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1. 发明授权

US07071272B2 Method for preparing unsaturated compound by pyrolysis reaction 有权
标题翻译：通过热解反应制备不饱和化合物的方法
公开(公告)号：US07071272B2
公开(公告)日：2006-07-04
申请号：US10307388
申请日：2002-12-02
申请人： Takashi Okazoe , Kunio Watanabe , Shin Tatematsu , Masakuni Sato , Hidenobu Murofushi , Koichi Yanase , Yasuhiro Suzuki
发明人： Takashi Okazoe , Kunio Watanabe , Shin Tatematsu , Masakuni Sato , Hidenobu Murofushi , Koichi Yanase , Yasuhiro Suzuki
IPC分类号： C08F16/24
CPC分类号： C07C43/17 , C07C41/18 , C07C41/28 , C07C43/172 , C07C2601/14
摘要： The present invention provides a method for preparing a compound of CF3CF2CF2OCF═CF2 by pyrolyzing a compound expressed by CF3CF2CF2OCF(CF3)COOCF2CF(CF3)OCF2CF2CF3 in a gas phase at a temperature of from 200° C. to 500° C.
摘要翻译：本发明提供了通过以下方法制备CF 3 CF 2 CF 2 OCF-CF 2的化合物的方法：热解由CF 3 CF 2 CO 2 CF 2（CF 3）COOCF 2表示的化合物， / CF 2 CF 3 CF 3 CF 3 CF 3 CF 3 CF 3在气相中在温度为从200℃至500℃

2. 发明授权

US07009018B2 Tetrafluoroethylene copolymer 失效
标题翻译：四氟乙烯共聚物
公开(公告)号：US07009018B2
公开(公告)日：2006-03-07
申请号：US11080636
申请日：2005-03-16
申请人： Kazuya Oharu , Hidekazu Okamoto , Shin Tatematsu , Shigeki Kobayashi , Shinya Higuchi , Masataka Arai , Hiroki Nagai
发明人： Kazuya Oharu , Hidekazu Okamoto , Shin Tatematsu , Shigeki Kobayashi , Shinya Higuchi , Masataka Arai , Hiroki Nagai
IPC分类号： C08F116/12 , C08F16/24 , C08F216/12 , C08F114/18 , C08F14/18
CPC分类号： C08F214/26
摘要： Provided is a tetrafluoroethylene copolymer consisting of a unit based on tetrafluoroethylene and a unit based on a monomer represented by CF2═CFORf1Rf2 (where Rf1 is a polyfluoroalkylene group which may contain an etheric oxygen atom and Rf2 is a polyfluorocycloalkyl group which may contain an etheric oxygen atom), wherein a content of the latter is from 0.005 to 0.5% by mass. The tetrafluoroethylene copolymer is excellent both in paste extrudability and in heat resistance, has characteristics such as excellent transparency of a molded product, and is suitably applicable to paste extrusion and compression molding.
摘要翻译：提供一种四氟乙烯共聚物，其由基于四氟乙烯的单元和基于由CF 2 - （CH 2）2表示的单体组成的单元组成其中R f1是可以含有醚性氧原子的多氟亚烷基，R f2是可以含有醚性氧原子的多氟环烷基），其中后者的含量为0.005〜0.5质量％。四氟乙烯共聚物在糊状挤出性和耐热性方面优异，具有成型品的透明性优异的特性，适用于糊料挤出和压塑。

3. 发明授权

US06410808B1 Method for producing a fluoroalcohol 有权
标题翻译：氟代醇的制造方法
公开(公告)号：US06410808B1
公开(公告)日：2002-06-25
申请号：US09840072
申请日：2001-04-24
申请人： Yutaka Furukawa , Nobuyuki Kasahara , Kazuya Oharu , Shin Tatematsu
发明人： Yutaka Furukawa , Nobuyuki Kasahara , Kazuya Oharu , Shin Tatematsu
IPC分类号： C07C3134
CPC分类号： C07C41/26 , C07C29/124 , C07C43/137 , C07C31/38
摘要： A method for producing a fluoroalcohol of the following formula 1a, which comprises reacting a compound of the following formula 1 with water in a liquid phase at a temperature of 150° C. or higher under a gauge pressure of 0.4 MPa or higher: wherein n is an integer of from 1 to 5, X is a chlorine atom, a bromine atom or an iodine atom, p is an integer of at least 1, and R is a p-valent organic group, provided that when p is 1, R may be a hydrogen atom or a halogen atom.
摘要翻译：一种下式1a的氟代醇的制造方法，其特征在于，在表压为0.4MPa以上的条件下，使下式1的化合物与液相中的水在150℃以上的温度下反应：其中n 为1〜5的整数，X为氯原子，溴原子或碘原子，p为1以上的整数，R为p价有机基团，条件是当p为1时，R 可以是氢原子或卤素原子。

