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1. 发明授权

US5672785A Process for producing 1,1-dichloro-12,2,2-tetrafluoroethane 失效
标题翻译： 1,1-二氯-1,2,2,4-四氟乙烷的制备方法
公开(公告)号：US5672785A
公开(公告)日：1997-09-30
申请号：US390422
申请日：1995-02-17
申请人： Shinsuke Morikawa , Shunichi Samejima , Masaru Yoshitake , Shin Tatematsu
发明人： Shinsuke Morikawa , Shunichi Samejima , Masaru Yoshitake , Shin Tatematsu
IPC分类号： B01J23/02 , B01J21/02 , B01J23/26 , B01J23/74 , B01J23/745 , B01J23/75 , B01J23/755 , B01J27/125 , B01J27/128 , B01J27/132 , B01J27/138 , B01J37/22 , C07B61/00 , C07C17/00 , C07C17/20 , C07C17/358 , C07C19/08 , C07C19/12 , C07C67/00 , C07C17/37
CPC分类号： C07C19/12 , B01J37/22 , C07C17/206 , C07C17/358
摘要： A process for producing 1,1-dichloro-1,2,2,2-tetrafluoroethane, which comprises isomerizing 1,1,2-trichloro-1,2,2-trifluoroethane to form 1,1,1-trichloro-2,2,2-trifluoroethane, followed by fluorination with hydrofluoric acid.
摘要翻译： 1,1-二氯-1,2,2,2-四氟乙烷的制备方法，其包括使1,1,2-三氯-1,2,2-三氟乙烷异构化形成1,1,1-三氯-2,2-二氯，然后用氢氟酸氟化。

2. 发明授权

US5334782A Method for producing a hydrogen-containing chloromethane 失效
标题翻译：含氢氯甲烷的制造方法
公开(公告)号：US5334782A
公开(公告)日：1994-08-02
申请号：US960423
申请日：1992-12-23
申请人： Shinsuke Morikawa , Masaru Yoshitake , Shin Tatematsu
发明人： Shinsuke Morikawa , Masaru Yoshitake , Shin Tatematsu
IPC分类号： B01J23/48 , B01J23/89 , C07C17/00 , C07C17/24 , C07C19/02 , C07C19/04
CPC分类号： C07C17/23 , B01J23/48 , B01J23/8926
摘要： The present invention relates to a method for producing a hydrogen-containing chloromethane such as chloroform at high selectivity in good yield by reducing a polychloromethane such as carbon tetrachloride in the presence of a reduction catalyst.In the present invention, it is important to conduct the reduction reaction in a liquid phase, whereby formation of impurities such as polymers which deactivate the catalyst, can effectively be suppressed, and the high selectivity and high activity of the reduction catalyst can adequately be obtained.As the reduction catalyst, at least one member selected from elements of Groups 8, 9 and 10, such as ruthenium, rhodium, palladium and platinum, may suitably be employed. Also a catalyst comprising, as the main component, such an element and having at least one member of Group 11 elements such as copper, silver and gold added thereto, may also suitably be employed.In a case where the liquid phase reduction reaction is conducted continuously, it is preferred to adopt a fixed bed system, particularly a trickle bed system.The method of the present invention is valuable also as a method for converting carbon tetrachloride which is regulated from the standpoint of global environmental protection, to chloroform which is useful as raw material for various fluorine-containing compounds.
摘要翻译： PCT No.PCT / JP92 / 00522 Sec。 371日期1992年12月23日 102（e）日期1992年12月23日PCT 1991年4月23日提交PCT公布。第WO92 / 18447号公报本发明涉及通过在还原催化剂的存在下还原多氯甲烷如四氯化碳，以高选择性以高产率生产含氢氯甲烷如氯仿的方法。在本发明中，重要的是在液相中进行还原反应，从而可以有效地抑制催化剂失活的诸如聚合物等杂质的形成，能够充分获得还原催化剂的高选择性和高活性。作为还原催化剂，可以适当选择选自元素8,9和10中的至少一种，例如钌，铑，钯和铂。还可以适当地使用包含作为主要成分的这种元素并且具有添加到其中的至少一种第11族元素如铜，银和金的元素的催化剂。在连续进行液相还原反应的情况下，优选采用固定床系统，特别是滴流床系统。本发明的方法作为从全球环境保护的角度将四氯化碳转化为可用作各种含氟化合物的原料的氯仿的方法也是有价值的。

