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1. 发明授权

US4138568A Process for the manufacture of benzimidazolones-(2) 失效
标题翻译：制造苯并咪唑酮的方法 - （2）
公开(公告)号：US4138568A
公开(公告)日：1979-02-06
申请号：US801941
申请日：1977-05-31
申请人： Stefan Hari , Ernesto Rinaldi , Josef Somlo
发明人： Stefan Hari , Ernesto Rinaldi , Josef Somlo
IPC分类号： C07D235/26
CPC分类号： C07D235/26
摘要： Process for the manufacture of benzimidazolones-(2) wherein an o-phenylenediamine is reacted with optionally alkylated urea in the ratio of 1 to 1.3 moles per mole o-phenylenediamine in an organic solvent which has a solubility in water of not more than 5 g/l and has a boiling point above 100.degree. C, at a temperature between 100.degree. and 200.degree. C.
摘要翻译：制备苯并咪唑酮的方法 - （2）其中邻苯二胺与任选烷基化的脲以1至1.3摩尔/摩尔邻苯二胺在有机溶剂中的比例反应，其在水中的溶解度不超过5克沸点高于100℃，温度在100〜200℃之间。

2. 发明授权

US5380870A Mixed crystals of sulfonated diketopyrrolopyrroles 失效
标题翻译：磺化二酮吡咯并吡咯的混合晶体
公开(公告)号：US5380870A
公开(公告)日：1995-01-10
申请号：US166750
申请日：1993-12-14
申请人： Stefan Hari , Olof Wallquist , Fritz Herren , Thomas Eichenberger
发明人： Stefan Hari , Olof Wallquist , Fritz Herren , Thomas Eichenberger
IPC分类号： C07D487/04 , C08K5/17 , C08K5/34 , C08K5/3412 , C08K5/3415 , C09B57/00 , C09B67/18 , C09B67/22 , C09B69/04
CPC分类号： C07D487/04 , C09B67/0039 , C09B69/04
摘要： Mixed crystals of at least two different compounds of formula ##STR1## wherein A and B are each independently of the other a cation of formula ##EQU1## or N.sup.+ H(R.sub.1)(R.sub.2)(R.sub.3) M is a mono-, di- or trivalent metal cation, n is 1, 2 or 3, R.sub.1, R.sub.2 and R.sub.3 are each independently of one another hydrogen, C.sub.1 -C.sub.22 alkyl, C.sub.7 -C.sub.24 aralkyl, C.sub.5 -C.sub.6 cycloalkyl or C.sub.6 -C.sub.18 aryl, m is 0 or 1, and R is hydrogen, C.sub.1 -C.sub.4 alkyl or C.sub.1 -C.sub.4 alkoxy, in which compounds of formula I that form the mixed crystals the cations A and B constitute a composite structure ##EQU2## wherein x is a value from 0.2 to 0.8, and the X-ray diffraction pattern of said mixed crystals differs from that of the corresponding compounds in which x is 1 or 0.These mixed crystals can be used as pigments for colouring organic material of high molecular weight and have exceptional properties, especially dispersibility, heat- and lightfastness.
摘要翻译：式（I）的至少两种不同的化合物的混合晶体，其中A和B各自独立地为式“阳离子”或“N + H”（R 1）（R 2）（R 3） - ，二价或三价金属阳离子，n为1,2或3，R 1，R 2和R 3各自独立地为氢，C 1 -C 22烷基，C 7 -C 24芳烷基，C 5 -C 6环烷基或C 6 -C 18芳基，m为0或 1，R是氢，C 1 -C 4烷基或C 1 -C 4烷氧基，其中形成阳离子A和B的混合晶体的式I化合物构成复合结构，其中x为0.2至0.8的值，所述混晶的X射线衍射图与其中x为1或0的相应化合物的X射线衍射图不同。这些混合晶体可以用作高分子量有机材料着色的颜料，具有特别的性能，特别是分散性，和耐光性。

