚合物。本发明也是将玻璃粘合到基底上的方法，其包括使根据本发明的密封剂与玻璃和另一个基底接触，将密封剂设置在玻璃和基底之间，然后使密封剂固化以将玻璃粘合到基质。

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