3. 发明授权

US5608126A Process for preparing 1,1,1,3,3-pentafluoropropane 失效
标题翻译：制备1,1,1,3,3-五氟丙烷的方法
公开(公告)号：US5608126A
公开(公告)日：1997-03-04
申请号：US494063
申请日：1995-06-23
申请人： Shinsuke Morikawa , Hidekazu Okamoto , Keiichi Ohnishi , Shin Tatematsu
发明人： Shinsuke Morikawa , Hidekazu Okamoto , Keiichi Ohnishi , Shin Tatematsu
IPC分类号： C07C17/20 , C07C17/278 , C07C19/08 , C07C17/08 , C07C21/18
CPC分类号： C07C19/08 , C07C17/206 , C07C17/278
摘要： A process for preparing 1,1,1,3,3-pentafluoropropane, which comprises reacting 1,1-difluoroethylene with dichlorofluoromethane in the presence of a Lewis acid catalyst to form 1,2,2-trihydrodichlorotrifluoropropane and fluorinating the 1,2,2-trihydrodichlorotrifluoropropane with hydrogen fluoride.
摘要翻译：一种制备1,1,1,3,3-五氟丙烷的方法，其包括在路易斯酸催化剂存在下使1,1-二氟乙烯与二氯一氟甲烷反应，形成1,2,2-三氢二氯三氟氟丙烷并氟化1,2， 2-氟二氟三氟甲烷与氟化氢反应。

4. 发明授权

US5426253A Process for producing 1,1,1,2-tetrafluoroethane 失效
标题翻译：生产1,1,1,2-四氟乙烷的方法
公开(公告)号：US5426253A
公开(公告)日：1995-06-20
申请号：US308612
申请日：1994-09-19
申请人： Shinsuke Morikawa , Shunichi Samejima , Masaru Yositake , Shin Tatematsu
发明人： Shinsuke Morikawa , Shunichi Samejima , Masaru Yositake , Shin Tatematsu
IPC分类号： C07C17/23 , C07C19/08
CPC分类号： C07C17/23
摘要： A process for producing 1,1,1,2-tetrafluoroethane, which comprises reacting 2,2-dichloro-1,1,1,2-tetrafluoroethane, 2-chloro-1,1,1,2-tetrafluoroethane or a mixture thereof with hydrogen in the presence of a hydrogenation catalyst consisting essentially of a Group VIII element as the main component and at least one element selected from the group consisting of Group IB elements, lanthanum and lanthanide elements, as an additional component.
摘要翻译：一种生产1,1,1,2-四氟乙烷的方法，其包括使2,2-二氯-1,1,1,2-四氟乙烷，2-氯-1,1,1,2-四氟乙烷或其混合物在基本上由VIII族元素作为主要成分组成的氢化催化剂和选自由IB族元素，镧和镧系元素组成的组中的至少一种元素作为附加成分的氢气存在下进行。

5. 发明授权

US5264639A Process for producing a 2,2-difluoropropane 失效
标题翻译： 2,2-二氟丙烷的制备方法
公开(公告)号：US5264639A
公开(公告)日：1993-11-23
申请号：US885250
申请日：1992-05-20
申请人： Shinsuke Morikawa , Shunichi Samejima , Hidekazu Okamoto , Keiichi Ohnishi , Shin Tatematsu , Toshihiro Tanuma , Takashi Ohmori
发明人： Shinsuke Morikawa , Shunichi Samejima , Hidekazu Okamoto , Keiichi Ohnishi , Shin Tatematsu , Toshihiro Tanuma , Takashi Ohmori
IPC分类号： C07C17/20 , C07C17/00 , C07C17/08
CPC分类号： C07C17/206 , C07C17/208
摘要： A process for producing a 2,2-difluoropropane of the following formula (2), which comprises fluorinating a chlorine-containing 2,2-halogenopropane of the following formula (1) by hydrogen fluoride or a fluorinating agent:C.sub.3 H.sub.a Cl.sub.b F.sub.c (1)C.sub.3 H.sub.a Cl.sub.b-x F.sub.c+x (2)wherein a, b, c and x are integers satisfying the following conditions:a.gtoreq.0, b.gtoreq.1, c.gtoreq.0, x.gtoreq.1, a+b+c=8.
摘要翻译：一种制备下式（2）的2,2-二氟丙烷的方法，其包括用氟化氢或氟化剂氟化下列式（1）的含氯2,2-二氯代丙烷：C3HaClbFc（1）C3HaClb -xFc + x（2）其中a，b，c和x是满足以下条件的整数：a> / = 0，b> / = 1，c> / = 0，x> / = 1，a + b + c = 8。

