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1. 发明授权

US09492763B2 Method for producing microparticles having controlled crystallite diameter 有权
标题翻译：具有受控微晶直径的微粒的制造方法
公开(公告)号：US09492763B2
公开(公告)日：2016-11-15
申请号：US14232124
申请日：2012-07-05
申请人： Shiho Aoyagi , Kaeko Araki , Masaki Maekawa , Jun Kuraki , Masakazu Enomura
发明人： Shiho Aoyagi , Kaeko Araki , Masaki Maekawa , Jun Kuraki , Masakazu Enomura
IPC分类号： B01D9/00 , C04B35/626 , C22B15/00 , B01J19/18
CPC分类号： B01D9/0063 , B01D9/0054 , B01J19/1887 , B01J2219/00085 , B01J2219/00164 , B01J2219/00177 , C04B35/626 , C22B15/0089
摘要： At least two types of fluids to be processed are mixed in a thin film fluid formed between at least two processing surfaces which are approachably and separably disposed facing each other. At least one processing surface rotates relative to the other, and a substance to be separated giving a controlled crystallite diameter is caused to separate. Specific conditions related to a fluid to be processed are varied to control the crystallite diameter of the substance to be separated. The specific conditions are the type of substance to be separated; the concentration of the substance to be separated included in the raw material fluid and/or substance included in the separating fluid; the pH of the raw material fluid and/or separating material fluid; the introduction temperature of the raw material fluid and/or separating fluid; and the introduction velocity of the raw material fluid and/or separating fluid.
摘要翻译：要处理的至少两种类型的流体在形成在彼此面对地和可分离地布置的至少两个处理表面之间的薄膜流体中混合。至少一个处理表面相对于另一个处理表面旋转，并且使被分离得到受控微晶直径的物质分离。改变与待处理流体有关的特定条件以控制待分离物质的微晶直径。具体条件是要分离的物质的类型; 要分离的物质的浓度包括在分离流体中包含的原料流体和/或物质中; 原料流体和/或分离材料流体的pH; 原料流体和/或分离流体的引入温度; 以及原料流体和/或分离流体的引入速度。

2. 发明申请

US20140155247A1 METHOD FOR PRODUCING MICROPARTICLES HAVING CONTROLLED CRYSTALLITE DIAMETER 有权
标题翻译：用于生产具有控制的结晶直径的微孔的方法
公开(公告)号：US20140155247A1
公开(公告)日：2014-06-05
申请号：US14232124
申请日：2012-07-05
申请人： Shiho Aoyagi , Kaeko Araki , Masaki Maekawa , Jun Kuraki , Masakazu Enomura
发明人： Shiho Aoyagi , Kaeko Araki , Masaki Maekawa , Jun Kuraki , Masakazu Enomura
IPC分类号： B01D9/00 , C04B35/626 , C22B15/00
CPC分类号： B01D9/0063 , B01D9/0054 , B01J19/1887 , B01J2219/00085 , B01J2219/00164 , B01J2219/00177 , C04B35/626 , C22B15/0089
摘要： At least two types of fluids to be processed are mixed in a thin film fluid formed between at least two processing surfaces which are approachably and separably disposed facing each other. At least one processing surface rotates relative to the other, and a substance to be separated giving a controlled crystallite diameter is caused to separate. Specific conditions related to a fluid to be processed are varied to control the crystallite diameter of the substance to be separated. The specific conditions are the type of substance to be separated; the concentration of the substance to be separated included in the raw material fluid and/or substance included in the separating fluid; the pH of the raw material fluid and/or separating material fluid; the introduction temperature of the raw material fluid and/or separating fluid; and the introduction velocity of the raw material fluid and/or separating fluid.
摘要翻译：要处理的至少两种类型的流体在形成在彼此面对地和可分离地布置的至少两个处理表面之间的薄膜流体中混合。至少一个处理表面相对于另一个处理表面旋转，并且使被分离得到受控微晶直径的物质分离。改变与待处理流体有关的特定条件以控制待分离物质的微晶直径。具体条件是要分离的物质的类型; 要分离的物质的浓度包括在分离流体中包含的原料流体和/或物质中; 原料流体和/或分离材料流体的pH; 原料流体和/或分离流体的引入温度; 以及原料流体和/或分离流体的引入速度。