3. 发明授权

US5071967A Disazo compounds containing long-chain alkyl ester radicals or alkylamide radicals 失效
标题翻译：含有长链氨基酸酯或碱性氨基酸的灭菌化合物
公开(公告)号：US5071967A
公开(公告)日：1991-12-10
申请号：US654140
申请日：1991-02-11
申请人： Stefan Hari , Jost von der Crone
发明人： Stefan Hari , Jost von der Crone
IPC分类号： C08K5/22 , C08K5/23 , C09B27/00 , C09B29/15 , C09B33/147 , C09B33/153 , C09B43/32
CPC分类号： C09B43/32 , C08K5/235 , C09B27/00 , C09B29/106 , C09B33/153
摘要： Compounds of the formula I ##STR1## in which R is a radical of the formula --OR.sub.5 or --NHR.sub.5, A is a radical of the formula II or III ##STR2## in which B is a radical of the formula ##STR3## in which n is the number 1 or 2, R.sub.1 and R.sub.3 independently of one another are --H or Cl, R.sub.2 and R.sub.4 independently of one another are --H, halogen, --NO.sub.2, --CN, C.sub.1 -C.sub.4 alkyl, C.sub.1 -C.sub.4 alkoxy, --CF.sub.3, C.sub.2 -C.sub.5 alkoxycarbonyl, or --CONH-phenyl, --NHCO-phenyl or phenyloxy which is unsubstituted or substituted on the phenyl nucleus by one or two chlorine atoms or one or two methyl, methoxy or ethoxy groups, R.sub.5 is alkyl having at least 10 C atoms, R.sub.6 and R.sub.7 independently of one another are --H, halogen, --NO.sub.2, --CN, --CF.sub.3, C.sub.1 -C.sub.4 alkyl or C.sub.1 -C.sub.4 alkoxy, R.sub.8 is --H, --Cl, --Br, --CH.sub.3 or --OCH.sub.3 and X is --H, --Br, --OCH.sub.3, --CN or --NO.sub.2, are particularly suitable as pigments for coloring polyolefins.
摘要翻译：其中R为式-OR5或-NHR5基团的式I化合物（Ⅰ）化合物，A为式II或III的基团。）其中B是式为“IMAGE”的基团，其中n为数1或2，R 1和R 3彼此独立地为-H或Cl，R 2和R 4彼此独立地为-H，卤素， - NO 2，-CN，C 1 -C 4烷基，C 1 -C 4烷氧基，-CF 3，C 2 -C 5烷氧基羰基或-CONH-苯基，-NHCO-苯基或苯氧基，其在苯基上被未取代或取代一个或两个氯原子或一个或两个甲基，甲氧基或乙氧基，R5是具有至少10个C原子的烷基，R 6和R 7彼此独立地是-H，卤素，-NO 2，-CN，-CF 3，C 1 -C 4烷基或C 1 -C 4烷氧基，R 8是 -H，-Cl，-Br，-CH 3或-OCH 3，X为-H，-Br，-OCH 3，-CN或-NO 2，特别适合作为着色聚烯烃的颜料。