6. 发明授权

US5545777A Process for producing a hydrogen-containing 2,2-difluoropropane 失效
标题翻译：含氢的2,2-二氟丙烷的制造方法
公开(公告)号：US5545777A
公开(公告)日：1996-08-13
申请号：US272622
申请日：1994-07-11
申请人： Shinsuke Morikawa , Shunichi Samejima , Masaru Yoshitake , Hidekazu Okamoto , Keiichi Ohnishi , Toshihiro Tanuma
发明人： Shinsuke Morikawa , Shunichi Samejima , Masaru Yoshitake , Hidekazu Okamoto , Keiichi Ohnishi , Toshihiro Tanuma
IPC分类号： C07C17/23 , C07C19/08
CPC分类号： C07C17/23
摘要： A process for producing a hydrogen-containing 2,2-difluoropropane of the following formula (2), which comprises subjecting a 2,2-difluoropropane of the following formula (1) to hydrogen reduction:C.sub.3 H.sub.a Cl.sub.b F.sub.c (1)C.sub.3 H.sub.a+x Cl.sub.b-y F.sub.c-z (2)wherein a, b, c, x, y and z are integers satisfying the following conditions:a.gtoreq.0, b.gtoreq.1, c.gtoreq.2, x.gtoreq.1, y.gtoreq.0, z.gtoreq.0, a+b+c=8, x=y+z b-y.gtoreq.0, and c-z.gtoreq.2.
摘要翻译：一种制备下式（2）的含氢2,2-二氟丙烷的方法，包括使下式（1）的2,2-二氟丙烷进行氢还原：C3HaClbFc（1）C3Ha + xClb-yFc -z（2）其中a，b，c，x，y和z是满足以下条件的整数：a> / = 0，b> / = 1，c> / = 2，x> / = 1，y> / = 0，z> / = 0，a + b + c = 8，x = y + z by> / = 0，cz> / = 2。

7. 发明授权

US5320683A Azeotropic or azeotropic-like composition of hydrochlorofluoropropane 失效
标题翻译：共沸或共沸组合物的氢氯氟丙烷
公开(公告)号：US5320683A
公开(公告)日：1994-06-14
申请号：US941269
申请日：1992-09-04
申请人： Shunichi Samejima , Kenroh Kitamura , Naohiro Watanabe , Teruo Asano , Toru Kamimura , Shinsuke Morikawa
发明人： Shunichi Samejima , Kenroh Kitamura , Naohiro Watanabe , Teruo Asano , Toru Kamimura , Shinsuke Morikawa
IPC分类号： C07C19/10 , C11D7/50 , C23G5/028 , B08B3/00 , H05C3/26
CPC分类号： C23G5/02841 , C07C19/10 , C11D7/5045
摘要： A hydrochlorofluoropropane azeotropic or azeotropic-like composition comprising at least two members selected from the group consisting of hydrochlorofluoropropanes of the formula I:CH.sub.a Cl.sub.b F.sub.c CF.sub.2 CH.sub.x Cl.sub.y F.sub.z (I)wherein a+b+c=3, x+y+z=3, a+x.gtoreq.1, b+y.gtoreq.1, and 0.ltoreq.a,b,c,x,y,z.ltoreq.3.
摘要翻译：一种氢氯氟丙烷共沸或共沸组合物，其包含选自式I的氢氯氟丙烷中的至少两种成员：CHaClbFcCF2CHxClyFz（I）其中a + b + c = 3，x + y + z = 3，a + x> / = 1，b + y> / = 1，0 = a，b，c，x，y，z 3。

8. 发明授权

US06514425B1 Dry etching gas 有权
标题翻译：干蚀刻气体
公开(公告)号：US06514425B1
公开(公告)日：2003-02-04
申请号：US09297320
申请日：1999-07-02
申请人： Akira Sekiya , Tetsuya Takagaki , Shinsuke Morikawa , Shunichi Yamashita , Tsuyoshi Takaichi , Yasuo Hibino , Yasuhisa Furutaka , Masami Iwasaki , Norifumi Ohtsuka
发明人： Akira Sekiya , Tetsuya Takagaki , Shinsuke Morikawa , Shunichi Yamashita , Tsuyoshi Takaichi , Yasuo Hibino , Yasuhisa Furutaka , Masami Iwasaki , Norifumi Ohtsuka
IPC分类号： C03C1500
CPC分类号： H01L21/3065
摘要： Disclosed is fluorocarbon-based dry etching gas which is free of global environmental problems and a dry etching method using a plasma gas obtained therefrom. The dry etching gas includes a fluorinated ether of carbon, fluorine, hydrogen and oxygen and having 2-6 carbon atoms.
摘要翻译：公开了没有全球环境问题的基于碳氟化合物的干蚀刻气体，以及使用由其获得的等离子体气体的干蚀刻方法。干蚀刻气体包括碳，氟，氢和氧的具有2-6个碳原子的氟化醚。