3. 发明授权

US09005567B2 Method for producing isolatable oxide microparticles or hydroxide microparticles 有权
标题翻译：生产可分离氧化物微粒或氢氧化物微粒的方法
公开(公告)号：US09005567B2
公开(公告)日：2015-04-14
申请号：US13818954
申请日：2011-08-26
申请人： Jun Kuraki , Kaeko Araki , Masaki Maekawa , Daisuke Honda , Masakazu Enomura
发明人： Jun Kuraki , Kaeko Araki , Masaki Maekawa , Daisuke Honda , Masakazu Enomura
IPC分类号： C01B13/14 , C01G23/047 , C01G23/053 , B01F7/00 , C01B13/36 , C01F5/02 , C01F5/20 , C01F5/14 , C01F17/00 , B01D9/00 , C01G25/02 , C01G1/02 , B82Y30/00
CPC分类号： C01G23/0536 , B01D9/0009 , B01F7/00775 , B01F7/00791 , B82Y30/00 , C01B13/36 , C01F5/02 , C01F5/14 , C01F5/20 , C01F17/0043 , C01G1/02 , C01G23/0532 , C01G25/02 , C01P2002/54 , C01P2004/04 , C01P2004/64
摘要： A method for producing isolatable oxide microparticles or hydroxide microparticles using an apparatus that processes a fluid between processing surfaces of processing members that are arranged opposite each other so as to be able to approach to or separate from each other and such that at least one can rotate relative to the other. At least two fluids are mixed and oxide microparticles or hydroxide microparticles are separated, said two fluids including: a fluid containing a microparticle raw material solution comprising a microparticle raw material mixed into a solvent, and a fluid containing a microparticle-separation solution. Immediately thereafter, the following are mixed to obtain isolatable oxide microparticles or hydroxide microparticles: a fluid containing the separated oxide microparticles or hydroxide microparticles; and a fluid containing a microparticle-treatment-substance-containing solution that contains a microparticle-treatment substance that adjusts the dispersibility of the separated oxide microparticles or hydroxide microparticles.
摘要翻译：一种用于制造可分离氧化物微粒或氢氧化物微粒的方法，该方法使用处理相互相对布置的处理构件的处理表面之间的流体以便能够彼此接近或分离并使得至少一个可旋转的装置相对于另一个。混合至少两种流体，分离氧化物微粒或氢氧化物微粒，所述两种流体包括：含有混合在溶剂中的微粒原料的微粒原料溶液的流体和含有微粒分离溶液的流体。之后，混合以下物质，得到可分离的氧化物微粒或氢氧化物微粒：含有分离的氧化物微粒或氢氧化物微粒的流体; 以及含有含微粒处理物质的溶液的流体，其含有调节分离的氧化物微粒或氢氧化物微粒的分散性的微粒处理物质。

4. 发明申请

US20140001663A1 METHOD FOR PRODUCING MICROPARTICLES 有权
标题翻译：生产微生物的方法
公开(公告)号：US20140001663A1
公开(公告)日：2014-01-02
申请号：US14005506
申请日：2012-03-21
申请人： Jun Kuraki , Kaeko Araki , Masaki Maekawa , Daisuke Honda , Masakazu Enomura
发明人： Jun Kuraki , Kaeko Araki , Masaki Maekawa , Daisuke Honda , Masakazu Enomura
IPC分类号： B01F3/22
CPC分类号： B01F3/22 , B01F7/00775 , B01F7/00791 , B01F13/1027 , B01F2215/0481 , B01J19/10 , B01J19/1806 , B01J19/1875 , B01J19/1887 , B01J19/20 , B01J2219/00779 , B82Y30/00 , C01G9/02 , C01P2004/54 , C01P2004/64
摘要： The problem addressed by the present invention is to provide a method for producing microparticles. Provided is a method that is for producing microparticles and that is characterized by containing at least the the following two steps: (I) a step for preparing a microparticle starting material solution by dissolving at least one type of microparticle starting material in a solvent using high speed stirring or ultrasonic waves, and (II) a step for precipitating microparticles by mixing the microparticle starting material solution and at least one type of precipitation solvent for precipitating the microparticle starting material in a thin film fluid formed between at least two processing surfaces that are disposed facing each other, are able to approach/separate from each other, and of which at least one rotates relative to the others.
摘要翻译：本发明提出的问题在于提供一种微粒的制造方法。本发明提供一种生产微粒的方法，其特征在于，至少包含以下两个步骤：（I）通过使用高分子量将至少一种微粒原料溶解在溶剂中来制备微粒原料溶液的步骤速度搅拌或超声波，以及（II）通过将微粒原料溶液和至少一种沉淀溶剂混合使微粒起始材料沉淀在形成在至少两个处理表面之间的薄膜流体中而使微粒沉淀的步骤彼此面对地布置，能够彼此接近/分离，并且其中至少一个相对于另一个旋转。