4. 发明授权

US4946948A Mono and disazo compounds based on b-hydroxy-naphthoic acid derivatives or acetoacetarylide derivatives containing long-chain alkyl ester or alkylamide radicals 失效
标题翻译：基于b-羟基 - 萘甲酸衍生物或含有长链烷基酯或烷基酰胺基团的乙酰乙酰胺衍生物的单和二重氮化合物
公开(公告)号：US4946948A
公开(公告)日：1990-08-07
申请号：US401349
申请日：1989-08-31
申请人： Stefan Hari , Fridolin Babler
发明人： Stefan Hari , Fridolin Babler
IPC分类号： C08K5/00 , C08K5/23 , C09B29/15 , C09B33/147 , C09B33/153 , C09B43/124
CPC分类号： C09B33/147 , C08K5/0041 , C08K5/235 , C09B29/103 , C09B33/153 , C09B43/124
摘要： Compounds of formula I: ##STR1## wherein R is a radical of the formula --OR.sub.3 or --NHR.sub.3, A is a radical of formula II or III: ##STR2## B is a radical of the formula ##STR3## n is the number 1 or 2, R.sub.1 is --H or --Cl, R.sub.2 is --H, halogen, --NO.sub.2, --CN, C.sub.1 -C.sub.4 alkyl, C.sub.1 -C.sub.4 alkoxy, --CF.sub.3, C.sub.2 -C.sub.5 alkoxycarbonyl or --CONH-phenyl, --NHCO-phenyl or phenoxy which is unsubstituted or substituted on the phenyl ring by one or two chlorine atoms or one or two methyl, methoxy or ethoxy groups, R.sub.3 is alkyl containing at least 10 C atoms, R.sub.4 and R.sub.5 are each independently of the other --H, halogen, --NO.sub.2, --CN, --CF.sub.3, C.sub.1 -C.sub.4 alkyl or C.sub.1 -C.sub.4 alkoxy, R.sub.6 is --H, --Cl, --Br, --CH.sub.3 or --OCH.sub.3 and X is --H, --Br, --OCH.sub.3, --CN or --NO.sub.2, are suitable as pigments, especially for coloring polyolefins, as well as novel intermediates of the formula ##STR4## wherein n is the number 1 or 2, R is a radical of the formula --OR.sub.3 or --NHR.sub.3, R.sub.1 is --H or --Cl, R.sub.2 is --H, halogen, --NO.sub.2, --CN, C.sub.1 -C.sub.4 alkyl, C.sub.1 -C.sub.4 alkoxy, --CF.sub.3, C.sub.2 -C.sub.5 alkoxycarbonyl or --CONH-phenyl, --NHCO-phenyl or phenoxy which is unsubstituted or substituted on the phenyl ring by one or two chlorine atoms or one or two methyl, methoxy or ethoxy groups, R.sub.3 is alkyl containing at least 10 C atoms, X is --H, --Br, --OCH.sub.3, --CN or --NO.sub.2 and Q is --OH or halogen.
摘要翻译：式I化合物：其中R是式-OR3或-NHR3基团，A是式II或III的基团：（III）B是式中的基团+图像n为数1或2，R 1为-H或-Cl，R 2为-H，卤素，-NO 2，-CN，C 1 -C 4烷基，C 1 -C 4烷氧基，-CF 3，C 2 -C 5烷氧基羰基或-CONH-苯基，-NHCO-苯基或苯氧基，其在苯环上未被取代或被一个或两个氯原子或一个或两个甲基，甲氧基或乙氧基取代，R3是含有至少10个C原子，R 4和R 5各自独立地为H，卤素，-NO 2，-CN，-CF 3，C 1 -C 4烷基或C 1 -C 4烷氧基，R 6为-H，-Cl，-Br， -CH 3或-OCH 3，X是-H，-Br，-OCH 3，-CN或-NO 2，适合作为颜料，特别是用于着色聚烯烃，以及下式的新型中间体：其中n为数1 或2，R是式-OR 3或-NHR 3的基团，R 1是-H或-Cl，R 2是-H，卤素，-NO 2，-CN，C 1 -C 4烷基，C 1 -C 4烷氧基，-CF 3， C2 -C 5烷氧基羰基或-CONH-苯基，-NHCO-苯基或苯氧基，其在苯环上未被取代或被一个或两个氯原子或一个或两个甲基，甲氧基或乙氧基取代，R3是含有至少10个C原子的烷基，X是-H，-Br，-OCH 3，-CN或-NO 2，Q是-OH或卤素。

5. 发明授权

US5395926A Bisazo, bisazomethine and azo-azomethine compounds derived from 1,4-phenylenediamine sulfonic acid salts 失效
标题翻译：双偶氮，双偶氮甲碱和衍生自1,4-苯二胺磺酸盐的偶氮偶氮甲碱化合物
公开(公告)号：US5395926A
公开(公告)日：1995-03-07
申请号：US125386
申请日：1993-09-22
申请人： Stefan Hari , Olof Wallquist
发明人： Stefan Hari , Olof Wallquist
IPC分类号： C07C309/45 , C07D213/85 , C07D215/22 , C07D231/20 , C07D231/22 , C07D231/26 , C07D239/47 , C07D239/52 , C07D403/12 , C07D487/04 , C09B35/03 , C09B35/033 , C09B35/04 , C09B55/00 , C09B56/02 , C09B63/00 , C09B69/04 , C09B31/14 , C08K5/00 , D06P5/06
CPC分类号： C09B56/02 , C09B35/03 , C09B35/033 , C09B55/005 , C09B63/005 , C09B69/045
摘要： Compounds of formula ##STR1## wherein R is hydrogen or a group ##STR2## M.sub.1 and M.sub.2 are each independently of the other an alkali metal or alkaline earth metal or aluminum or a group of formula ##STR3## wherein n is 1, 2 or 3, and R.sub.1, R.sub.2, R.sub.3 and R.sub.4 are hydrogen or C.sub.1 -C.sub.8 alkyl,X.sub.1 and X.sub.2 are each independently of the other --N.dbd. or --CH.dbd.,Q.sub.1 and Q.sub.2 are each independently of the other radicals of formula ##STR4## These compounds have excellent suitability for pigmenting organic material of high molecular weight, preferably polyolefins, and have superior lightfastness.
摘要翻译：式（I）的化合物其中R是氢或一个基团M1和M2各自独立地为碱金属或碱土金属或铝或其中n为1的式 2或3，R 1，R 2，R 3和R 4是氢或C 1 -C 8烷基，X 1和X 2各自独立地为-N =或-CH =，Q 1和Q 2各自独立地为式 > 这些化合物对于高分子量有机材料（优选聚烯烃）的着色具有优异的适用性，并且具有优异的耐光性。