9. 发明授权

US4372938A Producing sulfur tetrafluoride using amine/hydrogen fluoride complex 失效
标题翻译：使用胺/氟化氢络合物生产四氟化硫
公开(公告)号：US4372938A
公开(公告)日：1983-02-08
申请号：US370670
申请日：1982-04-22
申请人： Yoshio Oda , Hiroshi Otouma , Keiichi Uchida , Shinsuke Morikawa , Masaaki Ikemura
发明人： Yoshio Oda , Hiroshi Otouma , Keiichi Uchida , Shinsuke Morikawa , Masaaki Ikemura
IPC分类号： C01B17/45 , C10B17/00
CPC分类号： C01B17/4523
摘要： A process for producing sulfur tetrafluoride comprises reacting in the absence or presence of a solvent an amine/hydrogen fluoride complex having the formula:Am . (HF).sub.nwherein Am represents an amine selected from the group consisting of nitrogen-containing heterocyclic aromatic amines and derivatives thereof, and n represents 2-4, with sulfur dichloride, sulfur monochloride or a combination of chlorine and sulfur at a temperature of 0.degree. to 60.degree. C., the molar ratio of said amine/hydrogen fluoride complex to said sulfur dichloride, sulfur monochloride or sulfur being represented by the formula: ##EQU1## wherein n is as defined above, A represents moles of sulfur in said sulfur dichloride, sulfur monochloride or sulfur, and B represents moles of said amine/hydrogen complex.
摘要翻译：制备四氟化硫的方法包括在不存在或存在溶剂的情况下使具有下式的Am胺/氟化氢络合物反应。（HF）n其中Am表示选自含氮杂环芳族胺及其衍生物的胺，n表示2-4，二氯化硫，一氯化硫或氯和硫的组合，温度为0 所述胺/氟化氢络合物与所述二氯化硫，一氯化硫或硫的摩尔比由下式表示：其中n如上所定义，A表示所述硫中的硫的摩尔数二氯化物，一氯化硫或硫，B表示所述胺/氢络合物的摩尔数。

10. 发明授权

US06191327B1 Method for producing dichloropentafluoropropanes 失效
标题翻译：二氯五氟丙烷的制备方法
公开(公告)号：US06191327B1
公开(公告)日：2001-02-20
申请号：US08157429
申请日：1993-11-26
申请人： Shinsuke Morikawa , Keiichi Ohnishi , Hidekazu Okamoto , Toshihiro Tanuma
发明人： Shinsuke Morikawa , Keiichi Ohnishi , Hidekazu Okamoto , Toshihiro Tanuma
IPC分类号： C07C2118
CPC分类号： B01J27/135 , B01J27/08 , B01J27/125 , C07C17/278 , C07C19/10
摘要： The present invention relates to a simple method for producing 3,3-dichloro-1,1,1,2,2-pentafluoropropane (R225ca) and 1,3-dichloro-1,1,2,2,3-pentafluoropropane (R225cb) in good yield and at high selectivity by reacting tetrafluoroethylene (C2F4) and dichlorofluoromethane (R21) in the presence of a certain specific catalyst. The specific catalyst in the present invention is (1) a catalyst comprising halogenated oxide containing at least one element of Group 4, Group 5 and Group 13 such as Ti, Zr, Hf, V, B and Ga, or (2) a catalyst comprising halogenated oxide containing at least one element selected from Group 4, Group 5 and Group 13 such as Ti, Zr, Hf, V, B, Al and Ga and at least one element selected from Group 2, Group 6, Group 12 and Group 14 such as Ba, W, Zn, Si, Bi and P.
摘要翻译：本发明涉及制备3,3-二氯-1,1,1,2,2-五氟丙烷（R225ca）和1,3-二氯-1,1,2,2,3-五氟丙烷（R225cb）的简单方法），在一定的特定催化剂存在下，通过四氟乙烯（C 2 F 4）和二氯氟甲烷（R 21）的反应以高选择性。本发明中的具体催化剂是（1）包含含有至少一种元素第4族，第5族和第13族如Ti，Zr，Hf，V，B和Ga，或（2）包含选自第4族，第5族和第13族中的至少一种元素的卤代氧化物的催化剂， Zr，Hf，V，B，Al和Ga以及选自组2，组6，组12和组14中的至少一种元素如Ba，W，Zn，Si，Bi和P.

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