5. 发明授权

US09468891B2 Method for producing microparticles 有权
标题翻译：微粒的制造方法
公开(公告)号：US09468891B2
公开(公告)日：2016-10-18
申请号：US14005506
申请日：2012-03-21
申请人： Jun Kuraki , Kaeko Araki , Masaki Maekawa , Daisuke Honda , Masakazu Enomura
发明人： Jun Kuraki , Kaeko Araki , Masaki Maekawa , Daisuke Honda , Masakazu Enomura
IPC分类号： B01F3/22 , B01F7/00 , B01J19/10 , B01J19/18 , B01J19/20 , B82Y30/00 , C01G9/02 , B01F13/10
CPC分类号： B01F3/22 , B01F7/00775 , B01F7/00791 , B01F13/1027 , B01F2215/0481 , B01J19/10 , B01J19/1806 , B01J19/1875 , B01J19/1887 , B01J19/20 , B01J2219/00779 , B82Y30/00 , C01G9/02 , C01P2004/54 , C01P2004/64
摘要： The problem addressed by the present invention is to provide a method for producing microparticles. Provided is a method that is for producing microparticles and that is characterized by containing at least the following two steps: (I) a step for preparing a microparticle starting material solution by dissolving at least one type of microparticle starting material in a solvent using high speed stirring or ultrasonic waves, and (II) a step for precipitating microparticles by mixing the microparticle starting material solution and at least one type of precipitation solvent for precipitating the microparticle starting material in a thin film fluid formed between at least two processing surfaces that are disposed facing each other, are able to approach/separate from each other, and of which at least one rotates relative to the others.
摘要翻译：本发明提出的问题在于提供一种微粒的制造方法。本发明提供一种制造微粒的方法，其特征在于至少包含以下两个步骤：（I）通过使用高速将至少一种微粒起始材料溶解在溶剂中来制备微粒原料溶液的步骤搅拌或超声波，以及（II）通过将微粒原料溶液与至少一种沉淀溶剂混合，使微粒起始材料沉淀在形成在至少两个处理表面之间的薄膜流体中沉淀微粒的步骤彼此面对，能够彼此接近/分离，并且其中至少一个相对于其他旋转。