6. 发明授权

US5280121A Perylenetetracarboxylic acid diimides containing long-chain alkanoylamino radicals 失效
标题翻译：含有长链烷酰氨基的苝四羧酸二酰亚胺
公开(公告)号：US5280121A
公开(公告)日：1994-01-18
申请号：US908504
申请日：1992-06-30
申请人： Stefan Hari
发明人： Stefan Hari
IPC分类号： C07D471/06 , C08K5/3437 , C09B5/62 , C07D221/18
CPC分类号： C07D471/06 , C08K5/3437 , C09B5/62
摘要： Compounds of formula ##STR1## wherein R is C.sub.7 -C.sub.21 alkyl, C.sub.4 -C.sub.18 alkenyl, C.sub.5 -C.sub.12 cycloalkyl or C.sub.5 -C.sub.6 cycloalkyl-substituted C.sub.1 -C.sub.4 alkyl,R.sub.1, R.sub.2, R.sub.3 and R.sub.4 are each independently of one another hydrogen, chloro, bromo, methyl or methoxy,Z is a direct bond or --O--, --S--, --NH--, --CO--, --SO.sub.2 -- or --NHCO--, andn is 0 or 1.These compounds have excellent suitability as pigments for coloring organic material of high molecular weight, especially polyvinyl chloride, polyolefins and paints.
摘要翻译：其中R为C 7 -C 21烷基，C 4 -C 18烯基，C 5 -C 12环烷基或C 5 -C 6环烷基取代的C 1 -C 4烷基，R 1，R 2，R 3和R 4各自独立地为氢，氯，溴，甲基或甲氧基，Z是直接键或-O - ， - S - ， - NH - ， - CO - ， - SO 2 - 或-NHCO-，n是0或1.这些化合物具有优异的适合性作为颜料用于着色高分子量的有机材料，特别是聚氯乙烯，聚烯烃和油漆。

7. 发明授权

US5151505A Amine salts of azo pigments based on pyrazolone derivatives 失效
标题翻译：基于吡唑啉酮衍生物的AZO颜料的胺盐
公开(公告)号：US5151505A
公开(公告)日：1992-09-29
申请号：US612764
申请日：1990-11-13
申请人： Stefan Hari , Georg Cseh
发明人： Stefan Hari , Georg Cseh
IPC分类号： C08K5/34 , C08K5/3442 , C08K5/3445 , C08K5/41 , C08K5/42 , C08L101/00 , C09B29/01 , C09B29/46 , C09B29/50 , C09B69/04
CPC分类号： C09B29/0007 , C09B29/366 , C09B69/045
摘要： Compounds of formula ##STR1## wherein a and b are each independently of the other halogen, --CH.sub.3, --C.sub.2 H.sub.5, --OC.sub.2 H.sub.5 or the group of formula --NHCO--C.sub.1 -C.sub.4 alkyl, c and d are each independently of the other hydrogen, halogen, --CH.sub.3, --C.sub.2 H.sub.5, --OCH.sub.3, --OC.sub.2 H.sub.5 or the group of formula --NHCO--C.sub.1 -C.sub.4 alkyl, and R.sup.1 is --CH.sub.3, phenyl, --COOCH.sub.3, --COOC.sub.2 H.sub.5, --NHCO--C.sub.1 -C.sub.4 alkyl or --CONH--C.sub.1 -C.sub.4 alkyl, and R.sup.2, R.sup.3, R.sup.4 and R.sup.5 are each independently hydrogen, C.sub.1 -C.sub.4 alkyl, unsubstituted or substituted by a chlorine atom or a --OH group, or are C.sub.7 -C.sub.9 aralkyl, C.sub.5 -C.sub.8 cycloalkyl, phenyl or phenyl which is substituted by 1 to 3 halogen atoms or methyl or methoxy groups, or is a heterocyclic radical of the benzimidazole, benzoxazole, benzthiazole or pyridine series, or R.sup.3 and R.sup.4, together with the linking nitrogen atom, are a pyrrolidine, imidazolidine, piperidine, piperazine or morpholine radical, or R.sup.3, R.sup.4 and R.sup.5, together with the linking nitrogen atom, are a pyrrole, pyridine, picoline, pyrazine, quinoline or isoquinoline radical, are most suitable for coloring high molecular organic material.