4. 发明授权

US06172270B2 Process for producing halogenated hydrocarbons 失效
标题翻译：卤代烃的制备方法
公开(公告)号：US06172270B2
公开(公告)日：2001-01-09
申请号：US09147432
申请日：1998-12-23
申请人： Shin Tatematsu
发明人： Shin Tatematsu
IPC分类号： C07C1708
CPC分类号： C07C17/21 , C07C17/206 , C07C19/08 , C07C19/12
摘要： A dichlorotrifluoroethane or the like is fluorinated with hydrogen fluoride in the presence of a fluorination catalyst which is a compound oxide of at least one metal selected from the group consisting of zinc, zirconium and manganese, and chromium, to produce R-125 and related intermediate products.
摘要翻译：二氯三氟乙烷等在氟化催化剂存在下氟化，氟化催化剂是选自锌，锆和锰的至少一种金属的复合氧化物和铬，以产生R-125和相关的中间体产品。

5. 发明授权

US07022300B2 Process for producing inorganic spheres 失效
标题翻译：生产无机球体的方法
公开(公告)号：US07022300B2
公开(公告)日：2006-04-04
申请号：US10618656
申请日：2003-07-15
申请人： Toshiya Matsubara , Masaharu Tanaka , Shin Tatematsu , Kazuhiko Yamada , Kenji Yamada , Kenichi Ebata , Hajime Katayama , Kentarou Tsunozaki
发明人： Toshiya Matsubara , Masaharu Tanaka , Shin Tatematsu , Kazuhiko Yamada , Kenji Yamada , Kenichi Ebata , Hajime Katayama , Kentarou Tsunozaki
IPC分类号： C01B33/12
CPC分类号： C01B33/124 , B01F3/0811 , B01F5/0475 , B01J13/06
摘要： A process for producing inorganic spheres, which comprises injecting an aqueous liquid containing an inorganic compound through an inlet hole into an organic liquid which flows at a flow rate of from 0.001 to 2 m/s in a laminar flow state in a flow path to form a W/O type emulsion, and solidifying the aqueous liquid containing an inorganic compound in the W/O type emulsion.
摘要翻译：一种无机球体的制造方法，其特征在于，将含有无机化合物的含水液体通过入口孔注入到以流路为流量的0.001〜2m / s的有机液体中，形成流路 W / O型乳液，并且在W / O型乳液中固化含有无机化合物的含水液体。

6. 发明授权

US06956138B2 Method for producing a fluorine-containing compound 有权
公开(公告)号：US06956138B2
公开(公告)日：2005-10-18
申请号：US10833048
申请日：2004-04-28
申请人： Takashi Okazoe , Kunio Watanabe , Shin Tatematsu , Masahiro Ito , Daisuke Shirakawa , Masao Iwaya , Hidekazu Okamoto
发明人： Takashi Okazoe , Kunio Watanabe , Shin Tatematsu , Masahiro Ito , Daisuke Shirakawa , Masao Iwaya , Hidekazu Okamoto
IPC分类号： C07C51/58 , C07C55/40 , C07C59/135 , C07C67/307 , C07C69/63 , C07C69/708 , C07C43/30 , C07C53/38
CPC分类号： C07C69/708 , C07C51/58 , C07C55/40 , C07C59/135 , C07C67/307 , C07C69/63
摘要： The present invention provides a method for obtaining a compound useful as a raw material for various fluororesins in high yield by a short process by using a starting material which is inexpensive and readily available.