6. 发明申请

US20130156682A1 METHOD FOR PRODUCING ISOLATABLE OXIDE MICROPARTICLES OR HYDROXIDE MICROPARTICLES 有权
标题翻译：生产不溶性氧化镁微量元素或羟基微量元素的方法
公开(公告)号：US20130156682A1
公开(公告)日：2013-06-20
申请号：US13818954
申请日：2011-08-26
申请人： Jun Kuraki , Kaeko Araki , Masaki Maekawa , Daisuke Honda , Masakazu Enomura
发明人： Jun Kuraki , Kaeko Araki , Masaki Maekawa , Daisuke Honda , Masakazu Enomura
IPC分类号： C01G23/053 , C01F5/14 , C01F17/00
CPC分类号： C01G23/0536 , B01D9/0009 , B01F7/00775 , B01F7/00791 , B82Y30/00 , C01B13/36 , C01F5/02 , C01F5/14 , C01F5/20 , C01F17/0043 , C01G1/02 , C01G23/0532 , C01G25/02 , C01P2002/54 , C01P2004/04 , C01P2004/64
摘要： A method for producing isolatable oxide microparticles or hydroxide microparticles using an apparatus that processes a fluid between processing surfaces of processing members that are arranged opposite each other so as to be able to approach to or separate from each other and such that at least one can rotate relative to the other. At least two fluids are mixed and oxide microparticles or hydroxide microparticles are separated, said two fluids including: a fluid containing a microparticle raw material solution comprising a microparticle raw material mixed into a solvent, and a fluid containing a microparticle-separation solution. Immediately thereafter, the following are mixed to obtain isolatable oxide microparticles or hydroxide microparticles: a fluid containing the separated oxide microparticles or hydroxide microparticles; and a fluid containing a microparticle-treatment-substance-containing solution that contains a microparticle-treatment substance that adjusts the dispersibility of the separated oxide microparticles or hydroxide microparticles.
摘要翻译：一种用于制造可分离氧化物微粒或氢氧化物微粒的方法，该方法使用处理相互相对布置的处理构件的处理表面之间的流体以便能够彼此接近或分离并使得至少一个可旋转的装置相对于另一个。混合至少两种流体，分离氧化物微粒或氢氧化物微粒，所述两种流体包括：含有混合在溶剂中的微粒原料的微粒原料溶液的流体和含有微粒分离溶液的流体。之后，混合以下物质，得到可分离的氧化物微粒或氢氧化物微粒：含有分离的氧化物微粒或氢氧化物微粒的流体; 以及含有含微粒处理物质的溶液的流体，其含有调节分离的氧化物微粒或氢氧化物微粒的分散性的微粒处理物质。

7. 发明申请

US20140037519A1 METHOD FOR PRODUCING OXIDE/HYDROXIDE 有权
标题翻译：生产氧化物/氢氧化物的方法
公开(公告)号：US20140037519A1
公开(公告)日：2014-02-06
申请号：US14112887
申请日：2011-04-28
申请人： Jun Kuraki , Masaki Maekawa , Daisuke Honda , Masakazu Enomura
发明人： Jun Kuraki , Masaki Maekawa , Daisuke Honda , Masakazu Enomura
IPC分类号： C22B19/34 , C01G9/03
CPC分类号： C22B19/34 , B01F3/0807 , B01F7/00775 , B01F7/00791 , B01F15/0203 , B01F15/0243 , B01F15/0291 , B82Y30/00 , C01B13/32 , C01B13/34 , C01G9/02 , C01G9/03 , C01P2002/01 , C01P2002/72 , C01P2002/88 , C01P2004/04 , C01P2004/62 , C01P2004/64
摘要： Provided is a method for producing an oxide and/or hydroxide wherein the ratio of oxide and hydroxide has been controlled. The method produces an oxide, a hydroxide, or a mixture thereof, and obtains an oxide and/or a hydroxide wherein the ratio of oxide and hydroxide has been controlled by means of changing a specific condition relating to at least one fluid to be processed introduced between processing surfaces (1, 2) when causing the precipitation of the oxide, hydroxide, or mixture thereof by mixing an basic fluid containing at least one type of basic substance and a fluid containing at least one type of metal or metallic substance as the fluids to be processed between the processing surfaces (1, 2) that are provided facing each other, are able to approach to and separate from each other, and of which at least one rotates relative to the other. The specific condition is at least one condition selected from the group consisting of: the speed of introduction of at least one of the fluids to be processed; and the pH of at least one of the fluids to be processed.
摘要翻译：提供一种氧化物和/或氢氧化物的制造方法，其中氧化物和氢氧化物的比例已被控制。该方法产生氧化物，氢氧化物或其混合物，并获得氧化物和/或氢氧化物，其中氧化物和氢氧化物的比例已经通过改变与至少一种待处理流体相关的特定条件来控制当通过混合含有至少一种碱性物质的碱性流体和含有至少一种类型的金属或金属物质的流体作为流体而使氧化物，氢氧化物或其混合物沉淀时，处理表面（1,2）之间在彼此面对地设置的处理表面（1,2）之间进行处理，能够彼此接近并分离，并且至少一个相对于另一个旋转。所述具体条件是选自以下的至少一种条件：至少一种待处理流体的引入速度; 和至少一种要处理的流体的pH。