8. 发明授权

US4473500A Monoazo pigments derived from aminophthalimides and substituted acetoacetarylides or 2-hydroxy-3-naphthoylarylides 失效
标题翻译：衍生自氨基邻苯二甲酰亚胺和取代的乙酰乙酰胺或2-羟基-3-萘甲酰基的单偶氮颜料
公开(公告)号：US4473500A
公开(公告)日：1984-09-25
申请号：US374120
申请日：1982-05-03
申请人： Georg Cseh , Stefan Hari
发明人： Georg Cseh , Stefan Hari
IPC分类号： C09B29/09 , C09B29/00 , C09B29/20 , C09B29/33 , C09B29/036 , C09B29/32 , D06P1/44
CPC分类号： C09B29/337 , C09B29/0033 , C09B29/20
摘要： Monoazo pigment compounds of the formula ##STR1## wherein X is a group of the formula ##STR2## R is hydrogen or methyl, R.sub.1 and R.sub.2 are hydrogen, chlorine, methyl or methoxy, Y is methyl or phenyl, or Y is --O, --S--, --N(R.sub.3)-- or --C(R.sub.4).dbd.CH--, each of which is bound on the ring A in the ortho-position with respect to the --NHCO-- group to form a benzoxazolone, benzothiazolone, benzimidazolone or quinolone-2, with R.sub.3 and R.sub.4 being hydrogen or methyl, and m and n independently of one another are each 1 or 2, are useful as high-grade pigments, for pigmenting high-molecular weight organic material. The pigments are distinguished in particular by good fastness to light, migration and weather.
摘要翻译：其中X是下式的基团，其中X是氢或甲基，R 1和R 2是氢，氯，甲基或甲氧基，Y是甲基或苯基，或Y是-O， -S-，-N（R 3） - 或-C（R 4）= CH-，其各自相对于-NHCO-基团在邻位结合在环A上，形成苯并恶唑酮，苯并噻唑酮，苯并咪唑酮或喹诺酮-2，其中R 3和R 4为氢或甲基，m和n彼此独立地为1或2，可用作高级颜料，用于着色高分子量有机材料。颜料的特征是具有良好的耐光牢度，迁移性和耐候性。

9. 发明授权

US4062838A Disazo pigments containing acylamino groups 失效
标题翻译：含有酰氨基的双偶氮颜料
公开(公告)号：US4062838A
公开(公告)日：1977-12-13
申请号：US686431
申请日：1976-05-14
申请人： Georg Cseh , Stefan Hari
发明人： Georg Cseh , Stefan Hari
IPC分类号： C09B33/153 , C09B33/14
CPC分类号： C09B33/153
摘要： Disazo pigments of the formula ##STR1## wherein A denotes a phenylene or naphthylene radical, R denotes an aryl, alkyl or alkenyl group optionally substituted by halogen atoms, by hydroxyl, alkoxy or alkylmercapto groups containing 1-6 C atoms, by alkoxycarbonyl groups containing 2-6 C atoms or cyano, aryl, aryloxy, arylmercapto or heterocyclic radicals, or denotes a heterocyclic radical, and the X and Y denote H atoms or substituents which do not confer solubility in water are useful for coloring plastics lacquers and printing inks in yellow to orange shade of good fastness properties.
摘要翻译：其中A表示亚苯基或亚萘基，R表示任选被卤素原子取代的芳基，烷基或烯基，含1-6个碳原子的羟基，烷氧基或烷基巯基，通过含有 2-6个C原子或氰基，芳基，芳氧基，芳基巯基或杂环基，或表示杂环基，X和Y表示H原子或不赋予溶于水的取代基可用于着色塑料漆和印刷油墨黄色至橙色，色牢度好。