7. 发明申请

US20050208531A1 Biochip substrate and process for its production 审中-公开
标题翻译：生物芯片基板及其生产工艺
公开(公告)号：US20050208531A1
公开(公告)日：2005-09-22
申请号：US11003417
申请日：2004-12-06
申请人： Hideo Nomoto , Kenji Ishizeki , Shin Tatematsu , Masayuki Ishimaru
发明人： Hideo Nomoto , Kenji Ishizeki , Shin Tatematsu , Masayuki Ishimaru
IPC分类号： C12M1/34 , C12Q1/68 , G01N21/64 , H01L21/00
CPC分类号： G01N21/6452
摘要： The object of the present invention is to provide a biochip substrate which affords accurate and sensitive measurements using a biochip by enhancing the S/N ratio of the fluorescence from each spot. A biochip substrate for producing a biochip by immobilizing a biological high-molecular-weight oligomer, which substantially reflects fluorescence on the surface on which the oligomer is to be immobilized. Preferably, a biochip substrate which consists essentially of a support and a coating formed on the surface of the support on which the biological high-molecular-weight oligomer is to be immobilized, wherein the coating comprises a reflective film which has a higher refractive index than the support.
摘要翻译：本发明的目的是提供一种生物芯片衬底，其通过增强每个斑点的荧光的S / N比，使用生物芯片提供准确和灵敏的测量。一种用于通过固定生物高分子量低聚物来生产生物芯片的生物芯片基底，其基本上反射了要固定低聚物的表面上的荧光。优选地，生物芯片基底，其基本上由支撑体和形成在其上固定有生物高分子量低聚物的载体的表面上的涂层组成，其中所述涂层包括具有比具有更高折射率的折射率的反射膜支撑。

8. 发明授权

US06858752B2 Process for producing fluorinated polyvalent carbonyl compound 失效
标题翻译：制备氟化多价羰基化合物的方法
公开(公告)号：US06858752B2
公开(公告)日：2005-02-22
申请号：US10397230
申请日：2003-03-27
申请人： Takashi Okazoe , Kunio Watanabe , Daisuke Shirakawa , Masahiro Ito , Shin Tatematsu
发明人： Takashi Okazoe , Kunio Watanabe , Daisuke Shirakawa , Masahiro Ito , Shin Tatematsu
IPC分类号： C07C45/41 , C07C45/54 , C07C51/60 , C07C67/14 , C07C67/287 , C07C67/29 , C07C67/297 , C07C67/307 , C07C69/63
CPC分类号： C07C67/14 , C07C45/54 , C07C51/60 , C07C67/287 , C07C67/29 , C07C67/297 , C07C67/307 , C07C59/21 , C07C53/46 , C07C69/63
摘要： A fluorinated polyvalent carbonyl compound is produced by an economically advantageous method from inexpensive materials without requiring a complicated synthetic process step. Namely, the present invention comprises reacting a polyvalent alcohol having at least two kinds of alcohol skeletons selected among a primary alcohol, a secondary alcohol and a tertiary alcohol, with an acid halide to obtain a polyvalent ester compound, fluorinating it in a liquid phase to obtain a perfluorinated polyvalent ester compound, and cleaving the ester bonds derived from primary and secondary alcohols in the perfluoropolyvalent ester compound to obtain a fluorinated polyvalent carbonyl compound.
摘要翻译：氟化的多价羰基化合物通过经济上有利的方法从便宜的材料制备而不需要复杂的合成工艺步骤。即，本发明包括使具有选自伯醇，仲醇和叔醇中的至少两种醇骨架的多元醇与酰卤反应，得到多价酯化合物，以液相氟化为获得全氟化多价酯化合物，并且在全氟聚酯化合物中裂解衍生自伯醇和仲醇的酯键，得到氟化多价羰基化合物。