8. 发明授权

US09371236B2 Highly efficient method for producing ceramic microparticles 有权
标题翻译：高效制备陶瓷微粒的方法
公开(公告)号：US09371236B2
公开(公告)日：2016-06-21
申请号：US14004117
申请日：2011-03-23
申请人： Jun Kuraki , Masaki Maekawa , Daisuke Honda , Masakazu Enomura
发明人： Jun Kuraki , Masaki Maekawa , Daisuke Honda , Masakazu Enomura
IPC分类号： B01J14/00 , C01B33/113 , C01B13/14 , C01B21/00 , C01B19/00 , C01B31/00 , C01B33/00 , C01B35/00 , C01B9/00 , B01F7/00 , C01B33/193 , C01G9/02 , C01G23/00 , C01B13/36 , B01J19/18 , C01B13/16 , C04B35/626
CPC分类号： C01B33/113 , B01F7/00775 , B01F7/00791 , B01J14/00 , B01J19/1887 , C01B9/00 , C01B13/14 , C01B13/16 , C01B13/36 , C01B19/00 , C01B21/00 , C01B32/00 , C01B33/00 , C01B33/193 , C01B35/00 , C01G9/02 , C01G23/003 , C01P2002/72 , C01P2004/04 , C04B35/62625 , C04B2235/3284 , C04B2235/3418 , C04B2235/5445 , C04B2235/5454 , C04B2235/76
摘要： Provided is a more suitable method for producing ceramic microparticles. The present invention uses at least two types of fluids to be processed; at least one of the fluids to be processed is a fluid containing a ceramic starting material liquid that mixes and/or dissolves a ceramic starting material in a basic solvent; of the fluids aside from the ceramic starting material liquid, at least one of the fluids to be processed is a fluid containing a solvent for precipitating ceramic microparticles; and ceramic microparticles are precipitated by mixing the fluid containing the ceramic starting material liquid and the fluid containing the solvent for precipitating ceramic microparticles within a thin film fluid formed between at least two surfaces (1,2) for processing that are provided facing each other, are able to approach and separate each other, and of which one is able to rotate with respect to the other. Ceramic microparticles having as increased crystallinity are obtained by mixing the fluid containing the precipitated ceramic microparticles precipitate and a fluid containing an acidic substance.
摘要翻译：提供了一种更合适的陶瓷微粒的制造方法。本发明使用至少两种待处理的流体; 要处理的流体中的至少一种是含有在碱性溶剂中混合和/或溶解陶瓷原料的陶瓷原料液的流体; 的待处理流体中的至少一种是含有用于沉淀陶瓷微粒的溶剂的流体; 并且通过将包含陶瓷原料液的流体和含有溶剂的流体混合在陶瓷微粒沉淀物内形成的至少两个彼此面对的表面（1,2）之间形成的薄膜流体中来沉淀陶瓷微粒，能够彼此接近和分离，并且能够相对于另一个旋转。通过混合含有沉淀的陶瓷微粒沉淀物的液体和含有酸性物质的流体，获得结晶度增加的陶瓷微粒。