10. 再颁专利

USRE35359E Amine salts of azo pigments based on pyrazolone derivatives 失效
标题翻译：基于吡唑啉酮衍生物的偶氮颜料的胺盐
公开(公告)号：USRE35359E
公开(公告)日：1996-10-22
申请号：US312209
申请日：1994-09-26
申请人： Stefan Hari , Georg Cseh
发明人： Stefan Hari , Georg Cseh
IPC分类号： C08K5/34 , C08K5/3442 , C08K5/3445 , C08K5/41 , C08K5/42 , C08L101/00 , C09B29/01 , C09B29/46 , C09B29/50 , C09B69/04 , C09B29/03 , C09B29/10 , D06P1/44 , D06P5/00
CPC分类号： C09B29/0007 , C09B29/366 , C09B69/045
摘要： Compounds of formula ##STR1## wherein a and b are each independently of the other halogen, --CH.sub.3, --C.sub.2 H.sub.5, --OC.sub.2 H.sub.5 or the group of formula --NHCO--C.sub.1 -C.sub.4 alkyl, c and d are each independently of the other hydrogen, halogen, --CH.sub.3, --C.sub.2 H.sub.5, --OCH.sub.3, --OC.sub.2 H.sub.5 or the group of formula --NHCO--C.sub.1 -C.sub.4 alkyl, and R.sup.1 is --CH.sub.3, phenyl, --COOCH.sub.3, --COOC.sub.2 H.sub.5, --NHCO--C.sub.1 --C.sub.4 alkyl or --CONH--C.sub.1 -C.sub.4 alkyl, and R.sup.2, R.sup.3, R.sup.4 and R.sup.5 are each independently hydrogen, C.sub.1 -C.sub.4 alkyl, unsubstituted or substituted by a chlorine atom or a --OH group, or are C.sub.7 -C.sub.9 aralkyl, C.sub.6 -C.sub.8 cycloalkyl, phenyl or phenyl which is substituted by 1 to 3 halogen atoms or methyl or methoxy groups, or is a heterocyclic radical of the benzimidazole, benzoxazole, benzthiazole or pyridine series, or R.sup.3 and R.sup.4, together with the linking nitrogen atom, are a pyrrolidine, imidazolidine, piperidine, piperazine or morpholine radical, or R.sup.3, R.sup.4 and R.sup.5, together with the linking nitrogen atom, are a pyrrole, pyridine, picoline, pyrazine, quinoline or isoquinoline radical, are most suitable for coloring high molecular organic material.
摘要翻译：式（I）的化合物其中a和b各自独立于其它卤素，-CH 3，-C 2 H 5，-OC 2 H 5或式-NHCO-C 1 -C 4烷基基团，c和d各自独立地为另一个氢，卤素，-CH 3，-C 2 H 5，-OCH 3，-OC 2 H 5或式-NHCO-C 1 -C 4烷基的基团，并且R 1是-CH 3，苯基，-COOCH 3，-COOC 2 H 5，-NHCO-C 1 -C 4烷基或-CONH C 1 -C 4烷基，R 2，R 3，R 4和R 5各自独立地为氢，未被取代或被氯原子或-OH基取代的C 1 -C 4烷基，或者是C 7 -C 9芳烷基，C 6 -C 8环烷基，苯基或苯基，被1〜3个卤素原子取代或甲基或甲氧基，或者是苯并咪唑，苯并恶唑，苯并噻唑或吡啶系列的杂环基，或R3和R4与连接氮原子一起是吡咯烷，咪唑烷，哌啶，哌嗪或吗啉基，或R 3，R 4和R 5与连接氮原子一起为吡咯，吡啶，甲基吡啶，吡嗪，喹啉或异喹啉基，最适合着色高分子有机材料。

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