9. 发明授权

US6166125A Graded-refractive-index optical plastic material and method for its production 有权
$Graded-refractive-index optical plastic material and method for its production$
标题翻译：渐变折射率光学塑料材料及其制造方法
公开(公告)号：US6166125A
公开(公告)日：2000-12-26
申请号：US164371
申请日：1998-10-01
申请人： Norihide Sugiyama , Hidenobu Murofushi , Takashi Okazoe , Masayuki Tamura , Shin Tatematsu , Jun Irisawa
发明人： Norihide Sugiyama , Hidenobu Murofushi , Takashi Okazoe , Masayuki Tamura , Shin Tatematsu , Jun Irisawa
IPC分类号： G02B1/04 , G02B6/02
CPC分类号： G02B1/046
摘要： A graded-refractive-index optical plastic material comprising an amorphous fluorine-containing polymer (A) having substantially no C--H bond, and at least one fluorine-containing polycyclic compound (B) having a refractive index higher by at least 0.005 than the fluorine-containing polymer (A), wherein the fluorine-containing polycyclic compound (B) is distributed in the fluorine-containing polymer (A) with a concentration gradient such that the concentration decreases in a direction of from the center to the periphery, and the fluorine-containing polycyclic compound (B) is at least one fluorine-containing polycyclic compound selected from the group consisting of the following compounds (B1), (B2) and (B3):(B1) a fluorine-containing non-condensed polycyclic compound having at least two fluorine-containing rings bonded by a bond containing at least one member selected from the group consisting of a triazine ring, an oxygen atom, a sulfur atom, a phosphorus atom and a metal atom, each of said fluorine-containing rings being a carbon ring or a heterocyclic ring and having a fluorine atom or a perfluoroalkyl group, said polycyclic compound having substantially no C--H bond;(B2) a fluorine-containing non-condensed polycyclic compound having at least three fluorine-containing rings bonded directly or by a bond containing a carbon atom, each of said fluorine-containing rings being a carbon ring or a heterocyclic ring and having a fluorine atom or a perfluoroalkyl group, said polycyclic compound having substantially no C--H bond;(B3) a fluorine-containing condensed polycyclic compound which is a condensed polycyclic compound composed of at least three carbon rings or heterocyclic rings, and which has substantially no C--H bond.
摘要翻译：包含基本上不含CH键的无定形含氟聚合物（A）和至少一种折射率高于含氟聚合物的折射率至少为0.005的含氟多环化合物（B）的渐变折射率光学塑料材料，含氟聚合物（A），其中所述含氟多环化合物（B）以浓度梯度使得所述浓度从所述中心向周向的方向下降，并且所述氟（B）是选自下列化合物（B1），（B2）和（B3）中的至少一种含氟多环化合物：（B1）含氟非缩合多环化合物，其具有通过含有选自三嗪环，氧原子，硫原子，磷原子和金属原子中的至少一种的键的至少两个含氟环，各自为所述含氟环是碳环或杂环，并且具有氟原子或全氟烷基，所述多环化合物基本上不含C-H键; （B2）具有至少三个含氟环的含氟非缩合多环化合物或者含有碳原子的键，所述含氟环是碳环或杂环，并且具有氟原子或全氟烷基，所述多环化合物基本上不含CH键; （B3）由至少三个碳环或杂环构成的并且基本上不含C-H键的缩合多环化合物的含氟缩合多环化合物。

10. 发明授权

US5334782A Method for producing a hydrogen-containing chloromethane 失效
标题翻译：含氢氯甲烷的制造方法
公开(公告)号：US5334782A
公开(公告)日：1994-08-02
申请号：US960423
申请日：1992-12-23
申请人： Shinsuke Morikawa , Masaru Yoshitake , Shin Tatematsu
发明人： Shinsuke Morikawa , Masaru Yoshitake , Shin Tatematsu
IPC分类号： B01J23/48 , B01J23/89 , C07C17/00 , C07C17/24 , C07C19/02 , C07C19/04
CPC分类号： C07C17/23 , B01J23/48 , B01J23/8926
摘要： The present invention relates to a method for producing a hydrogen-containing chloromethane such as chloroform at high selectivity in good yield by reducing a polychloromethane such as carbon tetrachloride in the presence of a reduction catalyst.In the present invention, it is important to conduct the reduction reaction in a liquid phase, whereby formation of impurities such as polymers which deactivate the catalyst, can effectively be suppressed, and the high selectivity and high activity of the reduction catalyst can adequately be obtained.As the reduction catalyst, at least one member selected from elements of Groups 8, 9 and 10, such as ruthenium, rhodium, palladium and platinum, may suitably be employed. Also a catalyst comprising, as the main component, such an element and having at least one member of Group 11 elements such as copper, silver and gold added thereto, may also suitably be employed.In a case where the liquid phase reduction reaction is conducted continuously, it is preferred to adopt a fixed bed system, particularly a trickle bed system.The method of the present invention is valuable also as a method for converting carbon tetrachloride which is regulated from the standpoint of global environmental protection, to chloroform which is useful as raw material for various fluorine-containing compounds.
摘要翻译： PCT No.PCT / JP92 / 00522 Sec。 371日期1992年12月23日 102（e）日期1992年12月23日PCT 1991年4月23日提交PCT公布。第WO92 / 18447号公报本发明涉及通过在还原催化剂的存在下还原多氯甲烷如四氯化碳，以高选择性以高产率生产含氢氯甲烷如氯仿的方法。在本发明中，重要的是在液相中进行还原反应，从而可以有效地抑制催化剂失活的诸如聚合物等杂质的形成，能够充分获得还原催化剂的高选择性和高活性。作为还原催化剂，可以适当选择选自元素8,9和10中的至少一种，例如钌，铑，钯和铂。还可以适当地使用包含作为主要成分的这种元素并且具有添加到其中的至少一种第11族元素如铜，银和金的元素的催化剂。在连续进行液相还原反应的情况下，优选采用固定床系统，特别是滴流床系统。本发明的方法作为从全球环境保护的角度将四氯化碳转化为可用作各种含氟化合物的原料的氯仿的方法也是有价值的。

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