9. 发明申请

US20130343979A1 HIGHLY EFFICIENT METHOD FOR PRODUCING CERAMIC MICROPARTICLES 有权
标题翻译：用于生产陶瓷微生物的高效方法
公开(公告)号：US20130343979A1
公开(公告)日：2013-12-26
申请号：US14004117
申请日：2011-03-23
申请人： Jun Kuraki , Masaki Maekawa , Daisuke Honda , Masakazu Enomura
发明人： Jun Kuraki , Masaki Maekawa , Daisuke Honda , Masakazu Enomura
IPC分类号： C01B33/113 , C01G9/02
CPC分类号： C01B33/113 , B01F7/00775 , B01F7/00791 , B01J14/00 , B01J19/1887 , C01B9/00 , C01B13/14 , C01B13/16 , C01B13/36 , C01B19/00 , C01B21/00 , C01B32/00 , C01B33/00 , C01B33/193 , C01B35/00 , C01G9/02 , C01G23/003 , C01P2002/72 , C01P2004/04 , C04B35/62625 , C04B2235/3284 , C04B2235/3418 , C04B2235/5445 , C04B2235/5454 , C04B2235/76
摘要： Provided is a more suitable method for producing ceramic microparticles. The present invention uses at least two types of fluids to be processed; at least one of the fluids to be processed is a fluid containing a ceramic starting material liquid that mixes and/or dissolves a ceramic starting material in a basic solvent; of the fluids aside from the ceramic starting material liquid, at least one of the fluids to be processed is a fluid containing a solvent for precipitating ceramic microparticles; and ceramic microparticles are precipitated by mixing the fluid containing the ceramic starting material liquid and the fluid containing the solvent for precipitating ceramic microparticles within a thin film fluid formed between at least two surfaces (1,2) for processing that are provided facing each other, are able to approach and separate each other, and of which one is able to rotate with respect to the other. Ceramic microparticles having as increased crystallinity are obtained by mixing the fluid containing the precipitated ceramic microparticles precipitate and a fluid containing an acidic substance.
摘要翻译：提供了一种更合适的陶瓷微粒的制造方法。本发明使用至少两种待处理的流体; 要处理的流体中的至少一种是含有在碱性溶剂中混合和/或溶解陶瓷原料的陶瓷原料液的流体; 的待处理流体中的至少一种是含有用于沉淀陶瓷微粒的溶剂的流体; 并且通过将包含陶瓷原料液的流体和含有溶剂的流体混合在陶瓷微粒沉淀物内形成的至少两个彼此面对的表面（1,2）之间形成的薄膜流体中来沉淀陶瓷微粒，能够彼此接近和分离，并且能够相对于另一个旋转。通过混合含有沉淀的陶瓷微粒沉淀物的液体和含有酸性物质的流体，获得结晶度增加的陶瓷微粒。

10. 发明授权

US09127331B2 Method for producing oxide/hydroxide 有权
标题翻译：生产氧化物/氢氧化物的方法
公开(公告)号：US09127331B2
公开(公告)日：2015-09-08
申请号：US14112887
申请日：2011-04-28
申请人： Jun Kuraki , Masaki Maekawa , Daisuke Honda , Masakazu Enomura
发明人： Jun Kuraki , Masaki Maekawa , Daisuke Honda , Masakazu Enomura
IPC分类号： C22B19/00 , C22B19/34 , C01B13/32 , C01B13/34 , C01G9/02 , C01G9/03 , B01F7/00 , B01F15/02 , B01F3/08 , B82Y30/00
CPC分类号： C22B19/34 , B01F3/0807 , B01F7/00775 , B01F7/00791 , B01F15/0203 , B01F15/0243 , B01F15/0291 , B82Y30/00 , C01B13/32 , C01B13/34 , C01G9/02 , C01G9/03 , C01P2002/01 , C01P2002/72 , C01P2002/88 , C01P2004/04 , C01P2004/62 , C01P2004/64
摘要： Provided is a method for producing an oxide and/or hydroxide wherein the ratio of oxide and hydroxide has been controlled. The method produces an oxide, a hydroxide, or a mixture thereof, and obtains an oxide and/or a hydroxide wherein the ratio of oxide and hydroxide has been controlled by means of changing a specific condition relating to at least one fluid to be processed introduced between processing surfaces (1, 2) when causing the precipitation of the oxide, hydroxide, or mixture thereof by mixing an basic fluid containing at least one type of basic substance and a fluid containing at least one type of metal or metallic substance as the fluids to be processed between the processing surfaces (1, 2) that are provided facing each other, are able to approach to and separate from each other, and of which at least one rotates relative to the other. The specific condition is at least one condition selected from the group consisting of: the speed of introduction of at least one of the fluids to be processed; and the pH of at least one of the fluids to be processed.
摘要翻译：提供一种氧化物和/或氢氧化物的制造方法，其中氧化物和氢氧化物的比例已被控制。该方法产生氧化物，氢氧化物或其混合物，并获得氧化物和/或氢氧化物，其中氧化物和氢氧化物的比例已经通过改变与至少一种待处理流体相关的特定条件来控制当通过混合含有至少一种碱性物质的碱性流体和含有至少一种类型的金属或金属物质的流体作为流体而使氧化物，氢氧化物或其混合物沉淀时，处理表面（1,2）之间在彼此面对地设置的处理表面（1,2）之间进行处理，能够彼此接近并分离，并且至少一个相对于另一个旋转。所述具体条件是选自以下的至少一种条件：至少一种待处理流体的引入速度; 和至少一种要处理的流体的pH。

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